Smoking article comprising a friction ignitable combustible carbonaceous heat source
US-2017318859-A1 · Nov 9, 2017 · US
US11234456B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-11234456-B2 |
| Application number | US-201917049027-A |
| Country | US |
| Kind code | B2 |
| Filing date | Sep 25, 2019 |
| Priority date | Aug 13, 2018 |
| Publication date | Feb 1, 2022 |
| Grant date | Feb 1, 2022 |
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A modified carbon material, including a carbonaceous material and a water-insoluble modifier combined with the carbonaceous material, wherein the water-insoluble modifier is CuO, the carbonaceous material is one of or a mixture of biomass carbon or carbon black, a mass of the water-insoluble modifier is being 0.1-10 wt % of the carbonaceous material. The method for preparing the modified carbon material includes: (1) soaking the carbonaceous material in a copper sulfate solution for 5 to 36 hours, and (2) adding an alkali solution into a solution obtained in step (1) to provide a pH value ≥12, and after keeping the pH value for 0.5 to 2 hours, filtering and drying to obtain a solid. (3) using the carbonaceous material as a combustion heat source to reduce the ignition temperature, increase or reduce the peak thermal power temperature.
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What is claimed is: 1. A method for preparing a modified carbon material comprising CuO wherein the method comprises the following steps: (1) obtaining a first solution by soaking a carbonaceous material in a copper sulfate solution for 5 to 36 hours, wherein a ratio of the carbonaceous material to the copper sulfate solution is controlled to control the CuO in the modified carbon material to be 1% by weight of the carbonaceous material; (2) adding an alkali solution into the first solution obtained in step (1) to provide a pH value ≥12, and after keeping the pH value for 0.5 to 2 hours, filtering and drying to obtain a solid, wherein the solid is the modified carbon material. 2. The method according to claim 1 , wherein the copper sulfate solution in step (1) has a concentration of from 0.5 to 3 wt %. 3. The method according to claim 1 , wherein the alkali solution in step (2) is a sodium hydroxide solution or a potassium hydroxide solution, with a concentration of from 1 to 50 wt %. 4. The method according to claim 1 , wherein a drying temperature in step (2) is in a range from 80 to 95° C. 5. The method according to claim 1 , wherein the carbonaceous material is carbon black.
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