Method for producing carbon nanostructure and apparatus for producing carbon nanostructure

Patent metadata

Field	Value
Publication number	US-11220432-B2
Application number	US-201716308141-A
Country	US
Kind code	B2
Filing date	Mar 14, 2017
Priority date	Jun 10, 2016
Publication date	Jan 11, 2022
Grant date	Jan 11, 2022

Abstract

A method for producing a carbon nanostructure according to an aspect of the present invention is a method in which a carbon nanostructure is produced between a base body and a separable body while the separable body is relatively moved away from the base body, the base body including a carburizable metal that is a principal constituent, the separable body including a carburizable metal that is a principal constituent, the separable body being joined to or in contact with the base body in a linear or strip-like shape. The method includes a carburizing gas feed step, an oxidizing gas feed step, a heating step in which the portion of the base body at which the base body and the separable body are joined to or in contact with each other is heated, and a separation step in which the separable body is relatively moved away from the base body.

First claim

The invention claimed is:

1. A method for producing a carbon nano structure in which a carbon nano structure is produced between a base body and a separable body while the separable body is relatively moved away from the base body, the base body including a carburizable metal that is a principal constituent, the separable body including a carburizable metal that is a principal constituent, the separable body being joined to or in contact with the base body in a linear or strip-like shape, the method comprising:
a carburizing gas feed step in which a carburizing gas is fed to at least a portion of the base body at which the base body and the separable body are joined to or in contact with each other;
an oxidizing gas feed step in which an oxidizing gas is fed to at least a part of a portion of the base body which is other than the portion of the base body to which the carburizing gas is fed in the carburizing gas feed step;
a heating step in which the portion of the base body at which the base body and the separable body are joined to or in contact with each other is heated;
a separation step in which the separable body is relatively moved away from the base body,
wherein the oxidizing gas feed step overlaps the carburizing gas feed step in the separation step, and
wherein a separator hermetically isolates the portion of the base body to which the carburizing gas is fed from the other portion of the base body to which the oxidizing gas is fed.

2. The method for producing a carbon nanostructure according to claim 1 , wherein the carburizing gas includes at least one selected from the group consisting of a hydrocarbon, carbon monoxide, and an alcohol.

3. The method for producing a carbon nanostructure according to claim 1 , wherein the oxidizing gas includes at least one selected from the group consisting of oxygen, water vapor, and carbon dioxide.

4. The method for producing a carbon nanostructure according to claim 1 , wherein the principal constituents of the base body and the separable body are selected from iron, nickel, cobalt, and an alloy of any of iron, nickel, and cobalt.

5. The method for producing a carbon nanostructure according to claim 1 , wherein the base body and the separable body are joined to each other in a linear or strip-like shape, and
wherein the separation performed in the separation step is to divide the separable body from the base body.

6. The method for producing a carbon nanostructure according to claim 5 , wherein the portion of the base body at which the base body and the separable body are joined to each other has a notch formed therein, the notch inducing division of the separable body from the base body.

7. The method for producing a carbon nanostructure according to claim 1 , the method further comprising a gap observation step in which a gap formed in the separation step is observed.

8. The method for producing a carbon nanostructure according to claim 1 , the method further comprising an oxidizing-gas feed portion observation step in which the portion of the base body to which the oxidizing gas is fed in the oxidizing gas feed step is observed.

Assignees

• Sumitomo Electric Industries

Inventors

• Hikata Takeshi
• Okubo Soichiro
• Nakai Ryusuke
• Tanioka Daisuke

Classifications

• B01J19/127

  Sunlight; Visible light · CPC title

• C01B32/16

  Preparation · CPC title

• B82Y40/00

  Manufacture or treatment of nanostructures · CPC title

• D01F9/127

  by thermal decomposition of hydrocarbon gases or vapours {or other carbon-containing compounds in the form of gas or vapour, e.g. carbon monoxide, alcohols} · CPC title

• C01B32/15 Primary

  Nano-sized carbon materials · CPC title