Physical properties measurement system

Patent metadata

Field	Value
Publication number	US-11047817-B2
Application number	US-201916387340-A
Country	US
Kind code	B2
Filing date	Apr 17, 2019
Priority date	Apr 17, 2019
Publication date	Jun 29, 2021
Grant date	Jun 29, 2021

Abstract

A sealed container having gloves attached thereto is provided as part of a physical properties measuring system (PPMS). The PPMS includes a sealed pressurized portion that is pressurized with a gas to purge out air from inside the sealed pressurized portion to reduce water vapor inside the sealed pressurized portion below a water vapor threshold. The system further includes a cryogenic tank having a cryostat disposed therein. The cryogenic tank contains a cryogenic liquid cooled to a cryogenic temperature. Test samples are placed inside the sealed pressurized portion in preparation of measuring physical properties of the test samples. One of the test samples is immersed in the cryogenic liquid to measure the physical properties. The test sample is removed from the cryogenic liquid and is exchanged for another test sample inside the sealed pressurized portion to prevent ice formation inside the cryostat.

First claim

What is claimed is:

1. A physical properties measuring system comprising:
a cryogenic tank that contains a cryogenic liquid cooled to a cryogenic temperature, the cryogenic tank including a cryostat disposed therein and having an opening defined in a top surface;
a sealed container attached to the cryogenic tank, the sealed container including a mounting opening defined in a bottom surface that aligns with the opening in the top surface of the cryogenic tank and a fastening device that attaches the sealed container to the cryogenic tank such that an air tight seal is formed between the sealed container and the cryogenic tank;
a test rod retraction tube attached to a top surface of the sealed container, the test rod retraction tube having a seal flange that seals an opening defined in the top surface of the sealed container such that an air tight seal is formed between the sealed container and the test rod retraction tube;
a door attached to a door side wall of the sealed container, the door including a seal that forms an air tight seal between the door and the door side wall when the door is in a closed position; and
gloves that allow access the interior of the sealed container via glove openings defined in opposite side walls of the sealed container and seal ring assemblies that seal the gloves to the side walls of the sealed container such that an air tight seal is formed between the sealed container and the gloves.

2. The physical properties measuring system of claim 1 , wherein the sealed container further includes support legs that extend from the bottom surface of the sealed container toward the cryogenic tank and contact the top of the cryogenic tank to support the sealed container.

3. The physical properties measuring system of claim 1 further comprising a gas storage tank that supplies gas to the sealed container via a gas transfer hose to an opening defined in a side wall of the sealed container, wherein the gas pressurizes the sealed container to purge air out from inside the sealed container and the test rod retraction tube to reduce water vapor inside the sealed container and the test rod retraction tube to below a water vapor threshold.

4. The physical properties measuring system of claim 1 further comprising a test rod holding device attached between the top of the cryogenic tank and the bottom surface of the sealed container, wherein the test rod holding device secures a test rod in place during measurement of physical properties of a plurality of test samples.

5. The physical properties measuring system of claim 4 , wherein the test rod holding device is a vibrating mechanism that vibrates the test rod during measurement of the physical properties.

6. The physical properties measuring system of claim 1 , wherein a plurality of test samples are placed inside the sealed container via the door in preparation of measuring physical properties of the plurality of test samples.

7. The physical properties measuring system of claim 6 , wherein one of the plurality of test samples is immersed in the cryogenic liquid to measure the physical properties.

8. The physical properties measuring system of claim 7 , wherein the one of the plurality of test samples is removed from the cryogenic tank and is exchanged for another one of the plurality of test samples inside the sealed container to prevent ice formation inside the cryostat.

9. The physical properties measuring system of claim 8 , wherein the test rod retraction tube receives a test rod when the one of the plurality of test samples is removed from the cryogenic tank and is exchanged for another one of the plurality of test samples inside the sealed container.

10. The physical properties measuring system of claim 6 , wherein the test samples are silicon wafers and the measured physical properties include magnetic and superconductive properties.

11. The physical properties measuring system of claim 1 , wherein the cryogenic temperature is approximately 4 K.

12. The physical properties measuring system of claim 1 , wherein the cryogenic liquid is liquid helium.

Assignees

• Dietrich Kurt Edward
• Ambrose Thomas F
• Gingrich Eric C
• Barbour Timothy Richard
• Northrop Grumman Systems Corp

Inventors

• Dietrich Kurt Edward
• Ambrose Thomas F
• Gingrich Eric C
• Barbour Timothy Richard

Classifications

• H10W40/305

  the fluid being a liquefied gas, e.g. liquid nitrogen · CPC title

• B01L2300/1894

  Cooling means; Cryo cooling · CPC title

• G01N25/18 Primary

  by investigating thermal conductivity (by calorimetry G01N25/20; by measuring change of resistance of an electrically-heated body G01N27/18) · CPC title

• F17C2270/0509

  "Dewar" vessels · CPC title

• G01R33/1238

  Measuring superconductive properties · CPC title