Method for producing sealant

Patent metadata

Field	Value
Publication number	US-11285449-B2
Application number	US-201816497950-A
Country	US
Kind code	B2
Filing date	Mar 22, 2018
Priority date	Mar 31, 2017
Publication date	Mar 29, 2022
Grant date	Mar 29, 2022

Abstract

A method for producing a sealant includes a weighing and mixing step, a kneading step, a stirring and defoaming step, and a filling step. In the weighing and mixing step, a main component and a curing agent are weighed and mixed together. In the kneading step, the mixture mixed in the weighing and mixing step is kneaded. In the stirring and defoaming step, the kneaded product kneaded in the kneading step is stirred and defoamed. In the filling step, the kneaded product defoamed in the stirring and defoaming step is filled into a container. In the stirring and defoaming step, the kneaded product is stirred under a condition wherein a stirring rotational speed at which the kneaded product is stirred and a stirring time for which the kneaded product is stirred are within a range from an arithmetic product lower limit value to an arithmetic product upper limit value.

First claim

The invention claimed is:

1. A method for producing a sealant, comprising:
a weighing and mixing step in which a main component and a curing agent are weighed out and mixed together;
a kneading step in which the mixture mixed in the weighing and mixing step is kneaded;
a stirring and defoaming step in which the kneaded product kneaded in the kneading step is stirred and defoamed; and
a filling step in which the kneaded product defoamed in the stirring and defoaming step is filled into a container;
wherein the method further comprises a step in which, before the stirring and defoaming step,
each of a plurality of amounts of the kneaded product for evaluation is stirred at one of various stirring rotational speeds for one of various stirring times,
each of the plurality of amounts of the kneaded product for evaluation that has been stirred is evaluated for whether or not voids are removed,
each of the plurality of amounts of the kneaded product for evaluation that has been stirred is discharged from a container to measure a discharge amount per unit time and evaluate whether or not the discharge amount is favorable based on the discharge amount that has been measured, and
an arithmetic product upper limit value that is an upper limit value of an arithmetic product of the stirring rotational speed and the stirring time according to the plurality of amounts of the kneaded product for evaluation when the voids are evaluated as being removed and the discharge amount is evaluated as being favorable is obtained, and
an arithmetic product lower limit value that is a lower limit value of the arithmetic product of the stirring rotational speed and the stirring time according to the plurality of amounts of the kneaded product for evaluation is obtained,

wherein, in the stirring and defoaming step,
the kneaded product is stirred under a condition in which the arithmetic product of a stirring rotational speed at which the kneaded product is stirred and a stirring time for which the kneaded product is stirred is within a range from the arithmetic product lower limit value to the arithmetic product upper limit value that are predetermined according to an amount of the kneaded product to be stirred.

2. The method for producing a sealant according to claim 1 ,
wherein the arithmetic product lower limit value and the arithmetic product upper limit value are set so that the stirring time is within a range from an upper limit value to a lower limit value of the preset stirring time.

3. The method for producing a sealant according to claim 2 , wherein:
the upper limit value of the stirring time is 3 minutes, and
the lower limit value of the stirring time is 0.5 minutes.

4. The method for producing a sealant according to claim 3 , wherein:
the amount of the kneaded product to be stirred is 270 g to 370 g,
the stirring rotational speed is 700 rpm, and
the stirring time is 120 seconds.

5. The method for producing a sealant according to claim 3 ,
wherein, in the stirring and defoaming step, stirring is performed by setting the temperature of the kneaded product kneaded in the weighing and mixing step to 10 degrees to 32 degrees Celsius.

6. The method for producing a sealant according to claim 3 , comprising
a freezing step in which the kneaded product filled into the container is frozen.

7. The method for producing a sealant according to claim 2 , wherein:
the amount of the kneaded product to be stirred is 270 g to 370 g,
the stirring rotational speed is 700 rpm, and
the stirring time is 120 seconds.

8. The method for producing a sealant according to claim 2 ,
wherein, in the stirring and defoaming step, stirring is performed by setting the temperature of the kneaded product kneaded in the weighing and mixing step to 10 degrees to 32 degrees Celsius.

9. The method for producing a sealant according to claim 2 , comprising
a freezing step in which the kneaded product filled into the container is frozen.

10. The method for producing a sealant according to claim 1 , wherein:
the amount of the kneaded product to be stirred is 270 g to 370 g,
the stirring rotational speed is 700 rpm, and
the stirring time is 120 seconds.

11. The method for producing a sealant according to claim 10 ,
wherein, in the stirring and defoaming step, stirring is performed by setting the temperature of the kneaded product kneaded in the weighing and mixing step to 10 degrees to 32 degrees Celsius.

12. The method for producing a sealant according to claim 10 , comprising
a freezing step in which the kneaded product filled into the container is frozen.

13. The method for producing a sealant according to claim 1 ,
wherein, in the stirring and defoaming step, stirring is performed by setting the temperature of the kneaded product kneaded in the weighing and mixing step to 10 degrees to 32 degrees Celsius.

14. The method for producing a sealant according to claim 13 , comprising
a freezing step in which the kneaded product filled into the container is frozen.

15. The method for producing a sealant according to claim 1 , comprising
a freezing step in which the kneaded product filled into the container is frozen.

Assignees

• Mitsubishi Heavy Ind Ltd
• Kaga Sangyo Co Ltd
• Kaga Works Co Ltd

Inventors

• Yamane Shigemi
• Mizoguchi Osamu
• Tsujikawa Hitoshi

Classifications

• B29B7/845 Primary

  Venting, degassing or removing evaporated components in devices with rotary stirrers · CPC title

• B01F2215/0481

  Numerical speed values · CPC title

• B65B3/12

  mechanically, e.g. by pistons or pumps · CPC title

• B01F2101/2204

  Mixing chemical components in generals in order to improve chemical treatment or reactions, independently from the specific application · CPC title

• B29B7/005

  for mixing in batches · CPC title