Method of producing beer having a tailored flavour profile

Patent metadata

Field	Value
Publication number	US-11242501-B2
Application number	US-202016740933-A
Country	US
Kind code	B2
Filing date	Jan 13, 2020
Priority date	Sep 5, 2014
Publication date	Feb 8, 2022
Grant date	Feb 8, 2022

Abstract

A method of producing beer having a tailored flavour profile is provided comprising the successive steps of: (a) fermenting wort containing fermentable sugars with yeast to produce beer containing 1-10 vol. % ethanol and flavour substances diacetyl; acetaldehyde; dimethyl sulfide; ethyl acetate; isoamyl acetate; ethyl valerate; ethyl hexanoate; iso-amyl alcohol and 2-methylbutan-1-ol; (b) contacting the fermenting wort or beer with porous adsorbent particles, selectively adsorbing the beer flavour esters ethyl acetate, ethyl hexanoate, ethyl valerate and isoamyl acetate; (c) separating the adsorbent particles; (d) desorbing a portion of the beer flavour esters from the adsorbent particles; and (e) adding a fraction of the desorbed beer flavour esters to the flavour adjusted beer or to another beer, wherein the amount of beer flavour esters added is 5-95 wt. % of the amount of beer flavour esters removed by the adsorbent particles.

First claim

What is claimed is:

1. A method of producing beer, comprising the successive steps of:
(a) fermenting a wort containing fermentable sugars with an active yeast to produce a beer comprising 1-10 vol. % ethanol and beer flavour substances diacetyl, acetaldehyde, dimethyl sulphide, ethyl acetate, isoamyl acetate, ethyl valerate, ethyl hexanoate, iso-amyl alcohol, and 2-methylbutan-1-ol;
(b) contacting the fermenting wort or the beer with porous adsorbent particles to selectively adsorb one or more surplus flavour substances selected from diacetyl, acetaldehyde, and dimethyl sulphide, the adsorbent particles having a high affinity for one or more of the surplus flavour substances and a lower affinity for ethanol and the other beer flavour substances; and
(c) separating the adsorbent particles containing the one or more adsorbed surplus flavour substances from the beer to produce a flavour adjusted beer comprising 1-10 vol. % ethanol;
wherein the porous adsorbent particles comprise an adsorbent containing amine functionalities; and wherein the adsorbent particles' affinity ratio Oi for at least one of the surplus flavour substances exceeds 5;
the affinity ratio θ 1 for surplus flavour substance i being defined by the following equation: θ i =K i /K ethanol , wherein:
(i) K i represents the adsorbent particles' affinity constant for surplus flavour substance i; and
(ii) K ethanol represents the adsorbent particles' affinity constant for ethanol.

2. The method according to claim 1 , wherein the beer is contacted with the porous adsorbent particles.

3. The method according to claim 2 , wherein the beer is contacted with the adsorbent particles after the beer has been heated to a temperature of at least 60° C. for at least 5 minutes.

4. The method according to claim 1 , wherein the affinity ratio θ i for diacetyl exceeds 5.

5. The method according to claim 4 , wherein the affinity ratio θ i for diacetyl exceeds 10.

6. The method according to claim 1 , wherein the adsorbent particles have an affinity constant for diacetyl that is at least 3 times higher than the particles' affinity constant for ethyl acetate.

7. The method according to claim 1 , wherein the affinity ratio θ i for acetaldehyde exceeds 5.

8. The method according to claim 7 , wherein the affinity ratio θ i for acetaldehyde exceeds 10.

9. The method according to claim 1 , wherein the affinity ratio θ i for dimethyl sulfide exceeds 5.

10. The method according to claim 9 , wherein the affinity ratio θ i for dimethyl sulfide exceeds 10.

11. The method according to claim 1 , wherein yeast is separated from the beer before the beer is contacted with the adsorbent particles.

12. The method according to claim 1 , wherein yeast and the adsorbent particles are simultaneously separated from the beer to produce the flavour adjusted beer.

13. The method according to claim 1 , wherein the adsorbent particles consist of polymer or the surface of the adsorbent particles consists of polymer.

14. The method according to claim 1 , wherein the adsorbent containing amine functionalities are selected from chitosan, Sevalamer™ (copolymer of 2-(chloromethyl)oxirane(epichlorohydrin) and prop-2-en-1-amine) and Siliabond™ amine functionalised silica gels.

15. The method according to claim 1 , wherein the adsorbent particles have specific surface area of at least 50 m 2 /g.

16. The method according to claim 1 , wherein at least 80 wt. % of the adsorbent particles has a diameter in the range of 5-5,000 μm.

Assignees

• Heineken Supply Chain Bv

Inventors

• Ottens Marcel
• Saffarionpour Shima
• Noordman Tom Reinoud

Classifications

• C12H1/0432

  with the aid of ion-exchange material · CPC title

• C12H1/0424

  with the aid of a polymer · CPC title

• C12C5/026

  Beer flavouring preparations · CPC title

• C12C11/11 Primary

  Post fermentation treatments, e.g. carbonation, or concentration (methods for reducing the alcohol content after fermentation C12H3/00; methods for increasing the alcohol content after fermentation C12H6/00) · CPC title

• C12H1/063

  Separation by filtration · CPC title