Semi-passive control of solidification in powdered materials
US-2017021417-A1 · Jan 26, 2017 · US
US11045905B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-11045905-B2 |
| Application number | US-201715411386-A |
| Country | US |
| Kind code | B2 |
| Filing date | Jan 20, 2017 |
| Priority date | Jan 20, 2017 |
| Publication date | Jun 29, 2021 |
| Grant date | Jun 29, 2021 |
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A method of manufacturing an object is disclosed. In some aspects, the method includes selectively heating an initial layer of a composition, including elements of a granular material coated with a metallic material. The method further includes selectively heating an additional layer of the composition, disposed in contact with the initial layer, the selective heating of each respective layer to the threshold temperature actuating an exothermic reaction between the elements of the granular material and the metallic material coating associated therewith to form a molten portion of the respective layer, with turbulence in the molten portion of the respective layer disrupting oxidation of the molten granular material and promoting formation of an intermetallic compound in the molten portion of the respective layer upon cooling thereof below the threshold temperature, and with the portions of the respective layers combining to form the object.
Opening claim text (preview).
That which is claimed: 1. A method of manufacturing an object comprising: determining a thickness of a metallic material coating comprising nickel for coating particles of a granular material based on a desired weight fraction of the metallic material coating relative to a weight of the overall particle of the granular material coated with the metallic material coating, wherein the desired weight fraction of the metallic material coating comprising nickel is between 3.8 and 29.2 percent by weight; coating the particles of the granular material with the metallic material coating having the determined thickness; selectively heating an initial layer of a composition, comprising the particles of the granular material coated with the metallic material comprising nickel, to a threshold temperature using a laser in a selective laser melting (SLM) process; and selectively heating an additional layer of the composition comprising the particles of the granular material coated with the metallic material comprising nickel, disposed in contact with the initial layer, to the threshold temperature using the laser in the SLM process, the selective heating of each respective layer to the threshold temperature actuating an exothermic reaction between the particles of the granular material and the metallic material coating associated therewith to form a molten portion of the respective layer including molten granular material, with turbulence in the molten portion of the respective layer disrupting oxidation of the molten granular material and promoting formation of an intermetallic compound in the molten portion of the respective layer upon cooling thereof below the threshold temperature, and with the portions of the respective layers combining to form the object. 2. The method according to claim 1 , comprising distributing the initial layer of the composition on a substrate such that the initial layer has a thickness of between about 20 micrometers and about 150 micrometers, prior to selectively heating the initial layer. 3. The method according to claim 2 , wherein distributing the additional layer of the composition in contact with the initial layer comprises distributing the additional layer of the composition in contact with the initial layer, the composition of the additional layer having the same or different particles than the composition of the initial layer. 4. The method according to claim 1 , comprising distributing the additional layer of the composition in contact with the initial layer such that the additional layer has a thickness of between about 20 micrometers and about 150 micrometers, prior to selectively heating the additional layer. 5. The method according to claim 4 , wherein distributing the additional layer of the composition in contact with the initial layer comprises distributing the additional layer of the composition in contact with the initial layer, the composition of the additional layer having the same or different particles than the composition of the initial layer. 6. The method according to claim 1 , wherein coating the particles of the granular material comprises coating the particles of the granular material using an electroless plating process, an electrolytic plating process, a sputtering process, a chemical vapor deposition process, or other vapor deposition processes. 7. The method according to claim 1 , wherein coating the particles of the granular material comprises coating the particles of the granular material with the metallic material such that the coating has a thickness of between about 0.1 micrometers and about 1 micrometer. 8. The method according to claim 1 , wherein selectively heating the initial layer or selectively heating the additional layer comprises selectively heating the initial layer or selectively heating the additional layer, the initial layer or the additional layer comprising the particles of an aluminum powder or an aluminum alloy powder coated with the metallic material, to the threshold temperature. 9. The method according to claim 8 , wherein selectively heating the initial layer comprises selectively heating the initial layer comprising the particles of the aluminum powder or the aluminum alloy powder coated with the metallic material. 10. The method according to claim 8 , wherein selectively heating the additional layer comprises selectively heating the additional layer comprising the particles of the aluminum powder or the aluminum alloy powder coated with the metallic material. 11. The method according to claim 1 , comprising cooling the molten portion of the initial layer or the additional layer to a solidification temperature, the solidification temperature being less than the threshold temperature, so as to solidify the portion of the initial layer or the additional layer, with the solidified portion of the initial layer or the additional layer comprising discrete particles or eutectic colonies of the intermetallic compound and with oxide particles produced from the disrupted oxidation of the molten granular material being in spaced apart relation to each other. 12. The method according to claim 11 , comprising cooling the molten portion of the initial layer to the solidification temperature so as to solidify the portion of the initial layer, with the solidified portion of the initial layer comprising the discrete particles or eutectic colonies of the intermetallic compound and with the oxide particles produced from the disrupted oxidation of the molten granular material being in spaced apart relation to each other. 13. The method according to claim 11 , comprising cooling the molten portion of the additional layer to the solidification temperature so as to solidify the portion of the additional layer, with the solidified portion of the additional layer comprising the discrete particles or eutectic colonies of the intermetallic compound and with the oxide particles produced from the disrupted oxidation of the molten granular material being in spaced apart relation to each other. 14. A method of manufacturing an object comprising: determining a thickness of a metallic material coating comprising nickel for coating particles of a granular material based on a desired weight fraction of the metallic material coating relative to a weight of the overall particle of the granular material coated with the metallic material coating, wherein the desired weight fraction of the metallic material coating comprising nickel is between 3.8 and 29.2 percent by weight; coating the particles of the granular material with the metallic material coating having the determined thickness; and selectively heating a layer of a composition, comprising the particles of the granular material coated with the metallic material comprising nickel, to a threshold temperature using a laser in a selective laser melting (SLM) process so as to actuate an exothermic reaction between the particles of the granular material and the metallic material coating associated therewith and to form a molten portion of the layer including molten granular material, with turbulence in the molten portion of the layer disrupting oxidation of the molten granular material and promoting formation of an intermetallic compound in the molten portion of the layer upon cooling thereof below the threshold temperature. 15. The method according to claim 14 , comprising cooling the molten portion of the layer to a solidification temperature, the solidification temperature being less than the threshold temperature, so as to solidify the portion of the layer, with the solidified portion of the layer comprising discrete particles or eutectic c
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