Method for forming powder particles and a product

Patent metadata

Field	Value
Publication number	US-11247269-B2
Application number	US-201615572350-A
Country	US
Kind code	B2
Filing date	Apr 27, 2016
Priority date	May 7, 2015
Publication date	Feb 15, 2022
Grant date	Feb 15, 2022

Abstract

The invention relates to a method for forming powder particles, wherein the method comprises feeding a start material mixture including more than one constituents in the form of granules into a reactor comprising a reaction zone and a heat source, performing thermal synthesis in the reaction zone in which the start material mixture is moved and the constituents of the start material mixture react in the presence of heat so that the reaction is started by means of heat of the reactor and energy of the start material mixture is released in the form of heat in order to achieve the reaction, and producing powder particles during the reaction. Further, the invention relates to a powder particle product.

First claim

The invention claimed is:

1. A method for forming powder particles, the method comprising:
forming granules from a start material mixture including more than one constituent by granulating the start material mixture to the granules which comprise at least two constituents, the size of which is below 0.5 mm,
feeding the granules into a reaction zone of the reactor in which a thermal process is performed and the reactor comprises a flame-based heating unit,
performing the thermal process, as an in-situ synthesis in the reaction zone in which the granules are moved and the constituents of the granules react in the presence of heat to form composite powder particles, and the reaction is started by means of heat of the flame-based heating unit and heat energy is generated by means of the reaction in the reaction zone and is released in order to sustain the reaction between the constituents, and
producing directly the composite powder particles, wherein the particle size is below 500 μm and wherein the powder particles are carbide-based composite powder particles, during the reaction in the reaction zone.

2. The method according to claim 1 , wherein the start material mixture includes a binder that facilitates the formation of granules during the method, the binder being chosen from the group consisting of carbon, titanium oxide, aluminum oxide, and combinations thereof.

3. The method according to claim 1 , wherein the start material mixture is selected from the group consisting of: carbon, titanium, silicon, hafnium, zirconium, tantalum, boron, nitrogen, iron, nickel, cobalt, aluminum, and combinations thereof.

4. The method according to claim 1 , wherein the flame-based heating unit is sufficient to produce a processing temperature of at least 1100° C.

5. The method according to claim 1 , wherein a high processing temperature of at least 1100° C. and short retention time of less than 5 seconds are used in the reaction zone.

6. The method according to claim 1 , wherein the start material mixture is fluidized in the reaction zone.

7. The method according to claim 1 , wherein protective gas is used for avoiding oxidation in the reactor.

8. The method according to claim 1 , wherein the start material mixture feed, heat of the reactor and processing time are controllable and adjustable in the reactor.

9. The method according to claim 1 , wherein the powder particles are oxide metal particles, oxide-carbide particles.

Assignees

• Teknologian Tutkimuskeskus Vtt Oy

Inventors

• Lindroos Tomi
• Kanerva Ulla
• Lagerbom Juha
• Lintunen Pertti

Classifications

• B22F1/142

  Thermal or thermo-mechanical treatment · CPC title

• B22F1/065

  Spherical particles · CPC title

• B33Y70/00

  Materials specially adapted for additive manufacturing · CPC title

• B22F2301/205

  Titanium, zirconium or hafnium · CPC title

• B01J8/18

  with fluidised particles {(combustion apparatus with fluidised bed in general F23C10/00; furnaces with fluidised bed F27B15/00)} · CPC title