Multiple-bed catalytic reactor comprising a mixing device

Patent metadata

Field	Value
Publication number	US-10940448-B2
Application number	US-201716340909-A
Country	US
Kind code	B2
Filing date	Nov 3, 2017
Priority date	Nov 16, 2016
Publication date	Mar 9, 2021
Grant date	Mar 9, 2021

Abstract

The present invention relates to multi-bed catalytic reactor with a cylindrical shape comprising a mixing device mounted between two catalyst beds in the reactor, said mixing device has a circular outer rim which corresponds to the inner wall of the reactor, the mixing device comprises; collecting means disposed in a collecting section for collecting fluid from an up¬stream catalytic bed, mixing means disposed in a mixing section for mixing the collected fluid comprising guide vanes and guide ramps, and discharging means disposed in a discharging section for discharging the mixed fluid to a down-stream catalytic bed; wherein the collecting section, the mixing section and the discharging section are disposed outside the center of the circular cross-section of the reactor, as well as associated methods for mixing and the use of such a mixing device in catalytic reactors.

First claim

The invention claimed is:

1. A multi-bed catalytic reactor with a cylindrical shape comprising a mixing device mounted between two catalyst beds in said reactor, said mixing device has a circular outer rim adapted to fit within the inner wall of the reactor, the mixing device comprises:
collecting means disposed in a collecting section for collecting fluid from an up-stream catalytic bed,
mixing means disposed in a mixing section comprising a floor, a ceiling and inner and outer walls for mixing the collected fluid, and
discharging means disposed in a discharging section for discharging the mixed fluid to a down-stream catalytic bed;
wherein the mixing device has a donut shape with a central open space, and the collecting section, the mixing section and the discharging section are disposed in the radial outer third of the circular cross-sectional area of the reactor, and the central open space occupies the radial inner two-thirds of the circular cross-sectional area of the reactor, and
wherein said mixing means comprise guide vanes with a first and a second end, guide ramps with a first and a second end, or comprises said guide vanes and said guide ramps.

2. A multi-bed catalytic reactor with a cylindrical shape comprising a mixing device according to claim 1 , wherein the floor of said mixing section comprises guide vanes.

3. A multi-bed catalytic reactor with a cylindrical shape comprising a mixing device according to claim 1 , wherein the outer wall of said mixing section comprises guide ramps.

4. A multi-bed catalytic reactor with a cylindrical shape comprising a mixing device according to claim 1 , wherein the ceiling of said mixing section comprises guide vanes.

5. A multi-bed catalytic reactor with a cylindrical shape comprising a mixing device according to claim 1 , wherein said guide vanes have an inwards progression when seen in the flow direction from the collecting section to the discharging section and the inwards progression relative to the length of the guide vanes is less than 1 to 2.

6. A multi-bed catalytic reactor with a cylindrical shape comprising a mixing device according to claim 1 , wherein said guide ramps have an upwards progression when seen in the flow direction from the collecting section to the discharging section and the upwards progression relative to the length of the guide vanes is less than 1 to 2.

7. A multi-bed catalytic reactor with a cylindrical shape comprising a mixing device according to claim 1 , wherein said guide vanes have a height which is less than one third of the cross sectional width of said mixing section.

8. A multi-bed catalytic reactor with a cylindrical shape comprising a mixing device according to claim 1 , wherein said guide ramps have a height which is less than one third of the cross sectional height of said mixing section.

9. A multi-bed catalytic reactor with a cylindrical shape comprising a mixing device according to claim 1 , wherein the guide vanes and guide ramps are made from plate with a thickness between 0.25 and 4 mm.

10. A multi-bed catalytic reactor with a cylindrical shape comprising a mixing device according to claim 1 , wherein the first end of each guide vane is arranged adjacent to the outer wall of said mixing section and the second end of each guide vane is arranged adjacent to the inner wall of said mixing section.

11. A multi-bed catalytic reactor with a cylindrical shape comprising a mixing device according to claim 1 , wherein the first end of each guide ramp is arranged adjacent to the floor of said mixing section and the second end of each guide ramp is arranged adjacent to the ceiling of said mixing section.

12. A multi-bed catalytic reactor with a cylindrical shape comprising a mixing device according to claim 1 , wherein the number of guide vanes is between 2 and 200.

13. A multi-bed catalytic reactor with a cylindrical shape comprising a mixing device according to claim 1 , wherein the number of guide ramps is between 2 and 200.

14. A multi-bed catalytic reactor with a cylindrical shape comprising a mixing device according to claim 1 , wherein the outer rim of said mixing device is an integrated part of the reactor wall.

15. A multi-bed catalytic reactor with a cylindrical shape comprising a mixing device according to claim 1 , wherein the collecting means, the mixing means and the discharging means comprise channels comprising circular arc divider walls horizontally dividing one section from another section or dividing one section from the centre of the circular cross-section of the reactor.

16. A multi-bed catalytic reactor with a cylindrical shape comprising a mixing device according to claim 1 , wherein the mixing device further comprises a quench inlet for adding a quench fluid to the collected fluid, said quench inlet is disposed in the collecting section.

17. A multi-bed catalytic reactor with a cylindrical shape comprising a mixing device according to claim 1 , wherein the collecting section is disposed in an upstream axial level of the reactor relative to the discharging section.

18. A multi-bed catalytic reactor with a cylindrical shape comprising a mixing device according to claim 1 , wherein the collecting section is disposed in an outer generally circular cross sectional area of the reactor relative to the mixing section, and the mixing section is disposed in an outer generally circular cross sectional area of the reactor relative to the discharging section.

19. A multi-bed catalytic reactor with a cylindrical shape comprising a mixing device according to claim 1 , wherein the collecting section, the mixing section and the discharging section each is disposed in at least a 120° sector of the generally circular cross sectional area of the reactor.

20. A multi-bed catalytic reactor with a cylindrical shape comprising a mixing device according to claim 1 , wherein the discharging means comprise an inner circular arc divider walls providing a spilling brim for a liquid phase of the fluid.

21. A multi-bed catalytic reactor with a cylindrical shape comprising a mixing device according to claim 1 , wherein the mixing device forms an integrated part of a catalyst bed support of the reactor.

22. A multi-bed catalytic reactor with a cylindrical shape comprising a mixing device according to claim 1 , wherein the mixing device has a height of less than 1 m, preferably less than 0.5 m with respect to the axial direction of the reactor.

Assignees

• Haldor Topsoe As

Inventors

• Holm-Christensen Olav
• Manoharan Karthik Gopal
• Risbjerg Jarlkov Klaus
• Brix Jacob

Classifications

• B01F23/2323 Primary

  by circulating the flow in guiding constructions or conduits · CPC title

• B01F25/10

  Mixing by creating a vortex flow, e.g. by tangential introduction of flow components · CPC title

• B01F2101/2204

  Mixing chemical components in generals in order to improve chemical treatment or reactions, independently from the specific application · CPC title

• B01J8/04

  the fluid passing successively through two or more beds · CPC title

• B01J2208/00938

  Flow distribution elements · CPC title