Liquid delivery device and fluid chromatograph

Patent metadata

Field	Value
Publication number	US-11098702-B2
Application number	US-201716496740-A
Country	US
Kind code	B2
Filing date	Apr 26, 2017
Priority date	Apr 26, 2017
Publication date	Aug 24, 2021
Grant date	Aug 24, 2021

Abstract

A liquid delivery device includes a pump head having a pump chamber provided in the inside, a plunger whose tip is slidably inserted into the pump chamber, and at least one plunger pump having a drive mechanism that reciprocates the plunger in its axial direction. Then, at least one of the plunger pumps is a pressurizing pump that pressurizes a mobile phase including a compressible fluid sucked into the pump chamber and then discharges the mobile phase from the pump chamber, and at least the pump head of the pressurizing pump includes a cooling part that is connected to an outlet channel from the pump chamber, and allows the pump head to absorb heat of the mobile phase discharged from the pump chamber to cool the mobile phase.

First claim

The invention claimed is:

1. A liquid delivery device comprising:
at least one or more plunger pumps, wherein the at least one or more plunger pumps each include a pump head having a pump chamber provided in an inside, a plunger having a tip which is slidably inserted into the pump chamber, and a drive mechanism that reciprocates the plunger in an axial direction thereof,
at least one of the at least one or more plunger pumps is a pressurizing pump that pressurizes a mobile phase including a compressible fluid sucked into the pump chamber and then discharges the mobile phase from the pump chamber, and
at least the pump head of the pressurizing pump includes a cooling part formed by at least one channel connected with an outlet channel of the pump chamber, the cooling part is configured to cause the pump head to absorb heat of a mobile phase that is discharged from the pump chamber and flows into the at least one channel, and is provided to cool the mobile phase.

2. The liquid delivery device according to claim 1 , wherein the at least one channel forming the cooling part is a flat plate-shaped channel in which a ratio of an internal surface area to internal capacity is larger than that of the outlet channel.

3. The liquid delivery device according to claim 1 , wherein the at least one channel forming the cooling part is a plurality of channels having a smaller cross-sectional area than the outlet channel.

4. The liquid delivery device according to claim 1 , wherein the at least one channel forming the cooling part is a plurality of channels having a smaller cross-sectional area than the outlet channel and meander.

5. The liquid delivery device according to claim 2 ,
wherein one wall surface of the at least one channel forming the cooling part is configured to generate an elastic strain in accordance with pressure in the at least one channel,
the liquid delivery device further comprising:
a strain detection part that detects an amount of strain of the wall surface; and
a pressure detection part that detects pressure in the cooling part based on an amount of strain of the wall surface detected by the strain detection part.

6. The liquid delivery device according to claim 1 , further comprising a temperature detection part that detects a temperature of the cooling part.

7. The liquid delivery device according to claim 5 , further comprising a calorific value calculation part that calculates a calorific value of a mobile phase in the pump chamber based on a change amount of a pressure value detected by the pressure detection part.

8. The liquid delivery device according to claim 6 , further comprising a calorific value calculation part that calculates a calorific value of a mobile phase in the pump chamber based on a change amount of a temperature detected by the temperature detection part.

9. The liquid delivery device according to claim 1 comprising an outlet pipe disposed outside the pump head of the pressurizing pump and communicating with the outlet channel, the outlet pipe is covered with a heat insulating member.

10. A fluid chromatograph at least comprising:
an analysis channel;
a liquid delivery device that includes at least one or more plunger pumps,
wherein the at least one or more plunger pumps each include a pump head having a pump chamber provided in an inside, a plunger having a tip which is slidably inserted into the pump chamber, and a drive mechanism that reciprocates the plunger in an axial direction thereof,
at least one of the at least one or more plunger pumps is a pressurizing pump that pressurizes a mobile phase including a compressible fluid sucked into the pump chamber and then discharges the mobile phase from the pump chamber, and
at least the pump head of the pressurizing pump includes a cooling part formed by at least one channel connected with an outlet channel of the pump chamber, the cooling part is configured to cause the pump head to absorb heat of a mobile phase that is discharged from the pump chamber and flows into the at least one channel, and is provided to cool the mobile phase;
the liquid delivery device that delivers a mobile phase in an analysis channel;
a sample injection part that injects a sample into the analysis channel;
a separation column that is provided downstream of the sample injection part on the analysis channel, and separates a sample injected into the analysis channel by the sample injection part into components; and

a detector that is provided downstream of the separation column on the analysis channel and detects the components separated by the separation column.

Assignees

• Shimadzu Corp

Inventors

• Yanagibayashi Jun

Classifications

• F04B49/065

  and making use of computers · CPC title

• F04B11/0075 Primary

  connected in series · CPC title

• F04B53/08

  Cooling; Heating; Preventing freezing · CPC title

• F04B23/06 Primary

  the pumps being all of reciprocating positive-displacement type · CPC title

• F04B53/16

  Casings; Cylinders; Cylinder liners or heads; Fluid connections · CPC title