Active cooling of cold-spray nozzles

Patent metadata

Field	Value
Publication number	US-11148153-B2
Application number	US-201916389668-A
Country	US
Kind code	B2
Filing date	Apr 19, 2019
Priority date	Apr 20, 2018
Publication date	Oct 19, 2021
Grant date	Oct 19, 2021

Abstract

Various embodiments disclosed relate to a method of cold-spray deposition involving cooling the cold-spray nozzle by at least one of expanding and vaporizing a compressed cooling fluid in proximity to the cold-spray nozzle. The present disclosure also includes a cold-spray deposition spray head, a cooling jacket for a cold-spray deposition nozzle and a cold-spray deposition system comprising the same.

First claim

What is claimed is:

1. A method of cold-spray deposition comprising:
mixing a powder with a heated and pressurized process gas to produce a powder-gas mixture;
flowing the powder-gas mixture through a nozzle to produce an accelerated powder-gas mixture;
spraying the accelerated powder-gas mixture onto a substrate to deposit the powder; and
cooling the nozzle by at least one of expanding and vaporizing a compressed cooling fluid in proximity to the nozzle such that the compressed cooling fluid undergoes a phase change;
wherein the compressed cooling fluid has a liquid-vapor critical point between a pressure of 25-150 bar and between a temperature of 250-350 K.

2. The method of claim 1 , comprising flowing the compressed cooling fluid through a spray head comprising the nozzle and a cooling jacket which surrounds at least a portion of the nozzle.

3. The method of claim 2 , wherein the compressed cooling fluid is flowed through the spray head without mixing with any of the heated and pressurized process gas, the powder-gas mixture and the accelerated powder-gas mixture.

4. The method of claim 2 , comprising at least one of expanding and vaporizing the compressed cooling fluid in the spray head.

5. The method of claim 2 , comprising at least one of expanding and vaporizing the compressed cooling fluid in an outer channel between an inner wall of the cooling jacket and an outer wall of the nozzle.

6. The method of claim 2 , wherein the cooling jacket comprises:
a rigid body;
a nozzle channel extending through the rigid body from a nozzle entry port to a nozzle exit port;
an outer channel oriented coaxially to the nozzle channel and extending at least a portion of the length of the nozzle channel;
one or more cooling fluid inlets for providing a compressed cooling fluid to the outer channel; and
one or more cooling fluid outlets which communicate the outer channel to an area of ambient pressure;
wherein the cooling jacket is configured to secure placement of the nozzle through the nozzle channel and the compressed cooling fluid has a liquid-vapor critical point between a pressure of 25-150 bar and a temperature of 250-350 K.

7. The method of claim 1 , wherein the compressed cooling fluid is provided continuously.

8. The method of claim 1 , wherein the process gas is at a temperature of from about 100° C. to about 1000° C. and a pressure of from about 10 Bar to about 50 Bar.

9. The method of claim 1 , wherein the accelerated powder-gas mixture has a velocity of 300 to 1200 m/s.

10. The method of claim 1 , wherein the powder comprises metal particles.

11. The method of claim 1 , wherein the powder is at least 99% nickel.

12. The method of claim 1 , comprising performing the spraying for at least 6 minutes at 600° C. with the nozzle remaining clog-free.

13. The method of claim 1 , comprising performing the spraying for at least 10 minutes at a temperature of about 350° C. to about 600° C. with the nozzle remaining clog-free.

14. The method of claim 1 , comprising performing the spraying for at least 20 minutes at a temperature of about 350° C. to about 600° C. with the nozzle remaining clog-free.

15. The method of claim 1 , comprising flowing the compressed cooling fluid at a rate of at least 100 mL/min through a cooling jacket which surrounds at least a portion of the nozzle.

16. The method of claim 1 , comprising flowing the compressed cooling fluid through a spray head, wherein the spray head comprises:
the nozzle, wherein the nozzle is a cold-spray nozzle;
a cooling jacket coaxially oriented around the cold-spray nozzle to provide an annular outer channel between an inner wall of the cooling jacket and an outer wall of the cold-spray nozzle;
one or more cooling fluid inlets in communication with the outer channel; and
one or more cooling fluid outlets which communicate the outer channel to an area of ambient pressure;
wherein the cooling fluid inlets provide a flow pathway for a compressed cooling fluid to flow to the outer channel and cool the outer wall of the cold-spray nozzle by at least one of expanding and vaporizing in the outer channel.

17. The method of claim 16 , wherein the spray head comprises one or more cooling fluid pumps which compress cooling fluid from a cooling fluid source and provide compressed cooling fluid to the one or more cooling fluid inlets.

18. The method of claim 16 , wherein the spray head comprises two or more cooling fluid pumps linked to continuously compress cooling fluid from the cooling fluid source and continuously provide compressed cooling fluid to the one or more cooling fluid inlets.

19. The method of claim 18 , wherein the two or more cooling fluid pumps provide cooling fluid at a rate of at least 100 mL/min.

20. The method of claim 1 , wherein the compressed cooling fluid comprises carbon dioxide.

Assignees

• Watkins James J
• Schmidt David
• Rodriguez Jacobo Morere
• Champagne Victor K
• Univ Massachusetts
• Us Army

Inventors

• Watkins James J
• Schmidt David
• Rodriguez Jacobo Morere
• Champagne Victor K

Classifications

• B05B7/1486

  for spraying particulate material in dry state · CPC title

• C23C24/04 Primary

  Impact or kinetic deposition of particles · CPC title

• B05B7/1686

  involving vaporisation of the material to be sprayed or of an atomising-fluid-generating product · CPC title

• B05B7/168

  with means for heating or cooling after mixing (B05B7/201, B05B7/22 take precedence) · CPC title

• B05B7/1404 Primary

  Arrangements for supplying particulate material · CPC title