Apparatus for the distillation of air by cryogenic distillation

Patent metadata

Field	Value
Publication number	US-10969167-B2
Application number	US-201916655977-A
Country	US
Kind code	B2
Filing date	Oct 17, 2019
Priority date	Oct 29, 2018
Publication date	Apr 6, 2021
Grant date	Apr 6, 2021

Abstract

An apparatus for the distillation of air by cryogenic distillation is provided. The apparatus can include an enclosure; a first distillation column configured to operate at a first pressure; a second distillation column configured to operate at a second pressure that is lower than the first pressure, the second distillation column being placed above the first distillation column and forming therewith a double column; a subcooling heat exchanger configured to cool at least one liquid from the first distillation column upstream of the second distillation column and configured to warm a gaseous nitrogen stream from the second distillation column; and an argon column configured to separate an argon enriched stream from the second distillation column and configured to produce an argon rich stream. In certain embodiments, the first distillation column, the second distillation column, the argon column and the subcooling heat exchanger are disposed within the enclosure, and/or the subcooling heat exchanger is disposed directly underneath the first distillation column or the argon column.

First claim

The invention claimed is:

1. An apparatus for the distillation of air by cryogenic distillation comprising:
an enclosure;
a first distillation column configured to operate at a first pressure;
a second distillation column configured to operate at a second pressure that is lower than the first pressure, the second distillation column being placed above the first distillation column and forming therewith a double column;
a subcooling heat exchanger configured to cool at least one liquid from the first distillation column upstream of the second distillation column and configured to warm a gaseous nitrogen stream from the second distillation column; and
an argon column configured to separate an argon enriched stream from the second distillation column and configured to produce an argon rich stream,
wherein the first distillation column, the second distillation column, the argon column and the subcooling heat exchanger are disposed within the enclosure,
wherein the subcooling heat exchanger is disposed directly underneath the first distillation column or the argon column.

2. The apparatus according to claim 1 , wherein the double column is shorter than the argon column and the subcooling heat exchanger is placed directly underneath the first distillation column.

3. The apparatus according to claim 2 , wherein the first and second distillation columns and possibly the subcooling heat exchanger are supported by a supporting structure.

4. The apparatus according to claim 3 , wherein the base of the argon column is lower than the top of the supporting structure.

5. The apparatus according to claim 1 , wherein the sum of the heights of the supporting structure and the first distillation column and the second distillation column are substantially equal to the sum of the heights of the argon column and a supporting structure of the argon column.

6. The apparatus according to claim 1 , wherein the double column is longer than the argon column and the subcooling heat exchanger is placed directly underneath the argon column.

7. The apparatus according to claim 6 , wherein the base of the argon column and possibly the subcooling heat exchanger is/are supported by a supporting structure.

8. The apparatus according to claim 6 , wherein the sum of the heights of the argon column and the supporting structure is substantially equal to the sum of the heights of the double column and of a supporting structure for the double column.

9. The apparatus according to claim 1 further comprising a heat exchanger for cooling air to feed the first column, said heat exchanger being outside the enclosure.

Assignees

• Air Liquide

Inventors

• Cavagne Patrice
• Kurtz Remy

Classifications

• F25J3/0443

  A main column system not otherwise provided, e.g. a modified double column flowsheet · CPC title

• F25J2245/50

  the recycled stream being oxygen · CPC title

• F25J2215/40

  Air or oxygen enriched air, i.e. generally less than 30mol% of O2 · CPC title

• F25J2200/52

  in the high pressure column of a double pressure main column system · CPC title

• F25J2215/50

  Oxygen or special cases, e.g. isotope-mixtures or low purity O2 · CPC title