Silica microcapsules and methods of preparing same

Patent metadata

Field	Value
Publication number	US-11160761-B2
Application number	US-201716086198-A
Country	US
Kind code	B2
Filing date	Mar 20, 2017
Priority date	Mar 18, 2016
Publication date	Nov 2, 2021
Grant date	Nov 2, 2021

Abstract

Disclosed is a microcapsule containing: (i) a microcapsule core having an active material, and (ii) a microcapsule wall formed of a first polymer and second polymer. The first polymer is a sol-gel polymer. The second polymer is gum arabic, purity gum ultra, gelatin, chitosan, xanthan gum, plant gum, carboxymethyl cellulose, sodium carboxymethyl guar gum, or a combination thereof. The weight ratio between the first and second polymer is 1:10 to 10:1. Also disclosed are processes for preparing the microcapsule and uses of the microcapsules in consumer products.

First claim

What is claimed is:

1. A microcapsule comprising: (i) a microcapsule core containing an active material, and (ii) a microcapsule wall formed of a first polymer and second polymer, wherein the first polymer is a sol-gel polymer, the second polymer is gum arabic, purity gum ultra, gelatin, chitosan, xanthan gum, plant gum, carboxymethyl cellulose, sodium carboxymethyl guar gum, or a combination thereof, and the weight ratio between the first and second polymer is 1:10 to 10:1, wherein the microcapsule wall is single-layered containing a polymeric network of polymerized silica interlocked with a coacervate of the second polymer wherein the sol-gel polymer is a silica polymer and the second polymer is a combination of gelatin and gum Arabic, and the weight ratio between gum Arabic and gelatin is 1:5 to 5:1.

2. The microcapsule of claim 1 furthering comprising a dispersant selected from the group consisting of quillaja saponin, N-lauroyl-L-arginine ethyl ester, sorbitan esters, lecithins, lyso-lecithins, polyethoxylated sorbitan esters, polyglyceryl esters, fatty acid esters, gum arabic, pectin, carrageenan, chitosan, chondroitin sulfate, cellulose gum, modified starch, whey protein, pea protein, egg white protein, silk protein, gelatin of fish, proteins of porcine or bovine origin, ester gum, fatty acids, and combinations thereof.

3. The microcapsule of claim 1 , wherein the active material is a fragrance, pro-fragrance, flavor, malodor counteractive agent, anti-inflammatory agent, anesthetic, analgesic, anti-viral agent, anti-infectious agent, anti-acne agent, skin lightening agent, insect repellant, emollient, skin moisturizing agent, vitamin or derivative thereof, nanometer to micron size inorganic solid, polymeric or elastomeric particle, taste modulator, probiotic, cell, or combination thereof.

4. The microcapsule of claim 1 , wherein the microcapsule has a particle size in diameter of 1 to 250 μm, and the weight ratio of between the microcapsule wall and the microcapsule core 1:50 to 2:1.

Assignees

• Int Flavors & Fragrances Inc

Inventors

• Brahms John
• Gabbard Ronald
• Geng Feng
• Wieland Julie Ann
• Xu Li
• Popplewell Lewis Michael

Classifications

• A23L27/00

  Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof · CPC title

• C08L5/00 Primary

  Compositions of polysaccharides or of their derivatives not provided for in groups C08L1/00 or C08L3/00 · CPC title

• A23F3/12

  Rolling or shredding tea leaves · CPC title

• A23F3/18

  Extraction of water soluble tea constituents ({A23F3/166 takes precedence; } isolation of tea flavour or tea oil A23F3/42) · CPC title

• A23F3/14

  Tea preparations, e.g. using additives (flavouring A23F3/40) · CPC title