Biochars, biochar extracts and biochar extracts having soluble signaling compounds and method for capturing material extracted from biochar

Patent metadata

Field	Value
Publication number	US-11097241-B2
Application number	US-201816223050-A
Country	US
Kind code	B2
Filing date	Dec 17, 2018
Priority date	Oct 1, 2014
Publication date	Aug 24, 2021
Grant date	Aug 24, 2021

Abstract

A method for capturing material extracted from biochar is provided comprising the steps of: (i) providing a biochar; (ii) contacting the biochar with an extraction media, where the extraction media causes the removal of residual compounds from the pores and surface of the biochar, creating a resulting extract comprised of the extraction media and removed compounds; and (iii) collecting the resulting extract. The method also can include other steps of extraction and purification. The method further comprises the step of applying the resulting extract to seeds, plants, soil, other agricultural products, or for use in other applications. A biochar having high levels of soluble signaling compounds is also provided, where the biochar is derived from a biomass source that together with predefined pyrolysis parameters produces resulting biochar having increased levels of soluble signaling compounds that are known to increase seed germination rates and early plant growth. Such soluble signaling compounds can then be collected in a biochar extract by contacting the biochar with an extraction media.

First claim

We claim:

1. A method for capturing material extracted from biochar, the method comprising the steps of:
providing a biochar that includes soluble signaling compounds;
contacting the biochar with an extraction media, wherein the extraction media removes at least some of the soluble signaling compounds from the biochar, thereby creating a biochar extract containing soluble signaling compounds;
separating at least a majority of the biochar from the biochar extract; and
collecting the biochar extract for further use and/or processing separate from, or prior to, disposal, the biochar extract comprising the extraction media and the soluble signaling compounds collected from the biochar.

2. The method of claim 1 further including the step of reincorporating the biochar extract into a biochar.

3. The method of claim 1 where the soluble signaling compounds are cyanohydrins.

4. The method of claim 1 where the soluble signaling compounds are butenolides.

5. The method of claim 1 where the soluble signaling compounds are karrikins.

6. The method of claim 5 where the starting biochar has karrikin levels that exceed 10 ng/g.

7. The method of claim 1 , where the extraction media is water.

8. The method of claim 1 , where the extraction media is ethanol.

9. The method of claim 1 , where the extract method is used to improve the availability and effectiveness of the remaining level of soluble signaling compounds in the biochar.

10. The method of claim 1 where the biochar extract is further processed to concentrate the extracted compound, purify the extract to remove deleterious compounds, or to separate the extracted compounds from the initial extraction media and then suspend, mix, or dissolve the extracted compounds into a different media.

11. The method of claim 1 , where the soluble signaling compounds are carboxylic acids, anhydrous sugars, fatty acids, alkanes, ketones, aldehydes, aromatics, or phenolics.

12. The method of claim 1 , where the biochar extract is further processed to separate the extracted compounds from the initial extraction media and then those extracted compounds are suspended, mixed or dissolved into a different media.

13. A biochar extract having levels of soluble signaling compounds exceeding 0.005 ppb, where the soluble signaling compounds increases seed germination rates and early plant growth and where the biochar extract is made by washing the biochar with a extraction media and capturing the extraction media with or without further processing for subsequent use as a soil additive, plant treatment, or seed treatment.

14. A biochar extract produced by the method of claim 1 .

15. The biochar extract of claim 14 , where the biochar extract includes karrikins.

16. The biochar extract of claim 14 , where the biochar extract has been further processed to concentrate the amount of extracted compounds in the extract.

17. The biochar extract of claim 14 , where the biochar extract has been further processed to remove deleterious substances.

18. The biochar extract of claim 14 where the biochar extract is further treated with surfactant to improve the availability and effectiveness of the soluble signaling compounds.

19. A biochar extract extracted from a biochar having karrikin levels that exceed 10 ng of karrikin/g of biochar, where the biochar results from a source of biomass that has been pyrolyzed by controlling the pyrolysis parameters based on the source of biomass, where the biochar extract has properties that improve seed germination and early plant development, and where the biochar extract is made by washing the biochar with an extraction media and collecting the extraction media for subsequent use as a soil additive, plant treatment, or seed treatment.

20. The biochar extract of claim 19 having karrikin levels that exceed 0.005 ppb.

21. The biochar extract of claim 13 , where the soluble signaling compounds are carboxylic acids, anhydrous sugars, fatty acids, alkanes, ketones, aldehydes, aromatics, or phenolics.

22. The biochar extract of claim 13 where the soluble signaling compounds are cyanohydrins.

23. The biochar extract of claim 13 where the soluble signaling compounds are butenolides.

24. The biochar extract of claim 13 where the soluble signaling compounds are karrikins.

25. The biochar extract of claim 24 where the level of karrikin in the biochar extract exceeds 0.05 ppb.

26. The biochar extract of claim 24 where the karrikin levels exceed 0.5 ppb.

27. A method for capturing material extracted from biochar, the method comprising the steps of:
providing a biochar that includes soluble signaling compounds;
contacting the biochar with an extraction media, wherein the extraction media removes at least some of the soluble signaling compounds from the biochar, thereby creating a biochar extract containing soluble signaling compounds;
separating the biochar from the biochar extract; and
collecting the biochar extract from which the biochar has been separated for further use and/or processing separate from, or prior to, disposal, the biochar extract comprising the extraction media and the soluble signaling compounds from the biochar and wherein the biochar extract is further processed to concentrate the soluble signaling compounds.

28. A method for capturing material extracted from biochar, the method comprising the steps of:
providing a biochar that includes soluble signaling compounds;
contacting the biochar with an extraction media, wherein the extraction media removes at least some of the soluble signaling compounds from the biochar, thereby creating a biochar extract containing extraction media and soluble signaling compounds;
separating the biochar from the biochar extract;
collecting the biochar extract from which the biochar has been separated for further use and/or processing separate from, or prior to, disposal; and
applying the biochar extract to seeds, soil, or plants.

Assignees

• Cool Planet Energy Systems Inc
• Talipot Cool Extract Ip Llc

Inventors

• Kim Han Suk
• Smith Matthew William
• Wan Haijun
• Belcher Richard Wilson
• Bontchev Ranko Panayotov
• Buege Brian

Classifications

• A23K50/75

  for poultry · CPC title

• A23K20/147

  Polymeric derivatives, e.g. peptides or proteins · CPC title

• B01J20/3028

  Granulating, agglomerating or aggregating · CPC title

• A23K20/10

  Organic substances · CPC title

• B01J20/3007

  Moulding, shaping or extruding · CPC title