Green liquor clarification using sedimentation tank during white liquor preparation

Patent metadata

Field	Value
Publication number	US-11174591-B2
Application number	US-201816764029-A
Country	US
Kind code	B2
Filing date	Sep 20, 2018
Priority date	Nov 17, 2017
Publication date	Nov 16, 2021
Grant date	Nov 16, 2021

Abstract

The invention relates to a method for clarification of raw green liquor in a sedimentation tank. According to the invention is a part of dregs separated in the sedimentation tank recirculated back into the inflow of raw green liquor, and preferably after passing the dregs through at least one turbulence generator (30, 31) that could break up larger dregs particles into smaller dregs particles, and thus create larger total surface on the dregs particles, improving sedimentation rate in the sedimentation tank. In a preferred embodiment is the recirculated dregs added into the flow of raw green liquor before a flocculant is added into the flow of raw green liquor and mixed recirculated dregs.

First claim

The invention claimed is:

1. A method for clarification of raw green liquor, comprising:
feeding the raw green liquor to a sedimentation tank through a mixing chamber with a multitude of lower outlets that provide for an even distribution of the raw green liquor at low flow velocity in a lower half of the sedimentation tank via a rotating distributor sweeping over a cross section of the sedimentation tank,
said sedimentation tank being equipped with an underflow outlet in a bottom of the sedimentation tank for settled dregs and an overflow outlet in an upper part of the sedimentation tank for clarified green liquor;
recirculating a part of the dregs fed out from the underflow outlet, back to infeed of raw green liquor;
causing the part of the dregs fed out from the underflow outlet, to pass through a first turbulence generator;
causing the part of the dregs having passed through the first turbulence generator, to pass through a second turbulence generator that is directly connected to the first turbulence generator via a pipe; and
feeding (1) the raw green liquor and (2) the part of the dregs having passed through the second turbulence generator, to the mixing chamber of the sedimentation tank,
wherein the first turbulence generator and the second turbulence generator are configured to break up some of the dregs into smaller fractions, such that a total exposed area of the dregs is increased.

2. A method for clarification of raw green liquor according to claim 1 , wherein at least one of the first turbulence generator or the second turbulence generator is a pump.

3. A method for clarification of raw green liquor according to claim 2 , wherein the part of the dregs fed out from the underflow outlet passes through at least one centrifugal pump with chopping action on a pumped flow of dregs.

4. A method for clarification of raw green liquor according to claim 1 , wherein the recirculated part of the dregs has a volume ratio versus a volume of raw green liquor in the range of 5-30%.

5. A method for clarification of raw green liquor according to claim 1 , wherein a flocculant is added to a flow of raw green liquor.

6. A method for clarification of raw green liquor according to claim 5 , wherein a flocculant is added to the flow of raw green liquor after having been subjected to a turbulence generator and before being fed to the mixing chamber of the sedimentation tank.

7. A method for clarification of raw green liquor according to claim 1 , wherein a flocculant is added to a flow of raw green liquor and recirculated dregs in the mixing chamber under the influence of a rotating turbine mixer.

8. A method for clarification of raw green liquor according to claim 7 , wherein a total amount of flocculant added to a gross flow of raw green liquor and recirculated part of dregs is in the range of 1-5 ppm.

9. A method for clarification of raw green liquor according to claim 8 , wherein the flocculant is a polymer which comprises polyamine or polyacrylamide.

10. A method for clarification of raw green liquor according to claim 1 , further comprising:
causing a mixture of (1) a flow of raw green liquor and (2) the part of the dregs having passed through the first turbulence generator, to pass through the second turbulence generator before being fed to the mixing chamber of the sedimentation tank.

Assignees

• Valmet Oy

Inventors

• Zhang Zicheng
• Johnson John
• Ingelman Magnus
• Guo sanchuan

Classifications

• B01D21/2416

  Liquid distributors with a plurality of feed points · CPC title

• B01D21/06

  with rotating scrapers · CPC title

• B01D21/04

  with moving scrapers · CPC title

• B01D21/2422

  Vertically arranged feed points · CPC title

• B01D21/2427

  The feed or discharge opening located at a distant position from the side walls · CPC title