Device for mixing powders by cryogenic fluid

Patent metadata

Field	Value
Publication number	US-10981126-B2
Application number	US-201615772340-A
Country	US
Kind code	B2
Filing date	Nov 3, 2016
Priority date	Nov 4, 2015
Publication date	Apr 20, 2021
Grant date	Apr 20, 2021

Abstract

A device for mixing powders by cryogenic fluid, characterised in that it comprises at least: a chamber for mixing powders, comprising a cryogenic fluid; a chamber for supplying powders in order to allow the powders to be introduced into the mixing chamber; means for agitation in the mixing chamber so as to allow the mixing of the powders placed in suspension in the cryogenic fluid.

First claim

The invention claimed is:

1. A device for mixing powders by a cryogenic fluid, comprising:
a plurality of mixing chambers, each mixing chamber comprising an agitator and a cryogenic fluid, wherein the mixing chambers are arranged successively in series one after the other;
a plurality of supplying chambers configured to introduce the powders into at least a first mixing chamber;
a plurality of restricting systems, each restricting system being located between two successive mixing chambers, wherein each restricting system is configured to constrain the distribution of powders from one mixing chamber to the next, and wherein each restricting system is configured to adjust the flow of the powders through each successive mixing chamber; and
an electrostatic charge system for electrostatically charging the powders intended to be introduced into the mixing chambers.

2. The device as claimed in claim 1 , wherein the cryogenic fluid is liquefied nitrogen.

3. A device for mixing powders by a cryogenic fluid, comprising:
a plurality of mixing chambers, each mixing chamber comprising an agitator, wherein each mixing chamber is configured to accept a cryogenic fluid, wherein the mixing chambers are arranged successively in series one after the other;
a plurality of supplying chambers configured to introduce the powders into at least a first mixing chamber;
a plurality of restricting systems, each restricting system located between two successive mixing chambers, wherein each restricting system is configured to constrain the distribution of powders from one mixing chamber to the next, and wherein each restricting system is configured to adjust the flow of the powders through each successive mixing chambers; and
an electrostatic charge system for electrostatically charging the powders intended to be introduced into the mixing chambers.

4. The device according to claim 3 , wherein the cryogenic fluid comprises a liquified gas.

5. The device as claimed in claim 3 , wherein each agitator comprises mobile mixing devices.

6. The device according to claim 5 , wherein the mobile mixing devices comprise mobile grinding facilities.

7. The device as claimed in claim 3 , wherein each agitator comprises a device capable of generating vibrations.

8. The device as claimed in claim 3 , wherein the restricting systems comprise screens.

9. The device as claimed in claim 3 , wherein the restricting systems comprise diaphragms.

10. The device as claimed in claim 3 , wherein the restricting systems progressively restrict the flow of the powders through the plurality of mixing chambers such that a section of passage of an (n−1)th restricting system is configured to pass powder particles that are larger or at a greater rate than the powder particles passed by an nth restricting system.

11. The device as claimed in claim 3 , wherein a section of the restricting systems is less than a section length necessary for the powders to agglomerate.

12. The device as claimed in claim 3 , wherein the plurality of mixing chambers and the plurality of the restricting systems are arranged along the same vertical direction in such a way as to allow for a flow of powders under the effect of gravity.

13. The device according to claim 3 , wherein a portion of the powders is put into contact with a portion of the electrostatic charge system in order to be positively electrostatically charged and wherein the other portion of the powders is put into contact with the other portion of the electrostatic charge system in order to be negatively electrostatically charged, in order to allow for a differentiated local agglomeration.

14. The device as claimed in claim 3 , wherein the supplying chambers comprise hoppers with an adjustable supply and/or metering systems.

15. The device as claimed in claim 3 , wherein each agitator further comprises a gyroscopic agitator.

16. The device as claimed in claim 3 , wherein each mixing chamber further comprises a second means of agitation in the form of a device capable of producing ultrasonic vibrations further comprising sonotrodes.

17. The device as claimed in claim 3 , wherein each agitator is configured to create a suspension comprising the powders and the cryogenic fluid.

18. A method for mixing powders by a cryogenic fluid, employing the device of claim 3 , comprising the following steps:
a) introducing powders intended to be mixed into the mixing chambers through one or more of the supplying chambers,
b) mixing the powders in the mixing chambers to form a suspension of the powders in a cryogenic fluid and,
c) obtaining a mixture formed from the powders.

19. The method according to claim 18 , further comprising during the first step a), electrostatically charging the powders with positive or negative charges in order to favor differentiated local agglomeration.

20. The method according to claim 18 , comprising the step of progressively restraining the passage of the flow of the powders through the mixing chambers through the restricting systems with a decreasing section of passage according to the flow of the powders.

21. The method according to claim 18 , wherein the powders to be mixed are actinide powders.

Assignees

• Commissariat Energie Atomique

Inventors

• Brothier Méryl
• Vaudez Stéphane

Classifications

• B01F31/80

  Mixing by means of high-frequency vibrations above one kHz, e.g. ultrasonic vibrations · CPC title

• B01F27/60

  with stirrers rotating about a horizontal or inclined axis · CPC title

• B01F23/705

  Submitting materials to electrical energy fields to charge or ionize them · CPC title

• B01F23/66 Primary

  by evaporating or liquefying at least one of the components; using a fluid which is evaporated after mixing · CPC title

• B01F23/60

  Mixing solids with solids · CPC title