Method for producing perfluoroalkadiene compounds

US11001545B2 · US · B2

Patent metadata
FieldValue
Publication numberUS-11001545-B2
Application numberUS-201816482856-A
CountryUS
Kind codeB2
Filing dateFeb 2, 2018
Priority dateFeb 3, 2017
Publication dateMay 11, 2021
Grant dateMay 11, 2021

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  1. Title

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  2. Abstract

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  4. Key dates

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  5. First independent claim

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  6. CPC / IPC classifications

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Abstract

Official abstract text for this publication.

According to a method for producing a perfluoroalkadiene compound represented by general formula (1): CF2═CF—(CF2)n-4—CF═CF2 (1), wherein n is an integer of 4 or more, the method comprising a reaction step of adding a nitrogen-containing compound to a solution of a compound represented by general formula (2): X1CF2—CFX2—(CF2)n-4—CF2X1 (2), wherein n is the same as above, X1 is the same or different and is a halogen atom other than fluorine, and X2 is a halogen atom, the perfluoroalkadiene compound can be obtained at a high yield.

First claim

Opening claim text (preview).

The invention claimed is: 1. A method for producing a perfluoroalkadiene compound represented by general formula (1): CF 2 ═CF—(CF 2 ) n-4 —CF═CF 2   (1) wherein n is an integer of 4 or more, the method comprising a reaction step of adding a nitrogen-containing compound to a solution of a compound represented by general formula (2): X 1 CF 2 —CFX 2 —(CF 2 ) n-4 —CF 2 —CF 2 X 1   (2) wherein n is the same as above, X 1 is the same or different and is a halogen atom other than fluorine, and X 2 is chlorine, bromine, or iodine, and heating at reflux temperature. 2. The production method according to claim 1 , wherein the addition rate of the nitrogen-containing compound is 0.001 to 60 mol/h per mol of the compound represented by general formula (2). 3. The production method according to claim 1 , wherein the nitrogen-containing compound is N,N-dimethylformamide. 4. The production method according to claim 1 , wherein the solution is a solution of an organic solvent. 5. The production method according to claim 4 , wherein the boiling point of the organic solvent is lower than the boiling point of the nitrogen-containing compound. 6. The production method according to claim 1 , wherein in the reaction step, the solution of the compound represented by general formula (2) further comprises zinc or a zinc alloy. 7. The production method according to claim 1 , wherein the nitrogen-containing compound is added after the solution of the compound represented by general formula (2) is heated.

Assignees

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Classifications

  • Etching, surface-brightening or pickling compositions (for glass C03C15/00, {C03C25/66; for mortars, concrete, artificial or natural stone or ceramics C04B41/5338}; for metallic material C23F, C23G1/00, C25F1/00; {for semi-conductors H10P52/40}) · CPC title

  • Halogenated dienes · CPC title

  • C07C17/23Primary

    by dehalogenation · CPC title

  • C07C17/25Primary

    by splitting-off hydrogen halides from halogenated hydrocarbons · CPC title

  • containing halogen · CPC title

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What does patent US11001545B2 cover?
According to a method for producing a perfluoroalkadiene compound represented by general formula (1): CF2═CF—(CF2)n-4—CF═CF2 (1), wherein n is an integer of 4 or more, the method comprising a reaction step of adding a nitrogen-containing compound to a solution of a compound represented by general formula (2): X1CF2—CFX2—(CF2)n-4—CF2X1 (2), wherein n is the same as above, X1 is the same or diffe…
Who is the assignee on this patent?
Daikin Ind Ltd
What technology area does this patent fall under?
Primary CPC classification C07C17/23. Mapped technology areas include Chemistry & Metallurgy.
When was this patent published?
Publication date Tue May 11 2021 00:00:00 GMT+0000 (Coordinated Universal Time) (B2). Legal status and post-grant events are not shown on this page.
What related patents are in patentsdb?
We list 8 related publications on this page (citations in our corpus or others sharing the same primary CPC).