Belt dryer arrangement for drying an aqueous polymer gel and for comminuting the dried polymer gel to form dried polymer particles, and method for drying an aqueous polymer gel and for comminuting the dried polymer gel to form dried polymer particles

Patent metadata

Field	Value
Publication number	US-11022370-B2
Application number	US-201716317179-A
Country	US
Kind code	B2
Filing date	Jul 4, 2017
Priority date	Jul 15, 2016
Publication date	Jun 1, 2021
Grant date	Jun 1, 2021

Abstract

A belt drier arrangement for drying an aqueous polymer gel and for comminuting the dried polymer gel to give dried polymer particles, having: a belt drier having a drier setup and a conveyor belt for receiving and for drying the aqueous polymer gel to give a dry cake or fragments on a receiving surface of the conveyor belt, and a comminution arrangement, disposed downstream of the drier setup in product flow direction, for comminution of the dried polymer gel of the dry cake or fragments to give dried comminuted polymer particles. The comminution arrangement has a comminutor in the form of a milling drum which is disposed with an upper working line of a working edge of the milling drum at the level of or above a receiving surface of a conveyor belt, for mill processing of the dry cake or of the fragments, where the milling drum is designed to eject comminuted dried polymer particles of the dry cake or of the fragments in the downward direction.

First claim

The invention claimed is:

1. A belt drier arrangement for drying an aqueous polymer gel and for comminuting the dried polymer gel to give dried polymer particles, having:
a belt drier ( 36 ) having a drier setup ( 36 A) and a conveyor belt ( 36 F) for receiving and for drying the aqueous polymer gel to give a dry cake ( 35 ) or fragments ( 37 ) on a receiving surface (F) of the conveyor belt ( 36 F),
a comminution arrangement ( 38 ), disposed downstream of the drier setup in product flow direction, for comminution of the dried polymer gel of the dry cake ( 35 ) or fragments ( 37 ) to give dried comminuted polymer particles ( 39 ),
wherein
the comminution arrangement ( 38 ) has a comminutor in the form of a milling drum ( 38 . 1 ) and a support for the dry cake ( 35 ) or for the fragments ( 37 ) is disposed between the conveyor belt ( 36 F) and the milling drum ( 38 . 1 ), in an extension of the conveyor belt, wherein the support is disposed such that a front distance is left between a front edge of the support and a rear end of the conveyor belt,
the milling drum ( 38 . 1 ) is disposed with an upper working line (H) of a working edge ( 38 . 1 R) of the milling drum ( 38 . 1 ) at the level of or above a receiving surface (F) of a conveyor belt ( 36 F), for mill processing of the dry cake ( 35 ) or of the fragments ( 37 ), where the milling drum ( 38 . 1 ) is designed to eject comminuted dried polymer particles ( 39 ) of the dry cake ( 35 ) or of the fragments ( 37 ) in the downward direction.

2. The belt drier arrangement according to claim 1 , wherein
the milling drum ( 38 . 1 ) has a rotatable shaft (ZF 1 ) with functional elements (ZF 2 ) and the conveyor belt ( 36 F) has a deflecting roll ( 36 U), the rotatable shaft (ZF 1 ) having been designed to rotate with a direction of rotation (R 2 ) counter to a direction of rotation (R 1 ) of the deflecting roll ( 36 U).

3. The belt drier arrangement according to claim 1 , wherein a radius (r) of the milling drum ( 38 . 1 ) is not less than the thickness ( 35 D, 37 D) of the dry cake ( 35 ) or of the fragments ( 37 ).

4. The belt drier arrangement according to claim 1 , wherein the upper working line (H) of the milling drum ( 38 . 1 ) is above an upper edge ( 35 C) of the dry cake or above an upper edge ( 37 C) of the fragments ( 37 ), and/or a lower working line (H) of the milling drum ( 38 . 1 ) is below a receiving surface (F) of a conveyor belt ( 36 F).

5. The belt drier arrangement according to claim 1 , wherein the upper working line (H) of the milling drum ( 38 . 1 ) has an upper distance from the receiving surface (F) of the conveyor belt and the upper distance above the level of the receiving surface (F) of the conveyor belt is at least 5 cm.

6. The belt drier arrangement according to claim 1 , wherein an axis ( 38 . 1 A) of the milling drum ( 38 . 1 ), is at the level of or below the level of a receiving surface (F) of a conveyor belt ( 36 F).

7. The belt drier arrangement according to claim 1 , wherein the support is designed as a support table ( 36 T) with a closed support face, where a rear distance (D) is left between a rear edge of the support table ( 36 T) and a front working edge ( 38 . 1 R) of the milling drum ( 38 . 1 ).

8. The belt drier arrangement according to claim 1 , wherein the support takes the form of a support grid ( 36 G) having laterally interspaced support elements ( 36 B).

9. The belt drier arrangement according to claim 1 , wherein a front part of the support is designed as a support table with a closed support face and a rear part of the support takes the form of a support grid having laterally interspaced support elements.

10. The belt drier arrangement according to claim 8 , wherein functional elements (ZF 2 ) on the milling drum ( 38 . 1 ) can mesh into the interspaces between support elements ( 36 B) of a support grid ( 36 G).

11. The belt drier arrangement according to claim 1 , wherein the comminution arrangement, in addition to the milling drum ( 38 . 1 ) and an optional conveying screw ( 40 ), has a further comminution element and/or guide element ( 38 . 2 ).

12. The belt drier arrangement according to claim 1 , wherein
the comminution arrangement ( 38 ), especially the milling drum, is designed to comminute the dry cake to give dried polymer particles, where the comminuted dried polymer particles have a mass-average particle diameter between 0.5 mm and 10 mm.

13. The belt drier arrangement according to claim 1 , wherein the comminution arrangement ( 38 ) is designed for a dwell time of polymer particles below 90 sec in the comminution arrangement.

14. The belt drier arrangement according to claim 1 , wherein the comminution arrangement is designed to comminute the polymer particles at a temperature between 40° C. and 140° C.

15. The belt drier arrangement according to claim 1 , wherein
the milling drum ( 38 . 1 ) is designed to rotate (R 2 ) the shaft (ZF 1 ) at a speed of rotation of more than 50 rpm and less than 250 rpm.

16. The belt drier arrangement according to claim 1 , wherein
a number of functional elements (ZF 2 ) on the milling drum ( 38 . 1 ) takes the form of a number of rods, teeth, bars, paddle surfaces or toothed, zigzag or knurled elements or edges.

17. The belt drier arrangement according to claim 16 , wherein the milling drum ( 38 . 1 ) has a number of functional elements (ZF 2 ) arranged along a basic profile of a spiral to form a working edge ( 38 . 1 R), and the spiral especially has a screw flight with a flight angle between 20° and 70°.

18. The belt drier arrangement according to claim 17 , wherein the spiral has a single screw flight or the spiral has multiple uniformly directed or opposing screw flights.

19. A method of drying an aqueous polymer gel and of comminuting the dried polymer gel to give dried polymer particles with a belt drier arrangement according to claim 1 , having:
a belt drier ( 36 ) having a drier setup ( 36 A) and a conveyor belt ( 36 F) for receiving and for drying the aqueous polymer gel to give a dry cake ( 35 ) or fragments ( 37 ) on a receiving surface (F) of the conveyor belt ( 36 F),
a comminution arrangement ( 38 ), disposed downstream of the drier setup in product flow direction, for comminution of the dried polymer gel of the dry cake ( 35 ) or fragments ( 37 ) to give dried comminuted polymer particles ( 39 ),
wherein the comminution arrangement ( 38 ) has a comminutor in the form of a milling drum ( 38 . 1 ) and a support for the dry cake ( 35 ) or for the fragments ( 37 ) is disposed between the conveyor belt ( 36 F) and the milling drum ( 38 . 1 ), in an extension of the conveyor belt, wherein the support is disposed such that a front distance is left between a front edge of the support and a rear end of the conveyor belt, and, in the method:
the dried polymer gel of the dry cake ( 35 ) is comminuted to give dried comminuted polymer particles ( 39 ), where
the dry cake ( 35 ) or the fragments ( 37 ) are processed by milling with an upper working line (H) of a working edge ( 38 . 1 R) of the milling drum ( 38 . 1 ) at or above a receiving surface (F) of a conveyor belt ( 36 F) and the milling drum ( 38 . 1 ) ejects the comminuted dried polymer particles ( 39 ) of the dry cake ( 35 ) or fragments ( 37 ) in the downward direction.

20. A production method for production of water-absorbing polymer particles, having the steps of:
polymerizing a monomer solution or suspension to give water-absorbing polymer particles of an aqueous polymer gel, where the solution compri

Assignees

• Basf Se

Inventors

• Bennett Andrea Karen
• Mccormack Paul Walter
• Elliott Mark

Classifications

• B01J20/3078

  Thermal treatment, e.g. calcining or pyrolizing · CPC title

• B01J20/3021

  Milling, crushing or grinding · CPC title

• C08F2500/24

  Polymer with special particle form or size · CPC title

• F26B1/005

  by means of disintegrating, e.g. crushing, shredding, milling the materials to be dried (F26B17/102, F26B17/103 take precedence) · CPC title

• C08F6/06

  Treatment of polymer solutions {(C08F6/001, C08F6/006, C08F6/008, C08F6/02, C08F6/04 take precedence)} · CPC title