Methods of forming dynamic cross-linked polymer compositions using functional chain extenders under batch process
US-2019270847-A1 · Sep 5, 2019 · US
US11097976B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-11097976-B2 |
| Application number | US-201916418075-A |
| Country | US |
| Kind code | B2 |
| Filing date | May 21, 2019 |
| Priority date | May 23, 2018 |
| Publication date | Aug 24, 2021 |
| Grant date | Aug 24, 2021 |
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A method of processing an optical fiber includes drawing the optical fiber from a heated glass source, reheating the optical fiber, and cooling the optical fiber under vacuum at a cooling rate less than the cooling rate of the optical fiber in air at 25° C. and 1 atm. Cooling the optical fiber under vacuum is conducted after reheating the optical fiber. Cooling the optical fiber under vacuum reduces the rate of heat transfer from the optical fiber, which may enable further relaxation of the glass and reduction in the fictive temperature of the optical fiber. A system for processing an optical fiber includes a furnace containing a fiber preform, a first positioner, a reheating device, and a treatment device downstream of the reheating device, the treatment device operable to cool the optical fiber under vacuum to reduce the rate of heat transfer from the optical fiber.
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What is claimed is: 1. A method for processing an optical fiber, the method comprising: drawing the optical fiber from a heated glass source; positioning the optical fiber; reheating the optical fiber after the positioning the optical fiber; and cooling the optical fiber after the reheating the optical fiber, wherein the reheating and the cooling the optical fiber are conducted under vacuum and the cooling is conducted at a cooling rate less than a cooling rate of the optical fiber in air at 25° C. and 1 atm. 2. The method of claim 1 , wherein the vacuum has a pressure of from 0.005 atmospheres (atm) to 0.8 atm. 3. The method of claim 1 , the positioning the optical fiber occurs under vacuum at a pressure of from 0.005 atm to 0.8 atm. 4. The method of claim 1 , wherein the cooling the optical fiber comprises passing the optical fiber through a chamber of a treatment device, wherein the chamber is maintained at a pressure of from 0.005 atm to 0.8 atm as the optical fiber passes through the chamber. 5. The method of claim 4 , wherein at least a portion of the treatment device downstream of a reheating device has an inner diameter of from 4 cm to 40 cm. 6. The method of claim 4 , wherein a positioner for the positioning the optical fiber is disposed within the chamber of the treatment device. 7. The method of claim 4 , further comprising reducing a temperature gradient between the treatment device and the optical fiber by heating an internal surface of the treatment device. 8. The method of claim 4 , further comprising introducing a working gas to the treatment device, the working gas having a thermal conductivity less than the thermal conductivity of air. 9. The method of claim 8 , wherein the working gas is argon. 10. The method of claim 4 , wherein the optical fiber passed out of the treatment device has a temperature of greater than 500° C. 11. The method of claim 1 , wherein the positioning the optical fiber comprises passing the optical fiber over at least one fluid bearing. 12. The method of claim 1 , wherein the positioning the optical fiber comprises changing a direction of the process pathway of the optical fiber drawn from the heated glass source. 13. The method of claim 1 , further comprising passing the optical fiber through a heated slow-cooling device before the positioning the optical fiber. 14. The method of claim 1 , wherein the drawing occurs at a speed greater than 50 m/s. 15. The method of claim 1 , wherein the heated glass source comprises silica. 16. An optical fiber produced by the method of claim 1 , wherein the optical fiber has a fictive temperature less than or equal to 1450° C.
Improving the yield, e-g- reduction of reject rates · CPC title
Annealing or re-heating · CPC title
Drawing at high speed, i.e. > 10 m/s · CPC title
to the outside of the preform or fibre · CPC title
Thermal treatment of the fibre during the drawing process, e.g. cooling (coating C03C25/10) · CPC title
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