Apparatus and method for particulate capture from gas streams and a method of removing soluble particulate from a gas

Patent metadata

Field	Value
Publication number	US-11298646-B2
Application number	US-201415036714-A
Country	US
Kind code	B2
Filing date	Nov 14, 2014
Priority date	Nov 15, 2013
Publication date	Apr 12, 2022
Grant date	Apr 12, 2022

Abstract

Disclosed is a method for the removal of soluble particulate matter from a gas stream, such as urea dust from the off-gas of a finishing section of a urea production plant. The method comprises subjecting the off-gas to at least two quenching stages an aqueous quenching liquid. The quenching liquid used in a first, upstream quench stage, is allowed to have a higher concentration of dissolved particulate matter than the quenching liquid in the second, downstream quench stage. The quenched gas is led through a particle capture zone, typically comprising one or more of a wet scrubber, a Venturi scrubber, and a wet electrostatic precipitator.

First claim

The invention claimed is:

1. A method for removing urea dust from a gas stream that contains urea dust and has a flowing direction, the method comprising:
providing off-gas from a finishing section of a urea plant as said gas stream comprising urea dust,
subjecting the gas stream containing said urea dust to quenching with aqueous quenching liquid to give a quenched gas and passing the quenched gas in said flowing direction through at least one particle capture zone,
wherein the gas stream is subjected to said quenching in at least an upstream stage and a downstream stage in series, using an upstream quenching liquid and a downstream quenching liquid, with the terms upstream and downstream being defined with reference to the flowing direction of the gas stream,
wherein the urea dust dissolves in the aqueous quenching liquid to give a resulting upstream quenching liquid in said upstream stage and a resulting downstream quenching liquid in said downstream stage comprising said urea dust dissolved therein to provide dissolved urea dust,
recirculating the resulting upstream quenching liquid via an upstream reservoir and recirculating the resulting downstream quenching liquid via a downstream reservoir, wherein the resulting downstream quenching liquid collected in the downstream reservoir has a lower concentration of said dissolved urea dust than the resulting upstream quenching liquid in the upstream reservoir, and
wherein the particle capture zone comprises a venturi scrubber and wherein the downstream stage is upstream of said venturi scrubber.

2. The method of claim 1 , wherein the quenching is conducted by spraying.

3. The method of claim 1 , wherein the concentration of the dissolved urea dust in the upstream quenching liquid is between 20% and 50% by weight.

4. The method of claim 3 , wherein the concentration of the dissolved urea dust in the downstream quenching liquid is between 0.1% and 5% by weight.

5. The method of claim 3 wherein the concentration of the dissolved urea dust in the upstream quenching liquid is between 40% and 45% by weight.

6. The method of claim 5 wherein the concentration of the dissolved urea dust in the downstream quenching liquid is between 0.5% and 2% by weight.

7. The method of claim 1 wherein in the venturi scrubber, a throat spray liquid is sprayed into the throat thereof.

8. A method for removing urea dust from an off-gas gas stream of a finishing section of a urea production plant, the method comprising:
providing the gas stream as off-gas from a finishing section of a urea plant, wherein the gas stream comprises urea dust and has a flowing direction, and
subjecting the gas stream to quenching to give a quenched gas and passing the quenched gas through a venturi scrubber,
wherein said quenching is carried out in at least a first quenching stage, which uses a first quenching liquid, and a second quenching stage, which uses a second quenching liquid, wherein the first quenching stage is upstream of the second stage in said flowing direction of the gas stream, and wherein the second quenching stage is arranged upstream of the venturi scrubber in said flowing direction of the gas stream, wherein the first stage comprises an upstream reservoir adapted to collect and recirculate the first quenching liquid to form a recirculated first quenching liquid and the second stage comprises a downstream reservoir adapted to collect and recirculate the second quenching liquid to form a recirculated second quenching liquid,
wherein the recirculated first quenching liquid contains between 20% and 50% by weight dissolved urea, and wherein the recirculated second quenching liquid contains between 0.1% and 5% by weight dissolved urea.

Assignees

• Stamicarbon

Inventors

• Higgins Brian Sayre

Classifications

• B01D2251/506

  Sulfuric acid · CPC title

• B01D2252/103

  Water · CPC title

• B01D2247/04

  Regenerating the washing fluid · CPC title

• B01D53/58

  Ammonia · CPC title

• C07C273/16

  Separation; Purification · CPC title