Iron nitride permanent magnet and technique for forming iron nitride permanent magnet

Patent metadata

Field	Value
Publication number	US-11217371-B2
Application number	US-202016876675-A
Country	US
Kind code	B2
Filing date	May 18, 2020
Priority date	Feb 7, 2013
Publication date	Jan 4, 2022
Grant date	Jan 4, 2022

Abstract

A bulk permanent magnetic material may include between about 5 volume percent and about 40 volume percent Fe16N2 phase domains, a plurality of nonmagnetic atoms or molecules forming domain wall pinning sites, and a balance soft magnetic material, wherein at least some of the soft magnetic material is magnetically coupled to the Fe16N2 phase domains via exchange spring coupling. In some examples, a bulk permanent magnetic material may be formed by implanting N+ ions in an iron workpiece using ion implantation to form an iron nitride workpiece, pre-annealing the iron nitride workpiece to attach the iron nitride workpiece to a substrate, and post-annealing the iron nitride workpiece to form Fe16N2 phase domains within the iron nitride workpiece.

First claim

The invention claimed is:

1. A bulk iron nitride magnet, comprising:
a plurality of textured iron nitride workpieces sintered together to form a bulk iron nitride magnet, the textured iron nitride workpieces characterized as having a volume fraction of between about 5 volume percent and about 40 volume percent of Fe 16 N 2 phase domains, the balance volume fraction comprising a soft magnetic phase, wherein at least some of the Fe 16 N 2 phase domains are magnetically coupled to at least one phase domain in the soft magnetic phase by exchange spring coupling, and
a nonmagnetic material, wherein
the nonmagnetic material is disposed between two or more of the sintered textured iron nitride workpieces, or
the nonmagnetic material is disposed within at least one of the textured iron nitride workpieces;

wherein the nonmagnetic material gives rise to domain wall pinning sites within the bulk magnet, wherein the soft magnetic phase comprises Fe 8 N phase domains.

2. The bulk iron nitride magnet of claim 1 , wherein the crystallographic texture of the Fe 16 N 2 phase domains and the soft magnetic phase are coherent.

3. The bulk iron nitride magnet of claim 1 , wherein the Fe 16 N 2 phase domains are magnetically coupled to at least one of the Fe 8 N phase domains in the soft magnetic phase.

Assignees

• Univ Minnesota

Inventors

• Wang Jian-Ping
• Jiang Yanfeng

Classifications

• H01F1/086 Primary

  sintered · CPC title

• C23C14/48

  Ion implantation · CPC title

• C22C29/16

  based on nitrides {(containing cubic BN or wurtzitic BN and diamond C22C26/00)} · CPC title

• C23C8/26

  of ferrous surfaces · CPC title

• B22F7/08

  with one or more parts not made from powder {(B22F7/062 takes precedence)} · CPC title