Tri-axial centrifuge apparatus with electrical sensor, acoustic sensor, and x-ray instrument

Patent metadata

Field	Value
Publication number	US-11241701-B2
Application number	US-201916674741-A
Country	US
Kind code	B2
Filing date	Nov 5, 2019
Priority date	Oct 21, 2013
Publication date	Feb 8, 2022
Grant date	Feb 8, 2022

Abstract

A tri-axial centrifuge apparatus for testing of petro-physical properties of a test sample includes a tri-axial sample holder located within an inner bore of a cell body. An axial pressure fluid supply line delivers an axial pressure fluid to apply an axial pressure on the test sample. A confining pressure fluid supply line delivers a confining pressure fluid to apply a biaxial confining pressure on the test sample. A test fluid holder contains test fluid and is static relative to the cell body. The axial pressure fluid, the confining pressure fluid, and the test fluid are contained in separate flow systems. A centrifuge has a window that is located on a portion of a path of the tri-axial sample holder. The tri-axial sample holder is loaded in the centrifuge and spinning with the centrifuge. An x-ray instrument is static and is aligned with the window of the centrifuge.

First claim

What is claimed is:

1. A tri-axial centrifuge apparatus for testing of petro-physical properties of a test sample and gathering of geo-mechanical information, the tri-axial centrifuge apparatus having:
a tri-axial sample holder located within an inner bore of a cell body;
an axial pressure fluid supply line operable to deliver an axial pressure fluid to a fluid chamber of a piston assembly to apply an axial pressure on the test sample;
a confining pressure fluid supply line operable to deliver a confining pressure fluid to a cell chamber of the cell body to apply a biaxial confining pressure on the test sample;
a test fluid holder containing test fluid, the test fluid holder being sealingly secured to the cell body and static relative to the cell body, where the axial pressure fluid, the confining pressure fluid, and the test fluid are contained in separate flow systems;
a test fluid circulation system having a test fluid line extending between the tri-axial sample holder and the test fluid holder and a fluid circulation line extending outside of the cell body between the test fluid holder and the tri-axial sample holder, the test fluid circulation system providing a fluid circulation path for the test fluid;
a centrifuge with a window that is located on a portion of a path of the tri-axial sample holder, where the tri-axial sample holder is loaded in the centrifuge and spinning with the centrifuge;
an x-ray instrument, where the x-ray instrument is static and is aligned with the window of the centrifuge, the x-ray instrument including an x-ray source positioned on a bottom side of the centrifuge and a x-ray camera installed on a lid of the centrifuge.

2. The tri-axial centrifuge apparatus of claim 1 , further including a titanium tri-axial test casing, and wherein the tri-axial sample holder is located in the tri-axial test casing.

3. The tri-axial centrifuge apparatus of claim 1 , wherein the test fluid holder includes glass.

4. The tri-axial centrifuge apparatus of claim 1 , wherein the centrifuge includes an at least one additional tri-axial sample holder.

5. The tri-axial centrifuge apparatus of claim 1 , wherein the window of the centrifuge includes at least two glass windows.

6. The tri-axial centrifuge apparatus of claim 1 , further including a tri-axial test casing, and wherein an at least one electrical sensor is secured to the tri-axial test casing and is operable to gather data during the testing of a sample and store data for downloading at a later time.

7. The tri-axial centrifuge apparatus of claim 1 , further including a tri-axial test casing, and wherein an at least one acoustic sensor is secured to the tri-axial test casing and includes a transducer.

8. The tri-axial centrifuge apparatus of claim 1 , wherein the x-ray instrument is operable to perform an x-ray scan while the centrifuge is operating.

9. The tri-axial centrifuge apparatus of claim 1 , further including a fluid camera system secured to the centrifuge.

10. The tri-axial centrifuge apparatus of claim 1 , wherein the test fluid holder has an electrical measurement feed.

11. The tri-axial centrifuge apparatus of claim 1 , where the tri-axial sample holder further includes an electrical measurement jacket, the electrical measurement jacket being a tubular member that surrounds the test sample.

12. The tri-axial centrifuge apparatus of claim 11 , further including a piston seal forming a seal between an inner bore of electrical measurement jacket and an outer diameter of a piston member of the assembly, and a base seal forming a seal between the inner bore of the electrical measurement jacket and a base member of the tri-axial sample holder, the piston seal and the base seal sealing the test fluid from the cell body outside of the electrical measurement jacket.

13. The tri-axial centrifuge apparatus of claim 1 , further including a tri-axial test casing, and wherein an at least one acoustic sensor is secured to and rotationally fixed relative to the tri-axial test casing.

14. The tri-axial centrifuge apparatus of claim 1 , where the piston assembly is an axially oriented piston assembly with a piston stem located entirely within the inner bore of the cell body.

15. The tri-axial centrifuge apparatus of claim 14 , where the axially oriented piston assembly is operable to apply the axial pressure on the test sample that is greater than the biaxial confining pressure applied on the test sample, and is operable to apply the axial pressure on the test sample independent of increasing the biaxial confining pressure on the test sample.

Assignees

• Saudi Arabian Oil Co

Inventors

• Hakimuddin Mustafa

Classifications

• B04B5/0414 Primary

  comprising test tubes · CPC title

• G01N27/02

  by investigating impedance · CPC title

• G01N2291/0226

  Oils, e.g. engine oils · CPC title

• G01N33/241 Primary

  for hydrocarbon content · CPC title

• B04B7/00

  Elements of centrifuges (drives B04B9/00; feeding, charging, or discharging appurtenances or devices B04B11/00) · CPC title