Suppression of samson phase formation in Al—Mg alloys by boron addition

Patent metadata

Field	Value
Publication number	US-11028462-B2
Application number	US-201815977482-A
Country	US
Kind code	B2
Filing date	May 11, 2018
Priority date	May 23, 2017
Publication date	Jun 8, 2021
Grant date	Jun 8, 2021

Abstract

A method of suppressing the Samson phase, Al3Mg2, at grain boundaries in Aluminum, comprising providing aluminum in a container, adding boron to the container, providing an inert atmosphere, arc-melting the aluminum and the boron, and mixing the aluminum and the boron in the container to form an alloy mixture. An aluminum magnesium alloy with reduced Samson phase at grain boundaries made from the method of providing aluminum in a container, adding boron to the container, providing an inert atmosphere, arc-melting the aluminum and the boron, and mixing the aluminum and the boron in the container to form an alloy mixture.

First claim

What we claim is:

1. A method of suppressing the Samson phase, Al 3 Mg 2 , at grain boundaries in aluminum, comprising:
providing aluminum in a container;
adding boron to the container;
providing an inert atmosphere;
arc-melting the aluminum and the boron;
mixing the aluminum and the boron in the container to form an alloy mixture;

wherein the aluminum is Al-5083 or Al-5456 and wherein the boron reduces supersaturation of magnesium;
wherein the boron traps the magnesium in a solid solution as AlMgB 2 phase;
further comprising the steps of
adding copper to the container prior to the step of providing the inert atmosphere;
arc-melting the aluminum and the boron and the copper;
mixing and homogenizing the aluminum, the boron and the copper in the container to form an alloy mixture;

wherein the step of mixing and homogenizing is at 500° C. for 2 hours; and
annealing at 150° C. for about 190 hours.

2. The method of suppressing the Samson phase, Al 3 Mg 2 , at grain boundaries in aluminum of claim 1 further comprising the steps of:
repeating the step of arc-melting the aluminum, the boron and the copper in the container; and
ensuring homogeneity of the alloy mixture.

Assignees

• Us Gov Sec Navy

Inventors

• Goswami Ramasis
• Qadri Syed B

Classifications

• C22C1/1094

  comprising an after-treatment · CPC title

• C22C1/02

  by melting {(C22C1/1036 takes precedence)} · CPC title

• C22C21/06

  with magnesium as the next major constituent · CPC title

• C22C1/03 Primary

  using master alloys · CPC title

• C22C1/026

  Alloys based on aluminium · CPC title