Component measurement of a fluid

Patent metadata

Field	Value
Publication number	US-11237149-B2
Application number	US-202016743170-A
Country	US
Kind code	B2
Filing date	Jan 15, 2020
Priority date	Jan 15, 2020
Publication date	Feb 1, 2022
Grant date	Feb 1, 2022

Abstract

An apparatus for measuring the oil and water fractions of a fluid, such as a drilling fluid. The apparatus includes a vessel body having an inner chamber coupled with a fluid inlet and an outlet. A heating element is coupled with the vessel body operable to communicate heat sufficient to vaporize a fluid within the vessel body to a gas. A gas analytical device is coupled with the outlet operable to measure components of the gas exiting the vessel body via the outlet. A rotary milling cutter translatable through the inner chamber and into solids remaining from the vaporized fluid, and having cutters operable to break solids within the inner chamber remaining from the vaporized fluid. The solids may be ejected through a solids discharge port.

First claim

What is claimed is:

1. An apparatus for measuring a fluid input comprising: a vessel body having an inner chamber coupled with a fluid inlet and an outlet; a heating element coupled with the vessel body operable to communicate heat sufficient to vaporize a fluid within the vessel body to a gas; a gas analytical device coupled with the outlet operable to measure components of the gas exiting the vessel body via the outlet; and a rotary milling cutter translatable through the inner chamber and into solids remaining from the vaporized fluid, and having cutters operable to break the solids within the inner chamber remaining from the vaporized fluid.

2. The apparatus of claim 1 , further comprising a solids discharge port through which the broken solids exit.

3. The apparatus of claim 1 , further comprising a pump for injecting the fluid into the fluid inlet.

4. The apparatus of claim 1 , wherein the gas analytical device uses one or more members selected from the group of gas chromatography, mass spectroscopy, spectroscopy, IR spectroscopy, UV-Fluorescence spectroscopy, and UV-VIS spectroscopy.

5. The apparatus of claim 1 , wherein the gas analytical device determines chemical components making up the gas.

6. The apparatus of claim 1 , wherein the fluid used is drilling fluid comprising at least oil and water.

7. The apparatus of claim 6 , wherein the gas analytical device determines the oil and water fraction of the gas.

8. A method comprising:
introducing a fluid into an inner chamber of a vessel body;
heating the fluid in the vessel body such that the fluid vaporizes to form a gas, whereby solids from the fluid are left within the inner chamber as a result of the vaporization;
flowing the gas out the body via an outlet;
measuring components of the gas exiting the vessel body with a gas analytical device;
milling the solids with a rotary milling cutter; and
discharging solids from the inner chamber.

9. The method of claim 8 , further comprising flushing the inner chamber with an inert gas.

10. The method of claim 8 , wherein measuring the components of the gas exiting the body with the gas analytical device comprises determining a hydrocarbon fraction and a water fraction of the gas.

11. The method of claim 8 , wherein the gas analytical device to measure components of the gas, uses one or more members selected from the group of gas chromatography, mass spectroscopy, spectroscopy, IR spectroscopy, UV-Fluorescence spectroscopy, and UV-VIS spectroscopy.

12. The method of claim 8 , wherein the solids are in the form of a solid puck, and wherein the milling comprises translating cutters within the inner chamber through the solid puck.

13. The method of claim 8 , wherein the rotary milling cutter contacts a sidewall of the inner chamber thereby removing solids from the sidewalls during milling.

14. The method of claim 8 , wherein the fluid is introduced into the vessel and the gas is measured in a continuous process.

15. The method of claim 14 , wherein the fluid introduced into the vessel is introduced at a rate of from about 1 to 10 ml/min.

16. The method of claim 8 , wherein the fluid is introduced into the vessel and the gas is measured in a batch process.

17. The method of claim 8 , wherein the fluid is drilling fluid from a wellbore.

18. A system for measuring a fluid input comprising: a vessel body having an inner chamber coupled with a fluid inlet and an outlet; a heating element coupled with the vessel body operable to communicate heat sufficient to vaporize a fluid within the vessel body to a gas; a gas analytical device coupled with the outlet operable to measure components of the gas exiting the vessel body via the outlet; and a rotary milling cutter translatable through the inner chamber and into solids remaining from the vaporized fluid, and having cutters operable to break the solids within the inner chamber remaining from the vaporized fluid.

19. The system of claim 18 , wherein measuring the components of the gas exiting the body with the gas analytical device comprises determining an oil fraction and a water fraction of the gas.

20. The system of claim 18 , wherein the fluid is a drilling fluid received from a wellbore.

Assignees

• Halliburton Energy Services Inc

Inventors

• Dotson Adam Robert
• Jackson Brice Aaron

Classifications

• G01N2001/105

  from high-pressure reactors or lines · CPC title

• G01N33/2823 Primary

  Raw oil, drilling fluid or polyphasic mixtures · CPC title

• G01N1/34

  Purifying; Cleaning {(processes or apparatus for extracting or separating nucleic acids from biological samples C12N15/1003)} · CPC title

• G01N21/64

  Fluorescence; Phosphorescence · CPC title

• G01N21/3504

  for analysing gases, e.g. multi-gas analysis · CPC title