Process for reducing total acid number of heat transfer fluid

US11053446B2 · US · B2

Patent metadata
FieldValue
Publication numberUS-11053446-B2
Application numberUS-201816615114-A
CountryUS
Kind codeB2
Filing dateMay 18, 2018
Priority dateMay 19, 2017
Publication dateJul 6, 2021
Grant dateJul 6, 2021

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  1. Title

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  2. Abstract

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  3. Assignees and inventors

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  4. Key dates

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  5. First independent claim

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  6. CPC / IPC classifications

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  7. Citations and related patents

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Abstract

Official abstract text for this publication.

The present disclosure relates to a process to reduce total acid number (TAN) of a heat transfer fluid. The process comprises contacting the heat transfer fluid with an adsorbent composition at a temperature in the range of 50° C. to 350° C. and a pressure in the range of 1 bar to 10 bar to obtain a treated heat transfer fluid having total acid number (TAN) in the range of 0.003 to 0.03 and pH in the range of 6 to 7.5, wherein the adsorbent composition is provided in a fixed bed and the heat transfer fluid is passed through the fixed bed comprising the adsorbent composition at a liquid hourly space velocity (LHSV) in the range of 0.5 per hour to 10 per hour.

First claim

Opening claim text (preview).

The invention claimed is: 1. A process for reducing total acid number of heat transfer fluid, the process comprising step of contacting said heat transfer fluid with an adsorbent composition to obtain a treated heat transfer fluid having total acid number (TAN) in the range of 0.003 to 0.03 mg KOH/g and pH in the range of 6 to 7.5; wherein said adsorbent composition is provided in a fixed bed and said heat transfer fluid is passed through said fixed bed at a predetermined liquid hourly space velocity (LHSV), at a predetermined temperature and at a predetermined pressure; wherein said adsorbent composition comprises; a layered double hydroxide in an amount in the range of 15 to 70 wt % of the total mass of the composition; alumina in an amount in the range of 30 to 85 wt % of the total mass of the composition; and optionally, activated bauxite in an amount in the range of 15 to 50 wt % of the total mass of the composition. 2. The process as claimed in claim 1 , wherein said predetermined liquid hourly space velocity (LHSV) is in the range of 0.5 per hour to 10 per hour. 3. The process as claimed in claim 1 , wherein said predetermined liquid hourly space velocity (LHSV) is in the range of 1 per hour to 5 per hour. 4. The process as claimed in claim 1 , wherein said predetermined temperature is in the range of 50° C. to 350° C. 5. The process as claimed in claim 1 , wherein said predetermined temperature is in the range of 100° C. to 250° C. 6. The process as claimed in claim 1 , wherein said predetermined pressure is in the range of 1 bar to 10 bar. 7. The process as claimed in claim 1 , wherein said predetermined pressure is in the range of 1 bar to 5 bar. 8. The process as claimed in claim 1 , wherein the weight ratio of the heat transfer fluid to the adsorbent composition is in the range of 5:1 to 30:1. 9. The process as claimed in claim 1 , wherein the weight ratio of the heat transfer fluid to the adsorbent composition is in the range of 10:1 to 20:1.

Assignees

Inventors

Classifications

  • Used oils · CPC title

  • C10G25/006Primary

    of waste oils, e.g. PCB's containing oils · CPC title

  • C10G25/02Primary

    with ion-exchange material · CPC title

  • Refining of hydrocarbon oils, in the absence of hydrogen, by methods not otherwise provided for (by distillation C10G7/00) · CPC title

  • Liquid materials · CPC title

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What does patent US11053446B2 cover?
The present disclosure relates to a process to reduce total acid number (TAN) of a heat transfer fluid. The process comprises contacting the heat transfer fluid with an adsorbent composition at a temperature in the range of 50° C. to 350° C. and a pressure in the range of 1 bar to 10 bar to obtain a treated heat transfer fluid having total acid number (TAN) in the range of 0.003 to 0.03 and pH …
Who is the assignee on this patent?
Reliance Industries Ltd
What technology area does this patent fall under?
Primary CPC classification C10G25/006. Mapped technology areas include Chemistry & Metallurgy.
When was this patent published?
Publication date Tue Jul 06 2021 00:00:00 GMT+0000 (Coordinated Universal Time) (B2). Legal status and post-grant events are not shown on this page.
What related patents are in patentsdb?
We list 4 related publications on this page (citations in our corpus or others sharing the same primary CPC).