Detecting saturation levels of a core sample using magnetic fields

Patent metadata

Field	Value
Publication number	US-11327000-B2
Application number	US-201815984471-A
Country	US
Kind code	B2
Filing date	May 21, 2018
Priority date	May 21, 2018
Publication date	May 10, 2022
Grant date	May 10, 2022

Abstract

An example system is configured to detect saturation levels of a target, such as a core sample of a reservoir, using magnetic fields generated by hydrophilic magnetic nanoparticles within the target. The target contains both a hydrocarbon, such as oil or gas, and a mixture comprised of water and the hydrophilic magnetic nanoparticles. The system includes magnetic field detectors for spatial distribution across a dimension of the target. The magnetic field detectors are configured to detect a magnetic field associated with the hydrophilic magnetic nanoparticles. A data processing system is configured—for example, programmed—to determine a saturation profile of the target based on the magnetic field.

First claim

What is claimed is:

1. A system comprising:
magnetic field detectors for spatial distribution across a dimension of a target containing both a hydrocarbon and a mixture comprised of water and hydrophilic magnetic nanoparticles, the magnetic field detectors being configured to detect a magnetic field associated with the hydrophilic magnetic nanoparticles; and
a data processing system to determine a saturation profile of the target based on the magnetic field,
where the magnetic field detectors include a plurality of devices placed at discrete points on or in a sleeve of the target,
where the hydrophilic magnetic nanoparticles are immiscible in crude oil,
where the system comprises twelve magnetic field detectors arranged circumferentially around the core in three arrays of four magnetic field detectors each, and
where each magnetic field detector is offset 90 degrees from its circumferential neighbor.

2. The system of claim 1 , where the data processing system is configured to perform operations comprising:
obtaining first data based on the magnetic field, the first data representing a magnitude of the magnetic field and a direction of the magnetic field;
processing the first data to determine the saturation profile; and
outputting second data representing the saturation profile.

3. The system of claim 1 , where the data processing system is configured to determine, as part of the saturation profile, relative amounts of the hydrocarbon and the water across a dimension of the target, and
wherein the mixture contains between about 0.2 percent-by-weight (wt %) and about 0.3 wt % of hydrophilic magnetic nanoparticles.

4. The system of claim 1 , where the saturation profile comprises a magnitude component and a direction component, the magnitude component being indicative of an amount of water in the target and the direction component being indicative of a direction of flow of the water through the target.

5. The system of claim 1 , where the saturation profile comprises a temporal component and a spatial component, the temporal component being indicative of a duration of at least part of the spatial component.

6. The system of claim 1 , where the target is surrounded by the sleeve and a frame that are spaced with an annulus;
where the annulus is filled with a confining liquid;
where the target is a core of a reservoir formation comprised of porous rock, the core being held by a core holder;
where the magnetic field detectors are on the core holder; and
where the sleeve provides a seal around the core.

7. The system of claim 1 , where the hydrophilic magnetic nanoparticles have a stronger affinity with the water than with the hydrocarbon.

8. The system of claim 1 , where the magnetic field detectors comprise inductively-coupled coil arranged along a dimension of the target along which fluid flows through the target.

9. The system of claim 1 , where the magnetic field detectors comprise magnetometers arranged along a dimension of the target along which fluid flows through the target; and
where magnetometers include complementary metal-oxide semiconductor (CMOS).

10. The system of claim 9 , where the CMOS magnetometers are configured to determine, based on the magnetic field, a magnetic field strength vector in three dimensions, the magnetic field strength vector representing changes in magnetic field strength across the target;
where the CMOS magnetometers operate based upon the principle of tunneling magneto-resistance (TMR); and
where magnetic fields detected by two or more neighboring CMOS magnetometers are correlated using a computer-implemented process.

11. The system of claim 10 , where the magnetic field detectors are mounted on a flexible printed circuit board (PCB) on the sleeve.

12. The system of claim 10 , where each printed circuit board (PCB) containing a CMOS magnetometer includes a transceiver to enable direct wireless communications.

13. A method of generating a saturation profile of a target containing a hydrocarbon, the comprising:
forcing, through the target, a mixture comprised of water and hydrophilic magnetic nanoparticles to produce, within the target, a distribution of the mixture and the hydrocarbon;
detecting, by magnetic field detectors, a magnetic field associated with the hydrophilic magnetic nanoparticles within the target; and
generating the saturation profile of the target based on the magnetic field, the saturation profile representing at least part of the distribution,
where the magnetic field detectors include a plurality of devices placed at discrete points on or in a sleeve of the target,
where generating the saturation profile comprises determining, as part of the saturation profile, relative amounts of the hydrocarbon and the water across a length of the target, and
where generating the saturation profile comprises tracking a change in magnitude and a change in direction of magnetic field vectors of neighboring magnetic field detectors, the change in magnitude indicating a change in an amount of the mixture and the change in direction indicating a change in a flow direction of the mixture.

14. The method of claim 13 , where generating the saturation profile is performed using a data processing system and comprises:
obtaining first data based on the magnetic field, the first data representing a magnitude of the magnetic field and a direction of the magnetic field;
processing the first data to determine the saturation profile; and
outputting second data representing the saturation profile.

15. The method of claim 13 , where the saturation profile comprises a magnitude component and a direction component, the magnitude component being indicative of an amount of water in the target and the direction component being indicative of a direction of flow of the water through the target.

16. The method of claim 13 , where the saturation profile comprises a temporal component and a spatial component, the temporal component being indicative of a duration of at least part of the spatial component.

17. The method of claim 13 , where the target is surrounded by the sleeve and a frame that are spaced with an annulus;
where the annulus is filled with a confining liquid;
where the target is a core of a reservoir formation comprised of porous rock, the core being held by a core holder;
where detecting is performed by magnetic field detectors are on the core holder; and
where the sleeve provides a seal around the core.

18. The method of claim 17 , where the magnetic field detectors comprise inductively-coupled coil arranged along a dimension of the target along which fluid flows through the target, and
where the inductively-coupled coils comprise an inductance-capacitance-resistance (LCR) meter configured to receive, via a switch, signals from each of the inductively-coupled coils.

19. The method of claim 17 , where the magnetic field detectors comprise magnetometers arranged along a dimension of the target along which fluid flows through the target; and
where magnetometers include complementary metal-oxide semiconductor (CMOS).

20. The method of claim 19 , where the CMOS magnetometers are configured to determine, based on the magnetic field, a magnetic field strength vector in three dimensions, the magnetic field strength vector representing changes in magnetic field strength across the target;
where the CMOS magnetometers operate based upon the principle of tunneling magneto-resistance (TMR); and
where magnetic fields detected by two or more neighboring C

Assignees

• Saudi Arabian Oil Co
• Univ King Abdullah Sci & Tech

Inventors

• Karimi Muhammad Akram
• Ayub Muhammad
• Arsalan Muhammad
• Shamim Atif

Classifications

• G01N15/082 Primary

  Investigating permeability by forcing a fluid through a sample · CPC title

• G01N27/74 Primary

  of fluids (G01N24/00 takes precedence) · CPC title

• G01V3/10

  using induction coils · CPC title

• G01N15/0826

  and measuring fluid flow rate, i.e. permeation rate or pressure change · CPC title

• G01N33/24

  Earth materials (G01N33/42 takes precedence) · CPC title