Biodegradable Magnetic Nanoparticles and Related Methods
US-2016250331-A1 · Sep 1, 2016 · US
US11325184B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-11325184-B2 |
| Application number | US-201916548081-A |
| Country | US |
| Kind code | B2 |
| Filing date | Aug 22, 2019 |
| Priority date | Aug 24, 2018 |
| Publication date | May 10, 2022 |
| Grant date | May 10, 2022 |
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A method for producing a powder-metallurgical product, in particular a bearing element or a motor component, is provided. According to the method, a metal powder, typically with a grain size between 2 μm and 15 μm, is melt-metallurgically produced and agglomerated into a powder mixture having a grain size smaller than 400 μm by organic binders and waxes. Subsequently, the agglomerated powder mixture is formed into a green body typically by way of uniaxial pressing and the formed green body thermally debindered. Finally, the debindered green body is sintered typically at temperatures of 1000° C. to 1300° C. and the sintered body reworked into the powder-metallurgical product.
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What is claimed is: 1. A method for producing a powder-metallurgical product comprising the steps of: a) melt-metallurgical producing a metal powder with a mean granulate size between 2 μm and 15 μm; b) agglomerating the metal powder produced in step a) by organic binders and waxes into a powder mixture containing 1 to 1.4% by weight of carbon, 27 to 39% by weight of chromium, 0.1 to 0.5% by weight of manganese, 3.1 to 4.0% by weight of nickel, 2.6 to 5.0% by weight of molybdenum, 2.1 to 3.5% by weight of silicon, 2.1 to 3.5% by weight of tungsten, 2.1 to 3.5% by weight of vanadium, 0.1 to 3.5% by weight of copper, and 0.0 to 3.5% by weight each of cobalt and niobium, with the mean granulate size of less than 400 μm; c) forming the powder mixture agglomerated in step b) into a green body by uniaxial pressing; d) thermal debindering the green body formed in step c); e) sintering the green body debindered in step d) at temperatures of 1000° C. to 1300° C.; and f) reworking the green body sintered in step e) into the powder-metallurgical product. 2. The method according to claim 1 , wherein the metal powder produced in step a) is iron based and/or contains more than 20% by weight of chromium and more than 1% by weight of carbon. 3. The method according to claim 1 , further comprising: in step b) admixing further metal powders with proportions smaller than or equal to 5% each and/or solid lubricants and/or hard phases and/or further metal powders on iron base. 4. The method according to claim 1 , further comprising: in step c), forming the powder mixture agglomerated in step b) into the green body under a pressure of 400 MPa to 1500 MPa. 5. The method according to claim 1 , further comprising: in step d), debindering the green body formed in step c) at temperatures from 45° C. to 820° C. 6. The method according to claim 1 , further comprising: in step e), sintering the green body debindered in step d) at a temperature between 1115° C. and 1275° C. 7. The method according to claim 1 , further comprising: in step a), producing the metal powder by water atomization. 8. The method according to claim 1 , further comprising: in step b), agglomerating the metal powder by spray drying.
Agglomerating · CPC title
Metallic powder containing lubricating or binding agents; Metallic powder containing organic material · CPC title
with copper · CPC title
Removal of binder or filler (removal of binder from ceramics C04B35/638) · CPC title
with niobium or tantalum · CPC title
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