Calcium oxide or magnesium oxide production with alkali and sulfur dioxide intermediates
US-12017985-B2 · Jun 25, 2024 · US
US11326233B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-11326233-B2 |
| Application number | US-202016918534-A |
| Country | US |
| Kind code | B2 |
| Filing date | Jul 1, 2020 |
| Priority date | Nov 18, 2014 |
| Publication date | May 10, 2022 |
| Grant date | May 10, 2022 |
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A method of manufacturing an iron soap is disclosed herein. The method comprising the steps of: reacting, at a temperature equal to or lower than a crystal transition initiation temperature of the iron soap to be manufactured, between a straight-chain saturated fatty acid alkali metal salt aqueous solution having from 12 to 22 carbons and a trivalent iron salt aqueous solution with pH of 0.1 to 5.5 so as to prepare an iron soap slurry; and adjusting pH of the prepared iron soap slurry to from 0.1 to 6.0.
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What is claimed is: 1. A method of manufacturing an iron soap having a content A (%) of free fatty acid being 0.01≤A≤8.0, a content B (%) of water soluble salt being 0.01≤B≤0.5, and a granularity summary value C indicated in Formula (1) being 0.1≤C≤5.0, wherein the iron soap is a salt of a straight-chain saturated fatty acid having from 12 to 22 carbons and an iron, Granularity summary value C =( D 90− D 10)/ D 50 (where 1.0≤ D 50≤40.0) Formula (1) D10: 10% cumulative diameter (μm) of fatty acid metal salt particles on a volumetric basis D50: 50% cumulative diameter (μm) of fatty acid metal salt particles on a volumetric basis D90: 90% cumulative diameter (μm) of fatty acid metal salt particles on a volumetric basis the method comprising the steps of: reacting, at a temperature equal to or lower than a crystal transition initiation temperature of the iron soap to be manufactured, between a straight-chain saturated fatty acid alkali metal salt aqueous solution having from 12 to 22 carbons and a trivalent iron salt aqueous solution with pH of 0.1 to 5.5 so as to prepare an iron soap slurry; and adjusting pH of the prepared iron soap slurry to from 0.1 to 6.0.
containing inorganic lubricating or binding agents, e.g. metal salts · CPC title
Mixtures obtained by warm mixing · CPC title
by conversion of the acids, their salts, esters or anhydrides with the same carboxylic acid part · CPC title
Additives containing two or more different additives of the same subgroup in C08K · CPC title
Compositions of detergents based essentially on soap (compositions containing resin soap C11D15/04) · CPC title
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