Method for producing film

Patent metadata

Field	Value
Publication number	US-11045834-B2
Application number	US-201816011939-A
Country	US
Kind code	B2
Filing date	Jun 19, 2018
Priority date	Feb 2, 2016
Publication date	Jun 29, 2021
Grant date	Jun 29, 2021

Abstract

A method for producing a film comprises preserving a composition including a pigment, a resin, and a solvent under a condition of a viscosity ranging from 30 mPa·s to 150 mPa·s, and heating the composition to 40° C. to 70° C. so as to be applied during the application of the composition.

First claim

What is claimed is:

1. A method for producing a film, comprising:
preserving a composition including a pigment, a resin, and a solvent under a condition of a viscosity ranging from 30 mPa·s to 70.1 mPa·s at −20° C. to 30° C.;
heating the composition to 40° C. to 70° C.; and
applying the composition at 40° C. to 70° C. by a spin coating method,
wherein the pigment includes titanium oxide, and an average primary particle diameter of the titanium oxide is 50 nm or more and 250 nm or less.

2. The method for producing a film according to claim 1 ,
wherein the composition during the preservation has a sedimentation rate of a solid content of the composition of 10% by mass or less, when centrifuged under a condition of 3,500 revolutions for 47 minutes at a temperature for the preservation of the composition.

3. The method for producing a film according to claim 1 ,
wherein the composition is heated to 40° C. to 70° C. to adjust the viscosity of the composition to 1 mPa·s or more and less than 30 mPa·s during the application of the composition.

4. The method for producing a film according to claim 1 ,
wherein the composition is preserved by stirring intermittently, discontinuously, or continuously during the preservation of the composition.

5. The method for producing a film according to claim 1 ,
wherein the composition is preserved by allowing the composition to flow intermittently, discontinuously, or continuously during the preservation of the composition.

6. The method for producing a film according to claim 1 ,
wherein the composition further includes a polymerizable compound and a photopolymerization initiator.

7. The method for producing a film according to claim 6 ,
wherein the photopolymerization initiator includes an oxime compound.

8. The method for producing a film according to claim 1 ,
wherein the composition further includes a coloring inhibitor.

9. The method for producing a film according to claim 8 ,
wherein the coloring inhibitor is a phenol compound.

10. The method for producing a film according to claim 1 ,
wherein the composition further includes an epoxy compound.

11. The method for producing a film according to claim 1 , further comprising forming a pattern on a film formed by the application of the composition.

12. The method for producing a film according to claim 1 ,
wherein an average primary particle diameter of the titanium oxide is 50 nm or more and 180 nm or less.

13. The method for producing a film according to claim 1 ,
wherein the titanium oxide is an anatase type titanium oxide.

14. The method for producing a film according to claim 1 ,
wherein the specific surface area of the titanium oxide is 10 to 20 m 2 /g.

15. The method for producing a film according to claim 1 ,
wherein a purity of titanium dioxide of the titanium oxide is 85% or more.

16. A method for producing a film, comprising:
preserving a composition including a pigment, a resin, and a solvent by stirring intermittently, discontinuously, or continuously under a condition of a viscosity ranging from 30 mPa·s to 70.1 mPa·s;
heating the composition to 40° C. to 70° C.; and
applying the composition at 40° C. to 70° C. by a spin coating method,
wherein the pigment includes titanium oxide, and an average primary particle diameter of the titanium oxide is 50 nm or more and 250 nm or less.

17. A method for producing a film, comprising:
preserving a composition including a pigment, a resin, and a solvent by allowing the composition to flow intermittently, discontinuously, or continuously under a condition of a viscosity ranging from 30 mPa·s to 70.1 mPa·s;
heating the composition to 40° C. to 70° C.; and
applying the composition at 40° C. to 70° C. by a spin coating method,
wherein the pigment includes titanium oxide, and an average primary particle diameter of the titanium oxide is 50 nm or more and 250 nm or less.

Assignees

• Fujifilm Corp

Inventors

• Taguchi Yoshinori

Classifications

• C08F220/283 Primary

  and containing one or more carboxylic moiety in the chain, e.g. acetoacetoxyethyl(meth)acrylate · CPC title

• C08F222/102

  of dialcohols, e.g. ethylene glycol di(meth)acrylate or 1,4-butanediol dimethacrylate · CPC title

• B05D3/0218 Primary

  Pretreatment, e.g. heating the substrate · CPC title

• C08K2201/011

  Nanostructured additives · CPC title

• C08F2/44

  Polymerisation in the presence of compounding ingredients, e.g. plasticisers, dyestuffs, fillers · CPC title