Solid-liquid separating system and solid-liquid separating method

Patent metadata

Field	Value
Publication number	US-11185793-B2
Application number	US-201816607276-A
Country	US
Kind code	B2
Filing date	Apr 13, 2018
Priority date	Apr 26, 2017
Publication date	Nov 30, 2021
Grant date	Nov 30, 2021

Abstract

A solid-liquid separating method and system for separating a processing object into solid and liquid, is simplified by using fewer devices. A solid-liquid separating system includes a processing tank that houses a processing object, a first and a second heat exchanger, a material A supplying means, a collecting tank, a closed system including the first and second heat exchangers, a compressor, and an expansion valve, and a material B that circulates while a state is changed in this system. A material A that is gaseous at normal temperature and normal pressure, can dissolve oil when liquefied, and does not dissolve water is gasified in the first heat exchanger while being separated from the oil, is liquefied in the second heat exchanger, and the liquefied material A is supplied to the processing tank by the material A supplying means. The oil is collected in the tank from the first heat exchanger.

First claim

The invention claimed is:

1. A solid-liquid separating system in which, from a processing object containing water, oil, and solid, the oil is separated and collected from the processing object by use of a material A that is gaseous at normal temperature and normal pressure and when liquefied, can dissolve the oil and does not dissolve water, the solid-liquid separating system comprising:
a processing tank that houses the processing object;
a first heat exchanger that gasifies the material A contained in a mixture of the material A and the oil;
a second heat exchanger that liquefies the material A that has been gasified in the first heat exchanger;
a material A supplying means that supplies the material A that has been liquefied from the second heat exchanger to the first heat exchanger through the processing tank;
a collecting tank that is connected to the first heat exchanger via a second pipe and a valve;
a closed system configuration including the first heat exchanger, the second heat exchanger, a compressor, and an expansion valve; and
a material B that circulates in the closed system, such that the material B is in a liquefied state from the first heat exchanger to the expansion valve, is in a two-phase state from the expansion valve to the second heat exchanger and is in a gaseous state from the second heat exchanger to the first heat exchanger, wherein
the first heat exchanger condenses the material B which is compressed with the compressor and exchanges heat of condensation of the material B for heat of evaporation of the material A,
the expansion valve reduces pressure of the material B that has been condensed,
the second heat exchanger exchanges heat of evaporation of the material B for heat of condensation of the material A,
the material A that has been gasified while being separated from the oil in the first heat exchanger is liquefied in the second heat exchanger, and the material A that has been liquefied is supplied to the processing tank by the material A supplying means, and
by stopping the supply of the material A by the material A supplying means and continuing the circulation of the material B, the oil is collected from the first heat exchanger to the collecting tank.

2. The solid-liquid separating system according to claim 1 , wherein water solubility in the material A that has been liquefied is 1 g/L or less at 20° C.

3. The solid-liquid separating system according to claim 1 , wherein the material A has a boiling point of −100° C. or more and 10° C. or less.

4. The solid-liquid separating system according to claim 1 , wherein the material A has a saturated vapor pressure of 2 MPa or less at normal temperature.

5. The solid-liquid separating system according to claim 1 , wherein the material A contains at least one of propane, normal butane, isobutane, and neopentane as a main component.

6. The solid-liquid separating system according to claim 1 , wherein
the second heat exchanger, the processing tank, and the first heat exchanger are provided at positions that decrease in height in this order.

7. The solid-liquid separating system according to claim 1 , further comprising:
a pipe that connects between the first heat exchanger and the processing tank and supplies the material A that has been gasified in the first heat exchanger to the processing tank; and
an accumulator connected to the pipe between the processing tank and the first heat exchanger, wherein
the material A that has been liquefied in the processing tank is discharged and collected in the accumulator by the material A that has been gasified and supplied from the first heat exchanger to the processing tank through the pipe.

8. The solid-liquid separating system according to claim 7 , further comprising a second compressor connected to the pipe that connects between the first heat exchanger and the processing tank.

9. The solid-liquid separating system according to claim 1 , further comprising:
a heater connected to a pipe between the second heat exchanger and the processing tank; and
an accumulator connected to a pipe between the processing tank and the first heat exchanger, wherein
the material A that has been gasified by the heater in the pipe provided with the heater is supplied to the processing tank, and the material A that has been liquefied in the processing tank is discharged and collected in the accumulator.

10. The solid-liquid separating system according to claim 1 , further comprising:
a first accumulator connected to a pipe between the second heat exchanger and the processing tank;
a heater connected to the first accumulator; and
a second accumulator connected to a pipe between the processing tank and the first heat exchanger, wherein
the material A that has been liquefied is supplied from the second heat exchanger to the first accumulator, the material A that has been liquefied and housed in the first accumulator is gasified by the heater, the material A that has been gasified is supplied to the processing tank, and the material A that has been liquefied in the processing tank is discharged and collected in the second accumulator.

11. The solid-liquid separating system according to claim 1 , further comprising:
a heater connected to the processing tank; and
an accumulator connected to a pipe between the processing tank and the first heat exchanger, wherein
the material A that has been liquefied in the processing tank is gasified by the heater, the material A that has been gasified is supplied to the processing tank, and the material A that has been liquefied in the processing tank is discharged and collected in the accumulator.

12. A solid-liquid separating method in which, from a processing object containing water, oil, and solid, the oil is separated and collected from the processing object by use of a material A that is gaseous at normal temperature and normal pressure and when liquefied, can dissolve the oil and does not dissolve water, the method comprising:
a step of supplying the material A to the processing object in a liquid state so as to obtain a mixture in which the oil is dissolved in the material A;
a step of gasifying, via a first heat exchanger, the material A contained in the mixture by heating the mixture so as to separate the oil from the material A and collect the oil;
a step of cooling, via a second heat exchanger connected via a pipe to the first heat exchanger, the material A that has been gasified so as to liquefy the material A, and supplying the material A that has been liquefied to the processing object again; and
a step of stopping the supply of the material A and collecting, via a collecting tank that is connected to the first heat exchanger via a second pipe and a valve, the oil, wherein
the material A is gasified and liquefied while exchanging heat with a material B, the material B repeats a process of compression, condensation, expansion, and evaporation in a closed system.

13. A solid-liquid separating system in which, from a processing object containing liquid and solid, the liquid is separated and collected from the processing object by use of a material A that is gaseous at normal temperature and normal pressure and when liquefied, can dissolve the liquid, the solid-liquid separating system comprising:
a processing tank that houses the processing object;
a first heat exchanger that gasifies the material A contained in a mixture of the material A and the liquid;
a second heat exchanger that liquefies the material A that has been gasified in the first heat exchanger;
a material A supplying means that supplies the material A that has been liquefied from the second heat exchanger to the

Assignees

• Hitachi Ltd

Inventors

• Sano Tadashi
• Matsuzawa Mitsuhiro
• Sekiya Sachio

Classifications

• B01D11/028

  Flow sheets · CPC title

• B01D11/0492

  Applications, solvents used · CPC title

• B01D11/0288

  Applications, solvents · CPC title

• F25B1/00

  Compression machines, plants or systems with non-reversible cycle (F25B3/00, F25B5/00, F25B6/00, F25B7/00, F25B9/00 take precedence) · CPC title

• B01D11/0488 Primary

  Flow sheets · CPC title