Process for preparing a homogeneous solution of a polymer and melanin

Patent metadata

Field	Value
Publication number	US-11109589-B2
Application number	US-201716307617-A
Country	US
Kind code	B2
Filing date	Jun 8, 2017
Priority date	Jun 9, 2016
Publication date	Sep 7, 2021
Grant date	Sep 7, 2021

Abstract

The present invention discloses a process for preparing a homogeneous solution of a polymer and melanin. The present invention further discloses a process for preparation of fibers and films from said homogeneous solution.

First claim

We claim:

1. A process for preparing a solution of a polymer and melanin comprising the steps of:
a. dissolving a polymer in tetrabutylammonium hydroxide (TBAH) solution under continuous vortex mixing for a time period ranging from 1 to 2 hr to obtain a solution;
b. dissolving melanin in tetrabutylammonium hydroxide (TBAH) solution under continuous vortex mixing for a time period ranging from 1 to 2 hr followed by mixing with the solution of step (a) to obtain a mixed solution,
wherein the relative amounts of the polymer and the melanin in the mixed solution are in the range of 95 to 99 weight % and in the range of 1 to 5 weight %, respectively.

2. The process as claimed in claim 1 , wherein said mixed solution is used to obtain composite films, fibers, coatings and shaped forms.

3. The process as claimed in claim 2 , wherein said fibers are prepared by a process comprising extruding said mixed solution at a flow rate of 0.01 ml/min in a water bath and rolling on to a spool followed by drying the fibers at a temperature ranging from 30° C. to 40° C. for a time period ranging from 4 to 6 h under air convection to obtain said fibers.

4. The process as claimed in claim 1 , wherein the melanin is selected from natural or synthetic source and said polymer is selected from the group consisting of cellulose, silk, other natural polysaccharides, and proteins.

5. The process as claimed in claim 1 , wherein the melanin has a concentration of in the range of 0.1 to 1 weight % in the TBAH solution of the step (b) and the polymer has a concentration in the range of 1 to 10 weight % in the TBAH solution of the step (a).

6. The process as claimed in claim 1 , wherein said mixed solution shows antibacterial activity against gram positive and gram negative bacteria.

7. The process as claimed in claim 1 , wherein said mixed solution is used in removal of dyes from effluents.

Assignees

• Council Scient Ind Res

Inventors

• Shanmuganathan Kadhiravan
• Pimpalkar Nikhil Kamlakar
• Shete Abhijit Pravin
• Ram Farsa

Classifications

• A61Q17/04

  Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations · CPC title

• A61K8/72

  containing organic macromolecular compounds · CPC title

• D01D10/06

  Washing or drying · CPC title

• A01N43/90

  having two or more relevant hetero rings, condensed among themselves or with a common carbocyclic ring system · CPC title

• A61K8/96

  containing materials, or derivatives thereof of undetermined constitution · CPC title