Mixing device for two component polyurethane foam formulation
US-2016175788-A1 · Jun 23, 2016 · US
US11192072B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-11192072-B2 |
| Application number | US-201616094182-A |
| Country | US |
| Kind code | B2 |
| Filing date | Sep 30, 2016 |
| Priority date | Sep 30, 2016 |
| Publication date | Dec 7, 2021 |
| Grant date | Dec 7, 2021 |
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Systems and methods related to preparing foamed cement for laboratory analysis are provided. A prepared cement slurry is placed in a cement reservoir cell configured to pressurize the cement slurry contained within the cement reservoir cell to a capture pressure. After pressurization, the cement slurry and a compressed gas are introduced into a foam generator. Foamed cement generated in the foam generator is introduced from the tee into a foam capture cell where it can cure prior to analysis.
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What is claimed is: 1. A method of preparing foamed cement in a laboratory environment for analysis comprising: preparing a cement slurry; introducing the cement slurry into a cement reservoir cell; pressurizing the cement reservoir cell to a pressure equal to or greater than a capture pressure selected to correspond to the conditions at a well site; introducing a gas into a foam generator through a first leg of the foam generator; displacing the cement slurry from the cement reservoir cell into the foam generator through a second leg of the foam generator such that the cement slurry and gas mix to form a foamed cement that flows into a third leg of the foam generator; and introducing the foamed cement from the third leg into a foam capture cell. 2. The method of claim 1 , wherein a backpressure of the foam capture cell is controlled by a backpressure regulator so as to control the introduction of foamed cement. 3. The method of claim 2 , wherein the cement reservoir cell has a cylinder and a piston, the cement slurry is introduced into the cylinder, and the step of displacing the cement slurry comprises running a pump to move the piston within the cylinder so as to displace the cement slurry from the cylinder. 4. The method of claim 3 , wherein the step of preparing a cement slurry comprises the steps of mixing an aqueous fluid and cement to form a base cement composition, and adding a surfactant to the base cement composition. 5. The method of claim 4 , wherein the gas is introduced into the foam generator through a choke. 6. The method of claim 5 , wherein the first leg and the second leg are perpendicular. 7. The method of claim 6 , wherein the first leg and the third leg are parallel and in-line. 8. The method of claim 1 , wherein the gas is selected from air, nitrogen and hydrogen. 9. The method of claim 8 , wherein the gas is nitrogen. 10. The method of claim 1 , wherein the step of preparing a cement slurry comprises the steps of mixing an aqueous fluid and cement to form a base cement composition, and adding a surfactant to the base cement composition. 11. A method of preparing foamed cement in a laboratory environment for analysis comprising: preparing a cement slurry; introducing the cement slurry into a cement reservoir cell; pressurizing the cement reservoir cell to a pressure equal to or greater than a capture pressure selected to correspond to the conditions at a well site; introducing a gas into a foam generator through a first leg of the foam generator; displacing the cement slurry from the cement reservoir cell into the foam generator through a second leg of the foam generator such that the cement slurry and gas mix to form a foamed cement that flows into a third leg of the foam generator; introducing the foamed cement from the third leg into a foam capture cell; and removing the foamed cement from the foam capture cell and analyzing the foamed cement. 12. The method of claim 11 , further comprising: selecting a quality and composition of foamed cement that is determined to be most suitable for use in a well based on the analysis of the foamed cement, and using the selected quality and composition of foamed cement in a downhole process for the well. 13. A method of preparing foamed cement in a laboratory environment for analysis comprising: preparing a cement slurry, wherein the step of preparing a cement slurry comprises the steps of mixing an aqueous fluid and cement to form a base cement composition, and adding a surfactant to the base cement composition; introducing the cement slurry into a cement reservoir cell; pressurizing the cement reservoir cell to a pressure equal to or greater than a capture pressure selected to correspond to the conditions at a well site; introducing a gas into a foam generator through a first leg of the foam generator; displacing the cement slurry from the cement reservoir cell into the foam generator through a second leg of the foam generator such that the cement slurry and gas mix to form a foamed cement that flows into a third leg of the foam generator; and introducing the foamed cement from the third leg into a foam capture cell, wherein a backpressure of the foam capture cell is controlled by a backpressure regulator so as to control the introduction of foamed cement. 14. The method of claim 13 , further comprising removing the foamed cement from the foam capture cell and analyzing the foamed cement, and wherein the cement reservoir cell has a cylinder and a piston, the cement slurry is introduced into the cylinder, and the step of displacing the cement slurry comprises running a pump to move the piston within the cylinder so as to displace the cement slurry from the cylinder. 15. The method of claim 14 , wherein the gas is introduced into the foam generator through a choke. 16. A method of preparing foamed cement in a laboratory environment for analysis comprising: preparing a cement slurry, wherein the step of preparing a cement slurry comprises the steps of mixing an aqueous fluid and cement to form a base cement composition, and adding a surfactant to the base cement composition; introducing the cement slurry into a cement reservoir cell; pressurizing the cement reservoir cell to a pressure equal to or greater than a capture pressure selected to correspond to the conditions at a well site; introducing a gas into a foam generator through a first leg of the foam generator, wherein the gas is introduced into the foam generator through a choke; displacing the cement slurry from the cement reservoir cell into the foam generator through a second leg of the foam generator such that the cement slurry and gas mix to form a foamed cement that flows into a third leg of the foam generator, wherein the cement reservoir cell has a cylinder and a piston, the cement slurry is introduced into the cylinder, and the step of displacing the cement slurry comprises running a pump to move the piston within the cylinder so as to displace the cement slurry from the cylinder; and introducing the foamed cement from the third leg into a foam capture cell, wherein a backpressure of the foam capture cell is controlled by a backpressure regulator so as to control the introduction of foamed cement; and wherein the gas is selected from air, nitrogen and hydrogen. 17. The method of claim 16 , wherein the first leg and the second leg are perpendicular. 18. The method of claim 17 , wherein the first leg and the third leg are parallel and in-line. 19. The method of claim 16 , further comprising removing the foamed cement from the foam capture cell and analyzing the foamed cement. 20. The method of claim 19 , further comprising: selecting a quality and composition of foamed cement that is determined to be most suitable for use in a well based on the analysis of the foamed cement, and using the selected quality and composition of foamed cement in a downhole process for the well.
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