Method for manufacturing a part having a complex shape by flash sintering, and device for implementing such a method

Patent metadata

Field	Value
Publication number	US-11045873-B2
Application number	US-201214008334-A
Country	US
Kind code	B2
Filing date	Mar 29, 2012
Priority date	Mar 31, 2011
Publication date	Jun 29, 2021
Grant date	Jun 29, 2021

Abstract

The invention relates to a method for manufacturing a metal, ceramic, or composite part (PF) by flash sintering, which comprises simultaneously applying, inside a die (M), a uniaxial pressure and an electric current to a device containing a powder constituent material, said uniaxial pressure being applied by means of at least two pistons (P1, P2) which slide toward one another inside said die and each of which has a bearing surface (F1, F2) contacting said material, said bearing surfaces engaging so as to define the shape of the part to be manufactured, characterised in that: said part has a complex shape, including at least one first slender portion (V), such as a rod, plate, bevel, or shell, and a second portion (B), such as a base, plinth, or solid part, which is not slender in the slender direction of said first portion, and in that said uniaxial pressure is applied in a direction (z) substantially parallel to the smallest dimension of said first portion of the part, or to one of the two smallest dimensions thereof if said part is a rod. The invention also relates to a device for implementing such a method, and to a turbine blade made of a TiAl intermetallic alloy or a metal/silicide composite sintered by flash sintering.

First claim

The invention claimed is:

1. A method of manufacturing by flash sintering a component made of metal, ceramic or composite, directly from a powder constituent material, the method comprising:
at least one flash sintering step including a simultaneous application, within a die made of an electrically conducting material, of a uniaxial pressure and of an electrical current, said uniaxial pressure being applied either directly by at least two pistons having bearing surfaces in contact with said powder constituent material or via electrically conductive force-transmitting components, said electrically conductive force-transmitting components being interposed between said at least two pistons and the powder constituent material, said force-transmitting components or said pistons having bearing surfaces in contact with said powder constituent material, said at least two pistons sliding one toward the other inside said die, bearing surfaces of the at least two pistons or bearing surfaces of the electrically conductive force-transmitting components collaborating with one another and the powder constituent material to define the shape of the component to be manufactured,
wherein said component to be manufactured comprises a first part that is tapered according to a first direction and having a cross-sectional area that decreases from a second part along the first direction, the second part being a base, a mount, a solid component, or a plate component, and
said uniaxial pressure is applied in a direction: parallel to a direction defined by a smallest dimension of said first part of the component to be manufactured.

2. The method as claimed in claim 1 , wherein only one flash sintering step is employed.

3. The method as claimed in claim 1 , wherein the at least two pistons and the component to be manufactured are surrounded by inserts of D-shaped overall cross-section having a first surface having the shape of an assembly comprising the at least two pistons and the powder constituent material and a second surface in the shape of a cylindrical arc, having the shape of an internal surface of the die.

4. The method as claimed in claim 1 , further comprising:
calibrating temperatures so that a temperature field within an assembly comprising the die, the pistons, the powder constituent material and any inserts are associated with each value of temperature measured at a point on the die or the pistons by a temperature sensor; and
a feedback control of a strength of the electric current to control a difference between the temperature measured by said temperature sensor and a reference temperature.

5. The method as claimed in claim 4 , wherein said reference temperature is determined by numerical simulation.

6. The method as claimed in claim 1 , wherein said powder constituent material is based on a metal-metal alloy.

7. The method as claimed in claim 6 , wherein said metal-metal alloy is an alloy based on titanium.

8. The method as claimed in claim 1 , wherein said powder constituent material contains a metal, and a silicide of the metal or of a different metal.

9. The method as claimed in claim 1 , wherein said first part of the component to be manufactured is a skew shell.

10. The method as claimed in claim 9 , wherein said component to be manufactured is a turbine blade preform to near-finished dimensions.

11. A turbine blade in metal-metal alloy based on TiAl made by the method as claimed in claim 1 .

12. The method as claimed in claim 10 , wherein the turbine blade is based on metal-silicide.

13. The method as claimed in claim 1 , wherein a first dimension of the component to be manufactured according to the first direction is larger than other dimensions of the component to be manufactured that are other than the first dimension.

14. The method as claimed in claim 1 , wherein the second part extends in a plane which is perpendicular to the first direction.

15. The method as claimed in claim 1 , wherein the second part has a volume bounded by two surfaces distant from one another by a thickness that is smaller in comparison with other dimensions of the second part other than the thickness, a plurality of ratios between the other dimensions of the second part and the thickness being greater than 3.

16. The method as claimed in claim 1 , wherein the first part: has a volume bounded by two surfaces distant from one another by a thickness that is smaller in comparison with other dimensions of the first part other than the thickness, a plurality of ratios between the other dimensions of the first part and the thickness being greater than 3, or is elongated in one direction and is configured to be inscribed inside a cylinder or prism of length L and of base diameter or side length D, with an L/D ratio greater than or equal to 2.

17. The method as claimed in claim 1 , wherein the first part is one of a rod, a plate, a bevel, and a shell, and
wherein said axial direction is parallel to the smallest dimension of said first part or one of its two smallest dimensions when the first part is the rod.

18. The method as claimed in claim 1 , wherein:
the first part is a component of one of:
constant or variable cross-section, that is elongated in one direction and is configured to be inscribed inside a cylinder or prism of length L and of base diameter or side length D, with an L/D ratio greater than or equal to 2, and
volume bounded by two near-parallel planar or non-planar surfaces, distant from one another by a mean thickness e m that is smaller with respect to other dimensions d 1 , d 2 , with d 1 /e m and d 2 /e m ratios greater than or equal to 3, and

the second part is a component in which the ratio between a longest dimension or longest dimensions and a shortest dimension of the second part does not exceed a factor of 2.

19. The method as claimed in claim 1 , wherein the first part is tapered according to at least one longest dimension thereof and the smallest dimension of the first part is perpendicular to the first direction.

20. The method as claimed in claim 1 , wherein said uniaxial pressure is applied in a direction perpendicular to the first direction.

21. The method as claimed in claim 1 , wherein said uniaxial pressure is applied at right angles relative to the first direction and in a direction perpendicular to a direction defined by a longest dimension or longest dimensions of the second part.

22. The method as claimed in claim 1 , wherein at least one longest dimension of the second component is perpendicular to the direction in which the first part is tapered.

Assignees

• Couret Alain
• Monchoux Jean Philippe
• Durand Lise
• Jabbar Houria
• Voisin Thomas
• Centre Nat Rech Scient

Inventors

• Couret Alain
• Monchoux Jean-Philippe
• Durand Lise
• Jabbar Houria
• Voisin Thomas

Classifications

• B22F3/14 Primary

  simultaneously · CPC title

• C22C29/18

  based on silicides · CPC title

• F01D5/28

  Selecting particular materials; {Particular measures relating thereto;} Measures against erosion or corrosion · CPC title

• C04B2235/666

  Applying a current during sintering, e.g. plasma sintering [SPS], electrical resistance heating or pulse electric current sintering [PECS] · CPC title

• C04B2235/94

  Products characterised by their shape · CPC title