Flame atomic absorption spectrophotometer

Patent metadata

Field	Value
Publication number	US-11092552-B2
Application number	US-201716627169-A
Country	US
Kind code	B2
Filing date	Jul 10, 2017
Priority date	Jul 10, 2017
Publication date	Aug 17, 2021
Grant date	Aug 17, 2021

Abstract

A flame atomic absorption spectrophotometer in which an angle of a burner can be manually adjusted and a rotation position of the burner can be easily obtained is provided. An atomization unit burns mixed gas of fuel gas and supporting gas with a burner to form flame, and atomizes a sample by spraying the sample into the flame. Alight source emits a measuring beam into the flame. A detector detects the measuring beam that has passed through the flame. A manual rotation mechanism allows the burner to be manually rotated to change an angle of the burner with respect to an optical path of the measuring beam. A rotation position detection unit detects a rotation position of the burner.

First claim

The invention claimed is:

1. A flame atomic absorption spectrophotometer, comprising:
an atomization unit that atomizes a sample by burning mixed gas of fuel gas and supporting gas with a burner to form a flame, and spraying the sample into the flame;
a light source that emits a measuring beam into the flame;
a detector that detects a measuring beam that has passed through the flame;
a manual rotation mechanism for manually rotating the burner to change an angle of the burner with respect to an optical path of the measuring beam;
a rotation position detection unit that discretely detects a rotation position of the burner; and
a storage unit that stores, in association with calibration curve data obtained by measuring a known sample, as a device condition, a rotation position of the burner when the calibration curve data is obtained.

2. The flame atomic absorption spectrophotometer according to claim 1 , further comprising:
a sample concentration calculation unit that calculates a concentration of a sample based on measurement data obtained by measuring an unknown sample and the calibration curve data obtained under a same condition as that at the time of the measurement, wherein
in association with the concentration of the sample calculated by the sample concentration calculation unit and calibration curve data used when the concentration of the sample is calculated, the storage unit stores, as a device condition, a rotation position of the burner when the calibration curve data is obtained.

3. The flame atomic absorption spectrophotometer according to claim 2 , further comprising:
a data output unit that outputs, as report data, the concentration of the sample calculated by the sample concentration calculation unit, calibration curve data used when the concentration of the sample is calculated, and a device condition including a rotation position of the burner when the calibration curve data is obtained.

4. The flame atomic absorption spectrophotometer according to claim 1 , wherein
the rotation position detection unit includes an optical sensor that includes a light emitting unit and a light receiving unit.

5. The flame atomic absorption spectrophotometer according to claim 1 , wherein
the rotation position detection unit includes a plurality of optical sensors provided on a trajectory of a light shielding unit that moves as the burner rotates.

6. The flame atomic absorption spectrophotometer according to claim 5 , wherein
the plurality of optical sensors are disposed at equal intervals in a circumferential direction around a rotation shaft of the burner.

7. The flame atomic absorption spectrophotometer according to claim 1 , wherein
the rotation position detection unit transfers the rotation position to a computer processor, and
the computer processor receives the rotation position from the rotation position detection unit, generates calibration curve data by measuring a known sample, and transfers the calibration curve data and a rotation position of the burner when the calibration curve data is generated to the storage unit.

Assignees

• Shimadzu Corp

Inventors

• Kobayashi Osuke

Classifications

• G01N21/3103

  Atomic absorption analysis · CPC title

• G01N21/714 Primary

  Sample nebulisers for flame burners or plasma burners (nebulizers per se B05B) · CPC title