Method for manufacturing thermoplastic polymer particles

Patent metadata

Field	Value
Publication number	US-11149120-B2
Application number	US-201816491859-A
Country	US
Kind code	B2
Filing date	Mar 9, 2018
Priority date	Mar 9, 2017
Publication date	Oct 19, 2021
Grant date	Oct 19, 2021

Abstract

Provided is a method for manufacturing thermoplastic polymer particles, the method comprising the steps of: supplying a thermoplastic polymer resin to an extruder and extruding the same; supplying the extruded thermoplastic polymer resin and air to a nozzle, bringing the thermoplastic polymer resin into contact with the air to granulate the thermoplastic polymer resin, and then discharging the granulated thermoplastic polymer resin; and supplying discharged thermoplastic polymer particles to a cooling unit to cool the thermoplastic polymer particles, and then collecting the cooled thermoplastic polymer particles.

First claim

The invention claimed is:

1. A method for manufacturing thermoplastic polymer particles comprising:
(1) supplying a thermoplastic polymer resin to an extruder and extruding it;
(2) supplying the extruded thermoplastic polymer resin and air to a nozzle, bringing the thermoplastic polymer resin into contact with air to granulate the thermoplastic polymer resin, and then discharging the granulated thermoplastic polymer resins; and
(3) supplying the discharged thermoplastic polymer particles to a cooling unit to cool the thermoplastic polymer particles, and then collecting the cooled thermoplastic polymer particles;
wherein in step (2), based on a cross section of the nozzle, the air is supplied to a central portion and an outer portion, and the extruded thermoplastic polymer resin is supplied between the central portion and the outer portion to which the air is supplied, and
based on the cross section at the outlet of the nozzle, the ratio of the cross-sectional areas of the air supplied to the outer portion and the extruded thermoplastic polymer resin supplied between the central portion and the outer portion to which the air is supplied is 2:1 to 6:1,
in step (3), the cooling unit is located away from the outlet of the nozzle so that the discharged thermoplastic polymer particles are primarily cooled by ambient air before being introduced into the cooling unit, and
the cooling unit cools the thermoplastic polymer particles by air which has temperature of −30 to −20° C. and forms a rotary airflow.

2. The method for manufacturing thermoplastic polymer particles according to claim 1 , wherein in step (1), an inside of the extruder is maintained at 150 to 450° C.

3. The method for manufacturing thermoplastic polymer particles according to claim 1 , wherein in step (2), the extruded thermoplastic polymer resin supplied to the nozzle has a melt viscosity of 0.5 to 20 Pa·s.

4. The method for manufacturing thermoplastic polymer particles according to claim 1 , wherein in step (2), the extruded thermoplastic polymer resin is supplied to the nozzle at a flow rate of 1 to 10 kg/hr, the air is supplied to the nozzle at a flow rate of 1 to 300 m 3 /hr.

5. The method for manufacturing thermoplastic polymer particles according to claim 1 , wherein in step (2), the air is supplied to the nozzle at a temperature of 250 to 600° C.

6. The method for manufacturing thermoplastic polymer particles according to claim 1 , wherein in step (2), an inside of the nozzle is maintained at 250 to 450° C.

7. The method for manufacturing thermoplastic polymer particles according to claim 6 , wherein in step (2), a distal end of the nozzle is maintained at a temperature calculated by Formula below:
Distal end temperature=glass transition temperature ( T g )+(pyrolysis temperature ( T d )−glass transition temperature ( T g ))× A,   [Formula]

wherein the glass transition temperature and the pyrolysis temperature are values for thermoplastic polymer, and
A is 0.5 to 1.5.

8. The method for manufacturing thermoplastic polymer particles according to claim 1 , wherein in step (2), a discharging angle of the thermoplastic polymer resin from the nozzle is 10 to 60°.

Assignees

• Lg Hausys Ltd

Inventors

• Lee Hee-Jung
• Kang Sung Yong
• Kang Kyoung Min
• Kim Min Gyung
• Park Chang-Young
• Lim Jae Ho
• Choi Jun Ho
• Song Jae Han
• Go Yu Jin

Classifications

• C08G63/08

  Lactones or lactides · CPC title

• C08L23/12

  Polypropene · CPC title

• B29B9/10

  by moulding the material, i.e. treating it in the molten state · CPC title

• C08G63/06

  derived from hydroxycarboxylic acids · CPC title

• C08L2203/30

  used for thermoforming · CPC title