Systems and methods of nanofiltration using graphene oxide

Patent metadata

Field	Value
Publication number	US-11148070-B2
Application number	US-201815914993-A
Country	US
Kind code	B2
Filing date	Mar 7, 2018
Priority date	Mar 7, 2018
Publication date	Oct 19, 2021
Grant date	Oct 19, 2021

Abstract

Nanofiltration of aqueous solutions or other water-based fluids in various applications, such as desalination, dialysis, seawater purification, for example, may be enhanced through precisely controlling a filtration cutoff within graphene oxide nanofilters. By initially compressing and constraining the stacked thickness of multiple graphene oxide layers deposited between porous substrates, the interlayer gap size, and thus, the filtration cutoff may be adjusted and optimized.

First claim

What is claimed is:

1. A nanofilter comprising:
a first porous support plate;
a second porous support plate;
graphene oxide layers deposited between the first and the second porous support plates, wherein the graphene oxide layers have pore sizes different than pore sizes in the first and second support plates;
an adjusting control to allow adjustment and to set at least one of pressure and distance between the first and second porous plates to compress and constrain the graphene oxide layers at a set position, the at least one of the pressure and the distance set based upon a desired filtration cutoff; and
a programmable controller connected to the adjusting control, the controller configured to provide the adjustment to the adjusting control based upon programmed filtration cutoff states mapped to a separate distance set by the adjusting control.

2. The nanofilter of claim 1 , further comprising:
a seal arranged between the first and second porous plates and surrounding the graphene oxide layers.

3. The nanofilter of claim 1 , further comprising:
a first porous substrate filter between the graphene oxide layers and the first porous plate; and
a second porous substrate filter between the graphene oxide and the second porous plate.

4. The nanofilter of claim 1 , further comprising:
a support frame;
a first flow channel arranged upstream of the first porous plate; and
a second flow channel arranged downstream of the second porous plate.

5. The nanofilter of claim 1 , wherein the adjusting control is remotely operable.

6. The nanofilter of claim 1 , wherein the distance between the first and second porous plates is mapped against an interlayer gap size of the graphene oxide layers.

7. A nanofiltration system comprising:
a filter including:
a first porous support plate;
a second porous support plate;
graphene oxide layers deposited between the first and the second porous support plates, wherein the graphene oxide layers have pore sizes different than the first and second support plates; and
an adjusting control to allow adjustment and to set at least one of pressure and distance between the first and second porous plates to compress and constrain the graphene oxide layers, the at least one of the pressure and the distance based upon a desired filtration cutoff;
a programmable controller connected to the adjusting control, the controller configured to provide the adjustment to the adjusting control based upon programmed filtration cutoff states mapped to a separate distance set by the adjusting control; and
a flow channel arranged tangentially to the filter.

8. The nanofiltration system of claim 7 , wherein the adjusting control includes a fine pitch screw.

9. The nanofiltration system of claim 7 , wherein the adjusting control includes an inch worm piezo element.

10. The nanofiltration system of claim 7 , wherein the adjusting control includes a spring mount.

11. The nanofiltration system of claim 7 , wherein the adjusting control includes a pneumatic element.

12. The nanofiltration system of claim 7 , further comprising:
a second filter; and
a second flow channel arranged tangentially to the second filter.

Assignees

• Palo Alto Res Ct Inc

Inventors

• Biegelsen David K
• Volkel Armin R

Classifications

• B01D69/10

  Supported membranes; Membrane supports · CPC title

• B01D63/087

  Single membrane modules · CPC title

• B01D65/003

  Membrane bonding or sealing · CPC title

• B01D61/027

  Nanofiltration · CPC title

• B01D33/801

  Driving means, shaft packing systems or the like · CPC title