Methods for minimizing SHR in glass articles by producing a gas flow during pharmaceutical part converting

Patent metadata

Field	Value
Publication number	US-10968133-B2
Application number	US-201816201043-A
Country	US
Kind code	B2
Filing date	Nov 27, 2018
Priority date	Nov 30, 2017
Publication date	Apr 6, 2021
Grant date	Apr 6, 2021

Abstract

Systems for producing articles from glass tube include a converter having a base with a plurality of processing stations and a turret moveable relative to the base. The turret indexes a plurality of holders for holding the glass tubes successively through the processing stations. The systems further include a gas flow system or a suction system for producing a flow of gas through the glass tube during one or more heating, forming, separating or piercing operations. The flow of gas through the glass tube produced by the gas flow system or suction system may be sufficient to evacuate or purge volatile constituents of the glass from the glass tube and/or pierce a meniscus formed on the glass tube during separation, thereby reducing the Surface Hydrolytic Response (SHR) of the interior surface of the glass tube and articles made therefrom.

First claim

What is claimed is:

1. A method for producing an article from a glass tube having an inner surface, the method comprising:
introducing the glass tube to a converter having a plurality of processing stations comprising at least one heating station, at least one forming station, and a separating station;
heating a proximal end of the glass tube at the at least one heating station, wherein alkali is released from the glass tube during the heating;
forming at least one feature of the article at the proximal end of the glass tube in the at least one forming station;
separating the article from the proximal end of the glass tube at the separating station; and
producing a flow of gas adjacent to the proximal end of the glass tube by introducing a gas pulse into the glass tube through a distal end of the glass tube, wherein:
the gas pulse is introduced in one or more of the plurality of processing stations or between any two of the plurality of processing stations; and
the flow of gas is operable to remove at least a portion of the atmosphere in an interior of the glass tube.

2. The method of claim 1 , wherein contamination of the inner surface by the alkali released from the glass tube is at least reduced.

3. The method of claim 1 , wherein separating the article from the glass tube comprises thermally separating the article from the glass tube, wherein a meniscus of glass is formed on the proximal end of the glass tube during thermal separation and producing the flow of gas adjacent to the proximal end the glass tube further comprises opening the meniscus of glass.

4. The method of claim 1 , wherein separating the article from the glass tube comprises thermally separating the article from the glass tube and forming a meniscus of glass across a proximal end of the glass tube, wherein the gas pulse is sufficient to open the meniscus of the glass tube.

5. The method of claim 1 , wherein the gas pulse has a duration less than a sum of a dwell time and an index time of the converter.

6. The method of claim 1 , further comprising controlling at least one of a duration of the gas pulse, a pressure of the gas pulse, or a volume flow rate of the gas pulse in response to changes in the tube diameter, wall thickness, glass type, converter operating temperatures, or combinations of these.

7. The method of claim 1 , wherein the flow of gas adjacent to the proximal end of the glass tube is produced when the glass tube is positioned in at least one of the plurality of processing stations.

8. The method of claim 1 , further comprising indexing the glass tube between two of the plurality of processing stations, wherein the flow of gas adjacent to the proximal end of the glass tube is produced while indexing the glass tube between the two of the plurality of processing stations.

9. A method for producing an article from a glass tube having an inner surface, the method comprising:
introducing the glass tube to a converter having a plurality of processing stations comprising at least one heating station, at least one forming station, and a separating station;
heating a proximal end of the glass tube at the at least one heating station, wherein alkali is released from the glass tube during the heating;
forming at least one feature of the article at the proximal end of the glass tube in the at least one forming station;
separating the article from the proximal end of the glass tube at the separating station; and
producing a flow of gas adjacent to the proximal end of the glass tube, wherein:
producing the flow of gas adjacent to the proximal end of the glass tube comprises producing a negative pressure pulse adjacent to the proximal end of the glass tube;
the negative pressure pulse is produced in one or more of the plurality of processing stations or between any two of the plurality of processing stations; and
the flow of gas is operable to remove at least a portion of the atmosphere in an interior of the glass tube.

10. The method of claim 9 , wherein contamination of the inner surface by the alkali released from the glass tube is at least reduced.

11. The method of claim 9 , wherein producing a negative pressure pulse adjacent to the proximal end of the glass tube comprises producing a positive flow of gas orthogonal to a longitudinal axis of the glass tube across the proximal end of the glass tube.

12. The method of claim 9 , wherein producing a negative pressure pulse adjacent to the proximal end of the glass tube comprises producing a positive flow of gas external to the glass tube and at a non-zero angle with the longitudinal axis of the glass tube.

13. The method of claim 9 , wherein separating the article from the glass tube comprises thermally separating the article from the glass tube and forming a meniscus of glass across the proximal end of the glass tube, wherein the negative pressure pulse is sufficient to open the meniscus.

14. The method of claim 9 , wherein producing a negative pressure pulse adjacent to the proximal end of the glass tube comprises producing the flow of gas radially across a surface of a meniscus of glass formed on the glass tube during thermally separating the article from the glass tube, wherein the flow of gas produces the negative pressure pulse sufficient to open the meniscus.

15. The method of claim 9 , wherein the flow of gas adjacent to the proximal end of the glass tube is produced when the glass tube is positioned in at least one of the plurality of processing stations.

16. The method of claim 9 , further comprising indexing the glass tube between two of the plurality of processing stations, wherein the flow of gas adjacent to the proximal end of the glass tube is produced while indexing the glass tube between the two of the plurality of processing stations.

17. The method of claim 9 , wherein the negative pressure pulse has a duration less than a sum of a dwell time and an index time of the converter.

18. The method of claim 9 , further comprising controlling at least one of a duration of the negative pressure pulse or a negative pressure of the negative pressure pulse in response to changes in the tube diameter, wall thickness, glass type, converter operating temperatures, or combinations of these.

Assignees

• Corning Inc

Inventors

• Gaylo Keith Raymond
• Klingensmith Lewis Kirk
• Matusick Joseph Michael
• Mcenroe David John
• O'Malley Connor Thomas
• Panides Elias
• Trosa Matthew Daniel
• Wagner Steven Robert

Classifications

• C03B23/09

  Reshaping the ends, e.g. as grooves, threads or mouths · CPC title

• C03B23/11

  Reshaping by drawing without blowing, in combination with separating, e.g. for making ampoules · CPC title

• C03B23/049 Primary

  by pressing (C03B21/04 {, C03B23/092}, C03B23/26 take precedence) · CPC title

• C03B23/092

  by pressing · CPC title

• C03B35/26

  Transporting of glass tubes or rods · CPC title