Catalyst composition for alkaline electrochemical energy conversion reaction and use thereof
US-2017187046-A1 · Jun 29, 2017 · US
US11142836B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-11142836-B2 |
| Application number | US-201816204905-A |
| Country | US |
| Kind code | B2 |
| Filing date | Nov 29, 2018 |
| Priority date | Nov 29, 2018 |
| Publication date | Oct 12, 2021 |
| Grant date | Oct 12, 2021 |
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A method for manufacturing catalyst material is provided, which includes putting an M′ target and an M″ target into a nitrogen-containing atmosphere, in which M′ is Ni, Co, Fe, Mn, Cr, V, Ti, Cu, or Zn, and M″ is Nb, Ta, or a combination thereof. Powers are provided to the M′ target and the M″ target, respectively. Providing ions to bombard the M′ target and the M″ target to sputtering deposit M′ a M″ b N 2 on a substrate, wherein 0.7≤a≤1.7, 0.3≤b≤1.3, and a+b=2, wherein M′ a M″ b N 2 is a cubic crystal system.
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What is claimed is: 1. A catalyst material, having a chemical structure of: M′ a M″ b N 2 , wherein M′ is Ni, Co, Fe, Mn, Cu, or Zn; M″ is Nb, Ta, or a combination thereof; 0.7≤a≤1.7, 0.3≤b≤1.3, and a+b=2, wherein the catalyst material is a cubic crystal system. 2. The catalyst material as claimed in claim 1 , wherein M′ is Ni, M″ is Nb, 0.7≤a≤1.51, and 0.49≤b≤1.30. 3. A method for manufacturing the catalyst material as claimed in claim 1 , comprising: putting an M′ target and an M″ target into a nitrogen-containing atmosphere, wherein M′ is Ni, Co, Fe, Mn, Cu, or Zn, and M″ is Nb, Ta, or a combination thereof; providing power to the M′ target and the M″ target, respectively; and providing ions to bombard the M′ target and the M″ target, to sputtering deposition of M′ a M″ b N 2 on a substrate, wherein 0.7≤a≤1.7, 0.3≤b≤1.3, and a+b=2, wherein M′ a M″ b N 2 is a cubic crystal system. 4. The method as claimed in claim 3 , wherein the power provided to the M′ target is 10 W to 200 W, and the power provided to the M″ target is 10 W to 200 W. 5. The method as claimed in claim 3 , wherein the nitrogen-containing atmosphere has a pressure of 1 mTorr to 30 mTorr. 6. The method as claimed in claim 3 , wherein the nitrogen-containing atmosphere comprises carrier gas, and the nitrogen and the carrier gas have a partial pressure ratio of 0.1 to 10. 7. The method as claimed in claim 3 , wherein the substrate comprises a porous conductive layer.
using more than one target (C23C14/56 takes precedence) · CPC title
consisting of a single catalytic element or catalytic compound · CPC title
with iron, cobalt or nickel · CPC title
with two or more other elements chosen from metals, silicon or boron · CPC title
Carbides · CPC title
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