Laboratory measurement of dynamic fracture porosity and permeability variations in rock core plug samples

Patent metadata

Field	Value
Publication number	US-11125671-B2
Application number	US-201916506689-A
Country	US
Kind code	B2
Filing date	Jul 9, 2019
Priority date	Jul 9, 2019
Publication date	Sep 21, 2021
Grant date	Sep 21, 2021

Abstract

Fracture porosity and permeability variations with increasing effective stress, are measured and determined by laboratory testing of rock cylindrical core plugs of various types (carbonate, silico-clastic, shale, e.g.) and dimensions. The testing can be implemented for both natural and induced fractures propagating axially in the rock core plug. The testing begins with initial testing, sample preparation and obtaining measurements on an intact plug to define matrix properties in the rock core plug. A rock core plug with defined matrix properties is then after further preparation, subjected to an axial shear fracture (natural or induced) propagating through its body. Measurements are then obtained from the plug with an axial shear fracture (natural or induced) propagating through its body to determine fracture properties.

First claim

What is claimed is:

1. A method of laboratory measurement of dynamic variations in petrophysical properties of a subsurface formation as a result of changes in stress applied to a core plug rock sample obtained from a location of interest in the subsurface formation, comprising the steps of:
(a) performing computerized tomography on the core plug rock sample to determine a homogeneous density distribution in the core plug rock sample;
(b) determining, responsive to determining the homogeneous density distribution in the rock sample and based on application of different levels of stress within a stress interval to the core plug rock sample, a matrix porosity/stress relationship for the core plug rock sample and a matrix permeability/stress relationship for the core plug rock sample, the matrix porosity/stress relationship corresponding to measured changes in porosity of the core rock plug sample for the different levels of stress applied to the core rock plug, and the matrix permeability/stress relationship corresponding to measured changes in permeability of the core rock plug sample for the different levels of stress applied to the core rock plug;
(c) forming an axially extending shear fracture through the core plug rock sample to form a split core plug composed of fracture halves of the core plug rock sample;
(d) moving the fracture halves of the split core plug axially with respect to each other to generate a moved split core plug that simulates displacement during in-situ fracture of formation rock of the subsurface formation;
(e) joining the fracture halves of the moved split core plug together to form a joined split plug comprising the fracture halves of the split core plug joined together and displaced axially with respect to each other; and
(f) determining, based on application of different levels of stress within the stress interval to the joined split plug, a fracture porosity/stress relationship for the core plug rock sample and a fracture permeability/stress relationship of the core plug rock sample, the fracture porosity/stress relationship corresponding to measured changes in porosity of the joined split plug for the different levels of stress applied to the joined split plug, and the fracture permeability/stress relationship corresponding to measured changes in permeability of the joined split plug for the different levels of stress applied to the joined split plug.

2. The method of claim 1 , wherein determining the matrix porosity/stress relationship for the core plug rock sample and the matrix permeability/stress relationship for the core plug rock sample comprises:
performing a pore volume compressibility test of the core plug rock sample to determine the matrix porosity/stress relationship for the core plug rock sample; and
performing a stress-dependent permeability test of the core plug rock sample to determine the matrix permeability/stress relationship for the core plug rock sample.

3. The method of claim 2 , further including the step of:
obtaining measurements of physical properties of the core plug rock sample before performing the pore compressibility test.

4. The method of claim 2 , wherein the pore volume compressibility test is performed with the core rock sample under triaxial stress conditions.

5. The method of claim 2 , wherein the pore volume compressibility test is performed with the core rock sample under hydrostatic stress conditions.

6. The method of claim 2 , further including the step of:
obtaining measurements of physical properties of the core plug rock sample before performing the pore volume compressibility test.

7. The method of claim 1 , wherein determining the fracture porosity/stress relationship for the core plug rock sample and the fracture permeability/stress relationship of the core plug rock sample comprises:
performing a pore volume compressibility test of the joined split plug to determine the fracture porosity/stress relationship for the core plug rock sample;
performing a stress-dependent permeability test of the joined split plug to determine the fracture permeability/stress relationship of the core plug rock sample.

8. The method of claim 7 , wherein the pore volume compressibility test is performed under triaxial stress conditions.

9. The method of claim 7 , wherein the pore volume compressibility test is performed under hydrostatic stress conditions.

Assignees

• Saudi Arabian Oil Co

Inventors

• Santagati Antonio A
• Camargo Otto E Meza
• Mahmood Tariq
• Caliboso Edwin

Classifications

• G01N15/088 Primary

  Investigating volume, surface area, size or distribution of pores; Porosimetry · CPC title

• G01N15/082 Primary

  Investigating permeability by forcing a fluid through a sample · CPC title

• G01N2223/616

  earth materials · CPC title

• G01N33/241

  for hydrocarbon content · CPC title

• G01N15/0826 Primary

  and measuring fluid flow rate, i.e. permeation rate or pressure change · CPC title