Grain-oriented electrical steel sheet and method for manufacturing same
US-10147527-B2 · Dec 4, 2018 · US
US11031163B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-11031163-B2 |
| Application number | US-201716068121-A |
| Country | US |
| Kind code | B2 |
| Filing date | Jan 24, 2017 |
| Priority date | Jan 25, 2016 |
| Publication date | Jun 8, 2021 |
| Grant date | Jun 8, 2021 |
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An excellent low noise property and excellent low iron loss property are obtained. A grain-oriented electrical steel sheet includes refined magnetic domains formed by electron beam irradiation. When the maximum magnetic flux density is 1.7 T, the grain-oriented electrical steel sheet has a residual magnetic flux density of 0.1 to 0.7 times the residual magnetic flux density before the electron beam irradiation and a maximum magnetizing force of 1.1 to 2.0 times the maximum magnetizing force before the electron beam irradiation.
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The invention claimed is: 1. A grain-oriented electrical steel sheet comprising refined magnetic domains, wherein, in a condition excited by a magnetic field having a maximum magnetic flux density of 1.7 T, the grain-oriented electrical steel sheet has: (i) a residual magnetic flux density that is 0.1 to 0.7 times the residual magnetic flux density measured after the grain-oriented electrical steel sheet is subjected to annealing in a nitrogen atmosphere at 800° C. for 3 hours, and (ii) a maximum magnetizing force that is 1.1 to 2.0 times the maximum magnetizing force measured after the grain-oriented electrical steel sheet is subjected to annealing in a nitrogen atmosphere at 800° C. for 3 hours. 2. The grain-oriented electrical steel sheet comprising refined magnetic domains according to claim 1 , wherein the grain-oriented electrical steel sheet has a hysteresis loss at 50 Hz and 1.7 T of 0.28 W/kg or less. 3. The grain-oriented electrical steel sheet comprising refined magnetic domains according to claim 1 , wherein the grain-oriented electrical steel sheet has: (i) a residual magnetic flux density that is 0.1 to 0.5 times the residual magnetic flux density measured after the grain-oriented electrical steel sheet is subjected to annealing in a nitrogen atmosphere at 800° C. for 3 hours, and (ii) a maximum magnetizing force that is 1.1 to 1.5 times the maximum magnetizing force measured after the grain-oriented electrical steel sheet is subjected to annealing in a nitrogen atmosphere at 800° C. for 3 hours. 4. The grain-oriented electrical steel sheet comprising refined magnetic domains according to claim 2 , wherein the grain-oriented electrical steel sheet has: (i) a residual magnetic flux density that is 0.1 to 0.5 times the residual magnetic flux density measured after the grain-oriented electrical steel sheet is subjected to annealing in a nitrogen atmosphere at 800° C. for 3 hours, and (ii) a maximum magnetizing force that is 1.1 to 1.5 times the maximum magnetizing force measured after the grain-oriented electrical steel sheet is subjected to annealing in a nitrogen atmosphere at 800° C. for 3 hours. 5. A method for manufacturing the grain-oriented electrical steel sheet of claim 1 , the method comprising: subjecting a steel slab to hot rolling to obtain a hot rolled steel sheet; subjecting the hot rolled steel sheet to hot band annealing to obtain a hot rolled steel sheet after hot band annealing; subjecting the hot rolled steel sheet after hot band annealing to cold rolling once or cold rolling twice or more with intermediate annealing in between to obtain a cold rolled steel sheet with a final sheet thickness; subjecting the cold rolled steel sheet to decarburization annealing to obtain a cold rolled steel sheet after decarburization annealing; applying an annealing separator including MgO to a surface of the cold rolled steel sheet after decarburization annealing and then subjecting the cold rolled steel sheet after decarburization annealing to final annealing to obtain a steel sheet after final annealing; and subjecting the steel sheet after final annealing to magnetic domain refining treatment with electron beam irradiation; wherein during the magnetic domain refining treatment, the electron beam irradiation is performed with a beam diameter of 220 μm or less in an orthogonal direction that is orthogonal to a scanning direction of the electron beam, and with a ratio of beam maximum intensity in the orthogonal direction with respect to beam maximum intensity in the scanning direction of 0.7 or more to 1.3 or less; and wherein the electron beam irradiation is performed using two or more beam control coils, an accelerating voltage of 90 kV or more, and a stigmator, thereby producing the grain-oriented electrical steel sheet of claim 1 .
during manufacturing of plates or strips (C21D8/12 takes precedence) · CPC title
involving a localised treatment · CPC title
Cold rolling · CPC title
between cold rolling steps · CPC title
characterised by the heat treatment · CPC title
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