Method of forming a ceramic matrix composite (CMC) component having an engineered surface

Patent metadata

Field	Value
Publication number	US-11198276-B2
Application number	US-201916277189-A
Country	US
Kind code	B2
Filing date	Feb 15, 2019
Priority date	Feb 16, 2018
Publication date	Dec 14, 2021
Grant date	Dec 14, 2021

Abstract

A method of forming a ceramic matrix composite (CMC) component having an engineered surface includes applying a surface slurry comprising first particulate solids in a liquid carrier to an outer surface of a ceramic fiber preform. The surface slurry is dried to remove the liquid carrier, and thus a surface slurry layer comprising the first particulate solids is formed on the outer surface. The surface slurry layer is polished to a predetermined thickness and/or surface finish. After polishing, a ceramic tape comprising second particulate solids is applied to the surface slurry layer, and pressure is applied to attach the ceramic tape to the surface slurry layer and to induce consolidation of the ceramic tape and the surface slurry layer. Thus, a multilayer surface region comprising the surface slurry layer and a ceramic tape layer is formed on the ceramic fiber preform. The ceramic fiber preform and the multilayer surface region are infiltrated with a molten material, and, upon cooling, a CMC component having an engineered surface is formed.

First claim

The invention claimed is:

1. A method of forming a ceramic matrix composite (CMC) component having an engineered surface, the method comprising:
applying a surface slurry to an outer surface of a ceramic fiber preform, the surface slurry including first particulate solids in a liquid carrier;
drying the surface slurry to remove the liquid carrier, thereby forming a surface slurry layer comprising the first particulate solids on the outer surface;
polishing the surface slurry layer to a predetermined thickness and/or surface finish;
after polishing, applying a ceramic tape to the surface slurry layer, the ceramic tape comprising second particulate solids,
applying pressure to the ceramic tape to attach the ceramic tape to the surface slurry layer and to induce consolidation of the ceramic tape and the surface slurry layer, thereby forming a multilayer surface region comprising the surface slurry layer and a ceramic tape layer on the ceramic fiber preform;
infiltrating the ceramic fiber preform and the multilayer surface region with a molten material, and forming, upon cooling, a CMC component having an engineered surface.

2. The method of claim 1 , wherein the surface slurry is applied by spraying, dipping, or brushing.

3. The method of claim 1 , wherein the surface slurry is dried at an elevated temperature from about 30° C. to about 100° C.

4. The method of claim 1 , wherein the predetermined surface finish corresponds to an average surface roughness R a of about 300 micro-in or less.

5. The method of claim 1 , wherein the predetermined thickness is in a range from about 25 microns to about 800 microns.

6. The method of claim 1 , further comprising, after polishing and prior to applying the ceramic tape, applying an organic binder to the surface slurry layer to promote initial attachment of the ceramic tape.

7. The method claim 1 , wherein the pressure applied to the ceramic tape is in a range from about 500 psi to about 50,000 psi.

8. The method of claim 1 , wherein the pressure is applied by lamination, autoclaving, vacuum bagging, or isostatic pressing.

9. The method of claim 1 , further comprising, as the pressure is applied, heating the ceramic tape at a temperature in a range from about 30° C. to about 200° C.

10. The method of claim 1 , further comprising applying a plurality of the ceramic tapes to the surface slurry layer.

11. The method of claim 1 , wherein the surface slurry further comprises one or more reactive additives selected from the group consisting of graphite, diamond, carbon black, silicon, molybdenum, and tungsten.

12. The method of claim 11 , wherein the ceramic tape further comprises the one or more reactive additives, and
wherein an amount of the one or more reactive additives in the surface slurry is higher than an amount of the one or more reactive additives in the ceramic tape.

13. The method of claim 1 , wherein the first particulate solids comprise a material selected from the group consisting of: Si, SiC, silicon oxycarbide, and Si 3 N 4 .

14. The method of claim 1 , wherein the second particulate solids comprise a material selected from the group consisting of: Si, silicon oxycarbide, Si 3 N 4 , SiC, Y 2 Si 2 O 7 , Yb 2 Si 2 O 7 , Y 2 SiO 5 , and Yb 2 SiO 5 .

15. The method of claim 1 , wherein the first particulate solids comprise the same material as the second particulate solids.

16. The method of claim 1 , wherein the first particulate solids comprise a different material from the second particulate solids.

17. The method of claim 1 , wherein the second particulate solids comprise two or more different materials, and
wherein a plurality of the ceramic tapes are applied to the surface slurry layer, the ceramic tapes comprising varying amounts of the two or more different materials.

18. The method of claim 17 , wherein the engineered surface comprises a graded composition that varies across a thickness thereof.

19. The method of claim 1 , wherein the engineered surface includes a silicon bond coat underlying an environmental barrier layer.

20. The method of claim 1 , wherein the engineered surface comprises a thickness in a range from about 10 microns to about 1 mm.

21. The method of claim 1 , further comprising, before applying the surface slurry to the outer surface, infiltrating the ceramic fiber preform with a ceramic slurry comprising particulate ceramic solids in a carrier liquid.

22. The method of claim 1 , wherein the ceramic fiber preform comprises SiC fibers, and wherein the molten material comprises a silicon melt or a silicon alloy melt.

23. A CMC component for gas turbine engine applications made by the method of claim 1 .

Assignees

• Rolls Royce High Temperature Composites Inc
• Rolls Royce Corp

Inventors

• Shim Sungbo
• Lai Benjamin

Classifications

• C04B2235/425

  Graphite · CPC title

• C04B2235/963

  Surface properties, e.g. surface roughness · CPC title

• C04B2235/48

  Organic compounds becoming part of a ceramic after heat treatment, e.g. carbonising phenol resins · CPC title

• C04B2235/3225

  Yttrium oxide or oxide-forming salts thereof · CPC title

• C04B2237/365

  Silicon carbide · CPC title