Distribution system using meridian panels for a simulated moving bed separation method using N columns in series

Patent metadata

Field	Value
Publication number	US-11298632-B2
Application number	US-201816758885-A
Country	US
Kind code	B2
Filing date	Oct 17, 2018
Priority date	Oct 27, 2017
Publication date	Apr 12, 2022
Grant date	Apr 12, 2022

Abstract

The present invention describes a fluid distribution and collection device of a simulated moving bed separation unit comprising N plates, themselves divided into meridian panels, which device makes it possible to maintain an approximately identical residence time for each portion of fluid.

First claim

The invention claimed is:

1. A distribution and collection device for the simulated moving bed separation units with a diameter of greater than 4 meters, the unit comprising at least one column divided into N beds of adsorbent, each bed being divided into meridian panels, i.e. into panels that are mutually parallel and contiguous so as to ensure complete coverage of the cross section of said bed, the distribution and collection device comprising distribution channels ( 4 ) and collection channels ( 8 ), and each panel being fed by a distribution channel ( 4 ), and the withdrawal of the effluents from said panel taking place via a collection channel ( 8 ), the distribution channel ( 4 ) and the collection channel ( 8 ) surrounding each panel having heights that vary linearly over the entire length of the panel, and being such that the inlet velocity in the bed of each portion of fluid remains the same from the inlet section of the panel to its outlet section of the panel, and the sum of the heights of the distribution channel and of the collection channel taken at any point of the length of the panel remains constant.

2. The distribution and collection device for simulated moving bed separation units as claimed in claim 1 , comprising outer peripheral ducts, wherein the passage of the fluids from plate N to the next plate N+1 takes place by means of a peripheral duct outside of the column and that makes it possible to connect the various collection channels of the plate N to the various distribution plates of the plate N+1, said duct making it possible to carry out injections of feedstock and of solvent and withdrawals of extract and of raffinate.

3. The distribution and collection device for simulated moving bed separation units as claimed in claim 2 , wherein the distribution of the fluids over the various panels takes place by successive divisions into two of the stream originating from the outer peripheral duct ( 10 ) in order to supply a group of two inlets ( 14 ) of adjacent panels, and the collection of the effluents from the bed N also takes place by successive combining, in twos, of the outlets ( 13 ) of two adjacent panels, which feeds the outer peripheral duct ( 10 ) of the bed N+1.

4. The distribution and collection device for simulated moving bed separation units as claimed in claim 1 , comprising distribution manifolds ( 15 ) and collection manifolds ( 16 ), wherein the distribution of the fluids over the various panels takes place from a distribution manifold ( 15 ) which directly supplies the various inlets ( 14 ) of each panel, and the collection of the effluents from the bed N takes place in the same manner directly by means of a collection manifold ( 16 ) which recovers the effluents from the outlets ( 13 ) of each panel.

5. A process using the distribution and collection device as claimed in claim 1 , wherein the incoming fluid is introduced into each panel of the plate N by means of inlet ducts ( 14 ), each inlet ( 14 ) supplying a distribution channel ( 4 ), the height of which is maximum at the inlet and minimum at the outlet of said channel, each portion of fluid supplying a fraction of the granular bed located immediately below the distribution channel, and said fraction of fluid leaving the granular bed in order to enter into the collection channel ( 8 ) located immediately below the granular bed, said collection channel having its maximum height at the outlet, the outlet effluent then being recovered by the outer peripheral duct ( 10 ), and being reintroduced via the inlets ( 14 ) of the bed N+1 into the distribution channel of said bed N+1, said process being characterized in that the residence time of each portion of fluid taken from the inlet of the plate N to the outlet of said plate N, is the same for each portion of fluid, and the outer peripheral duct ( 10 ) not adding any dispersion to this residence time.

6. An application of the distribution and collection device as claimed in claim 1 to the process for separating xylenes in a simulated moving bed operating with a number of beds of between 4 and 24, and preferentially of between 8 and 12.

Assignees

• Ifp Energies Now

Inventors

• Royon-Lebeaud Aude
• Augier Frederic

Classifications

• B01D15/1842 Primary

  characterised by apparatus features · CPC title

• C07C7/12

  by adsorption, i.e. purification or separation of hydrocarbons with the aid of solids, e.g. with ion-exchangers · CPC title