Separation of manganese bismuth powders

Patent metadata

Field	Value
Publication number	US-11043319-B2
Application number	US-201816014055-A
Country	US
Kind code	B2
Filing date	Jun 21, 2018
Priority date	Jun 21, 2018
Publication date	Jun 22, 2021
Grant date	Jun 22, 2021

Abstract

A method of increasing volume ratio of magnetic particles in a MnBi alloy includes depositing a MnBi alloy powder containing magnetic particles and non-magnetic particles on a sloped surface having a magnetic field acted thereupon. The method further includes collecting falling non-magnetic particles while separated magnetic particles are magnetically retained on the sloped surface.

First claim

What is claimed is:

1. A method comprising:
melting Mn and Bi into homogenous MnBi alloy;
annealing the MnBi alloy to form bulk alloy;
crushing the bulk alloy into powder; and
directing the powder onto a sloped surface having a magnetic field acting thereupon such that MnBi particles in the powder remain on the surface and non-magnetic Bi particles in the powder fall from the surface to separate the MnBi particles and non-magnetic Bi particles, wherein the sloped surface is a plurality of adjacent planar sloped surfaces that define an inverted-V defining an apex, and wherein the powder is directed proximate the apex.

2. The method of claim 1 further comprising vibrating the sloped surface during the directing.

3. The method of claim 1 further comprising adjusting an angle of inclination of the sloped surface during the directing.

4. The method of claim 1 further comprising adjusting a strength of the magnetic field during the directing.

5. The method of claim 1 wherein the directing includes directing the powder onto an apex of the sloped surface.

6. The method of claim 1 wherein the magnetic field is applied to the sloped surface using one or more magnets disposed below the sloped surface.

7. The method of claim 6 wherein the one or more magnets are a plurality of permanent magnets adapted to be moved toward and away from the sloped surface.

8. The method of claim 6 wherein the one or more magnets includes an electromagnet, wherein the MnBi particles are magnetically maintained when an electric current is provided to the electromagnet, and wherein the MnBi particles are not magnetically maintained when the electric current is reduced.

9. The method of claim 1 , wherein the directing includes dropping the powder from a nozzle disposed vertically above at least a portion of the sloped surface.

10. The method of claim 1 wherein non-magnetic Bi particles are collected in one or more bins disposed vertically below bottom portions of the planar sloped surfaces.

11. The method of claim 1 wherein the sloped surface has an angle of inclination in a range of approximately 15 degrees to approximately 75 degrees.

12. The method of claim 11 wherein the angle of inclination is in a range of approximately 15 degrees to approximately 45 degrees.

13. A method comprising:
depositing MnBi alloy powder containing magnetic MnBi low temperature phase (LTP) particles and non-magnetic Bi particles on a sloped surface having a magnetic field of initial strength acting thereupon such that some of the magnetic MnBi LTP particles are retained on the sloped surface and the non-magnetic Bi particles fall from the sloped surface;
reducing the magnetic field to release the MnBi LTP particles retained on the sloped surface;
collecting the magnetic MnBi LTP particles released from the sloped surface;
increasing the magnetic field to a secondary strength less than the initial strength; and
depositing the collected magnetic MnBi LTP particles on the sloped surface; and
forming a magnet from the MnBi LTP particles retained on the sloped surface.

Assignees

• Ford Global Tech Llc

Inventors

• Li Wanfeng
• Liang Feng

Classifications

• C22C1/047

  comprising intermetallic compounds {(C22C1/0441 takes precedence)} · CPC title

• B02C23/08 Primary

  Separating or sorting of material, associated with crushing or disintegrating (B02C23/18 takes precedence {; beater mills combined with sifting devices B02C13/13, B02C13/14; for tumbling mills B02C17/1835}) · CPC title

• B22F2301/40

  Intermetallics other than rare earth-Co or -Ni or -Fe intermetallic alloys · CPC title

• C22C2202/02

  Magnetic · CPC title

• C22C22/00 Primary

  Alloys based on manganese · CPC title