Method for discharging solids from a solids-laden gas

Patent metadata

Field	Value
Publication number	US-11208605-B2
Application number	US-201916451356-A
Country	US
Kind code	B2
Filing date	Jun 25, 2019
Priority date	Apr 10, 2017
Publication date	Dec 28, 2021
Grant date	Dec 28, 2021

Abstract

A solids discharge system (SDS) is configured to separate solids from product gas. The system includes a solids separation device and at least one solids transfer conduit configured to receive solids from the solids separation device. The solids transfer conduit is selectively partitioned into a plurality of compartments (or “sections”) along its length by isolation valves. A gas supply conduit and a gas discharge conduits are connected to one of the sections to facilitate removal of solids. A filter in fluid communication with that section is configured to prevent solids from passing through the gas discharge conduit so that the solids can be removed from one of the sections of the solids transfer conduit. A product gas generation system incorporates first and second reactors, the latter of which receives products created by the second reactor.

First claim

What is claimed is:

1. A method for discharging solids from a solids-laden gas, the method comprising:
(a) separating solids from the solids-laden gas with a solids separation device;
(b) transferring the separated solids to a solids transfer conduit;
(c) isolating the separated solids within an isolated section of the solids transfer conduit;
(d) depressurizing the isolated section at a depressurization rate of between 0.5 PSI per minute to 100 PSI per minute, by releasing gas within the isolated section through a filter with pore sizes or openings ranging from 0.1 microns to 100 microns, an area ranging from 5 square inches to 10,000 square inches, and at a face velocity ranging from 0.5 feet per minute to 50 feet per minute while retaining the separated solids within the solids transfer conduit;
(e) draining the separated solids from the solids transfer conduit; and
(f) after step (f), pressurizing at least a portion of the solids transfer conduit with a gas at a pressurization rate between 1 PSI per minute to 200 PSI per minute.

2. The method according to claim 1 , further comprising, in step (b), transferring said solids to a plurality of solids transfer conduits.

3. The method according to claim 1 , further comprising, after step (b) and before step (c) mixing the separated solids with carbon dioxide, within the solids transfer conduit.

4. The method according to claim 3 , further comprising, mixing carbon dioxide with solids at a carbon dioxide to solids weight ratio less than 0.05:1.

5. The method according to claim 1 , further comprising, in step (d) releasing gas from the isolated section for a duration of no more than 5 minutes and at a frequency no greater than once every 10 minutes and no less than once every 60 minutes.

6. The method according to claim 5 , further comprising, in step (d) releasing gas from the isolated section through a filter and then through a restriction orifice while retaining the separated solids within the isolated section.

7. The method according to claim 1 , further comprising, in step (d) releasing gas from the isolated section through a filter and then through a restriction orifice while retaining the separated solids within the solids transfer conduit.

8. The method according to claim 1 , further comprising, after step (e), reducing the temperature of the separated solids with a heat exchanger.

9. The method according to claim 1 , further comprising, in step (f) pressurizing said at least a portion of the solids transfer conduit with carbon dioxide for a duration of no more than 5 minutes and at a frequency no greater than once every 10 minutes and no less than once every 60 minutes.

10. The method according to claim 1 , further comprising:
in step (d) releasing gas for a duration of no more than 5 minutes and at a frequency no greater than once every 10 minutes and no less than once every 60 minutes; and
in step (f) pressurizing the solids transfer conduit with carbon dioxide for a duration of no more than 5 minutes and at a frequency no greater than once every 10 minutes and no less than once every 60 minutes.

11. The method according to claim 10 , further comprising, in step (d) releasing gas from the solids transfer conduit through a filter and then through a restriction orifice while retaining the separated solids within the solids transfer conduit.

12. The method according to claim 11 , further comprising, after step (e), reducing the temperature of the separated solids with a heat exchanger.

13. A method for producing a first reactor product gas and a second reactor product gas from a carbonaceous material using a first reactor having a first interior and a second reactor having a second interior, the method comprising:
reacting carbonaceous material with steam and optionally also with carbon dioxide and/or an oxygen-containing gas, in the first reactor to produce a first reactor product gas containing char;
separating char from the first reactor product gas;
reacting the separated char with an oxygen-containing gas in the second reactor to produce a second reactor product gas containing solids; and
removing solids from the second reactor product gas in accordance with the method of claim 1 .

Assignees

• Thermochem Recovery Int Inc

Inventors

• Chandran Ravi
• Newport Dave G
• Leo Daniel Michael
• Burciaga Daniel A
• Miller Justin Kevin
• Harrington Kaitlin Emily
• Attwood Brian Christopher
• SCHULTHEIS Emily Jane
• Kishton Kelly Ann

Classifications

• C10G2/34 Primary

  Apparatus, reactors · CPC title

• C01B3/32

  by reaction of gaseous or liquid organic compounds with gasifying agents, e.g. water, carbon dioxide or air · CPC title

• C10K1/026

  by centrifugal forces (cyclones B04C) · CPC title

• C01B2203/0283

  containing a CO-shift step, i.e. a water gas shift step · CPC title

• C01B2203/0216

  containing a non-catalytic steam reforming step · CPC title