Sintered porous material having nodes and fibers of different materials, with different sintering points, and related methods of preparation and use

Patent metadata

Field	Value
Publication number	US-11273492-B2
Application number	US-201816762421-A
Country	US
Kind code	B2
Filing date	Nov 2, 2018
Priority date	Nov 8, 2017
Publication date	Mar 15, 2022
Grant date	Mar 15, 2022

Abstract

Described are porous sintered metal bodies, methods of making and using the porous sintered metal bodies, and methods of using the porous sintered metal bodies for commercial applications that include filtering a fluid, including in applications requiring high efficiency (high LRV) filtration.

First claim

The invention claimed is:

1. A porous sintered metal body comprising a metal matrix comprising elongate metal fibers connected at connective metal nodes, the matrix comprising:
connective metal nodes comprising a first metal material having a first sintering point;
elongate metal fibers of a second metal material having a second sintering point that is greater than the first sintering point;
wherein the first metal material and the second metal material are different, and wherein the connective metal nodes are fused to the elongate metal fibers without the elongate metal fibers being fused to each other to form an interconnected metal matrix comprising the elongate metal fibers connected by and extending between the connective metal nodes.

2. The porous sintered metal body of claim 1 comprising:
from 30 to 70 weight percent of the first metal material, and
from 70 to 30 weight percent of the second metal material.

3. The porous sintered metal body of claim 1 comprising less than 1 weight percent non-metal material.

4. The porous sintered metal body of claim 1 wherein the second sintering point is at least 200 degrees Celsius higher than the first sintering point.

5. The porous sintered metal body of claim 1 wherein the first sintering point is in a range from 530 to 630 degrees Celsius.

6. The porous sintered metal body of claim 1 wherein the first metal material is nickel or a nickel alloy.

7. The porous sintered metal body of claim 1 wherein the second metal material is stainless steel.

8. The porous sintered metal body of claim 1 having a porosity in a range from 70 to 90 percent.

9. The porous sintered metal body of claim 1 having a surface area defined by the Brunauer, Emmett and Teller (BET) theory of at least 0.30 meter 2 per gram.

10. The porous sintered metal body of claim 1 having a thickness that is less than 1 millimeter.

11. The porous sintered metal body of claim 1 in the form of a closed cylinder.

12. A method of forming a metal matrix that includes elongate metal fibers connected at connective metal nodes, the method comprising:
providing a blend of metal particles including powdered metal particles of a first metal material having a first sintering point, elongate metal fiber particles of a second metal material having a second sintering point, and with the second sintering point being above the first sintering point, wherein the first metal material and the second metal material are different; and
sintering the blend at a temperature that is above the first sintering point and below the second sintering point to sinter the powdered metal material to the elongate metal fiber particles but not cause the elongate metal fiber particles to sinter to each other and form a metal matrix comprising the elongate metal fibers connected at connective metal nodes formed by sintering the powdered metal particles.

13. The method of claim 12 comprising:
placing the blend in a mold;
pressing the blend, in the mold and
sintering the blend in the mold.

14. The method of claim 13 wherein the blend of metal materials has an apparent density of less than 0.5 grams per cubic centimeter before being placed in the mold.

Assignees

• Entegris Inc

Inventors

• Zeller Robert S

Classifications

• B22F1/062

  Fibrous particles · CPC title

• B22F1/052

  characterised by a mixture of particles of different sizes or by the particle size distribution · CPC title

• B22F1/05

  Metallic powder characterised by the size or surface area of the particles · CPC title

• Y10T428/12056

  Entirely inorganic · CPC title

• B01D2239/1233

  Fibre diameter · CPC title