Method for additive manufacturing

Patent metadata

Field	Value
Publication number	US-11325191-B2
Application number	US-201715495250-A
Country	US
Kind code	B2
Filing date	Apr 24, 2017
Priority date	May 24, 2016
Publication date	May 10, 2022
Grant date	May 10, 2022

Abstract

A method for forming a three-dimensional article through successive fusion of parts of a metal powder bed is provided, comprising the steps of: distributing a first metal powder layer on a work table inside a build chamber, directing at least one high energy beam from at least one high energy beam source over the work table causing the first metal powder layer to fuse in selected locations, distributing a second metal powder layer on the work table, directing at least one high energy beam over the work table causing the second metal powder layer to fuse in selected locations, introducing a first supplementary gas into the build chamber, which first supplementary gas comprising hydrogen, is capable of reacting chemically with or being absorbed by a finished three-dimensional article, and releasing a predefined concentration of the gas which had reacted chemically with or being absorbed by the finished three dimensional article.

First claim

I claim:

1. An apparatus for forming a three-dimensional article through successive fusion of parts of a metal powder bed, which parts corresponds to successive cross sections of the three-dimensional article, the apparatus comprising:
a build chamber;
a working table onto which layers of metal powder are to be placed;
at least one high energy beam source; and
at least one control unit comprising a processor and computer program instructions that, when executed by the processor of the at least one control unit, cause the apparatus to:
distribute a first metal powder layer on a work table inside the build chamber,
direct at least one high energy beam from the at least one high energy beam source over the work table causing the first metal powder layer to fuse in selected locations to form a first cross section of the three-dimensional article,
distribute a second metal powder layer on the work table,
direct at least one high energy beam over the work table causing the second metal powder layer to fuse in selected locations to form a second cross section of the three-dimensional article, wherein the second layer is bonded to the first layer,
release a predefined concentration of at least one gas from the first metal powder layer into the build chamber when fusing the first metal powder layer and the second metal powder layer,
release a first supplementary gas into the build chamber, which first supplementary gas comprising hydrogen, is capable of reacting chemically with or being absorbed by the finished three-dimensional article, and
heat the finished three-dimensional article to a predetermined temperature at which a predefined concentration of the first supplementary gas which had reacted chemically with or being absorbed by the finished three-dimensional article is released from the finished three-dimensional article,

wherein the releasing of the predefined concentration of the first supplementary gas which had reacted chemically with or being absorbed by the three dimensional article is performed by holding the finished three-dimensional article at a predetermined temperature interval for a predefined time interval in the build chamber when a second supplementary gas is introduced into the build chamber, the second supplementary gas is free from H 2 .

2. The apparatus according to claim 1 , wherein the predefined concentration of the gas which is released from the finished three-dimensional article is at least 95% of the amount being absorbed or chemically reacted with the finished three-dimensional article.

3. The apparatus according to claim 1 , wherein the first supplementary gas further comprises at least one inert gas.

4. The apparatus according to claim 1 , wherein the first supplementary gas further comprises a gas selected from the group consisting of: deuterium, hydrocarbons, gaseous organic compounds, ammonia, nitrogen, oxygen, carbon monoxide, carbon dioxide, nitrogen, nitrous oxide, helium, Argon, Neon, Krypton, Xenon and Radon.

5. The apparatus according to claim 1 , wherein the metal powder is Ti, Ti-6Al-4V or any other Ti alloy and wherein the first supplementary gas, absorbed by or chemically reacted with the finished three-dimensional article, is capable of hydrogenizing the Ti, Ti-6Al-4V or the Ti alloy.

6. The apparatus according to claim 1 , wherein either:
the high energy beam is either an electron beam or a laser beam; or
the high energy beam is an electron beam and the build chamber is a vacuum chamber.

7. The apparatus according to claim 1 , wherein:
the at least one gas comprises hydrogen and is absorbed into or chemically bonded to the titanium or titanium alloy powder to a concentration of 0.01-0.5% by weight of the hydrogen; and
at least a portion of the released gas is configured for forming ions when being irradiated by the at least one electron beam such that ions are formed for balancing an amount of charged powder particles produced by the at least one electron beam to keep the electrical field strength below E max .

8. A method for forming a three-dimensional article through successive fusion of parts of a metal powder bed, which parts corresponds to successive cross sections of the three-dimensional article, the method comprising the steps of:
distributing a first metal powder layer on a work table inside a build chamber,
directing at least one high energy beam from at least one high energy beam source over the work table causing the first metal powder layer to fuse in selected locations to form a first cross section of the three-dimensional article,
distributing a second metal powder layer on the work table,
directing at least one high energy beam over the work table causing the second metal powder layer to fuse in selected locations to form a second cross section of the three-dimensional article, wherein the second layer is bonded to the first layer,
releasing a predefined concentration of at least one gas from the first metal powder layer into the build chamber when fusing the first metal powder layer and the second metal powder layer,
releasing a first supplementary gas into the build chamber, which first supplementary gas comprising hydrogen, is capable of reacting chemically with or being absorbed by the finished three-dimensional article, and
heating the finished three-dimensional article to a predetermined temperature at which a predefined concentration of the first supplementary gas which had reacted chemically with or being absorbed by the finished three-dimensional article is released from the finished three-dimensional article,
wherein the releasing of the predefined concentration of the first supplementary gas which had reacted chemically with or being absorbed by the three dimensional article is performed by holding the finished three-dimensional article at a predetermined temperature interval for a predefined time interval in the build chamber when a second supplementary gas is introduced into the build chamber, the second supplementary gas is free from H 2 .

9. The method according to claim 8 , wherein the predefined concentration of the gas which is released from the finished three-dimensional article is at least 95% of the amount being absorbed or chemically reacted with the finished three-dimensional article.

10. The method according to claim 8 , wherein the predefined concentration of the gas which is released from the finished three-dimensional article is at least 99% of the amount being absorbed or chemically reacted with the finished three-dimensional article.

11. The method according to claim 8 , wherein the first supplementary gas comprises at least one inert gas.

12. The method according to claim 8 , wherein the first supplementary gas comprises a gas selected from the group consisting of: deuterium, hydrocarbons, gaseous organic compounds, ammonia, nitrogen, oxygen, carbon monoxide, carbon dioxide, nitrogen, nitrous oxide, helium, Argon, Neon, Krypton, Xenon and/or Radon.

13. The method according to claim 8 , wherein the metal powder is Ti, Ti-6Al-4V or any other Ti alloy and wherein the first supplementary gas, absorbed by or chemically reacted with the finished three-dimensional article, is capable of hydrogenizing the Ti, Ti-6Al-4V or the Ti alloy.

14. The method according to claim 8 , wherein the releasing of a predefined concentration of the gas which had reacted chemically with or being absorbed by the three dimensional article is performed by holding the finished three-dimensional article at a predetermined temperature interval for a predefined time interval in the build chamber when a second supplementary gas is introduced into the build chambe

Assignees

• Arcam Ab

Inventors

• Ackelid Ulf

Classifications

• B33Y40/10

  Pre-treatment · CPC title

• B33Y70/00

  Materials specially adapted for additive manufacturing · CPC title

• B33Y40/20

  Post-treatment, e.g. curing, coating or polishing · CPC title

• B33Y40/00

  Auxiliary operations or equipment, e.g. for material handling · CPC title

• B22F10/28 Primary

  Powder bed fusion, e.g. selective laser melting [SLM] or electron beam melting [EBM] · CPC title