Electrolytic capacitor containing a valve metal sourced from a conflict-free mine site and a method of forming thereof

Patent metadata

Field	Value
Publication number	US-10937600-B2
Application number	US-201916695540-A
Country	US
Kind code	B2
Filing date	Nov 26, 2019
Priority date	Sep 22, 2016
Publication date	Mar 2, 2021
Grant date	Mar 2, 2021

Abstract

A method of forming an electrolytic capacitor is provided. The method includes obtaining an unverified mineral sample from a mine site, analyzing the unverified mineral sample via quantitative mineralogical analysis and comparing data collected during the quantitative mineralogical analysis for the unverified mineral sample to data in a database that corresponds to quantitative mineralogical analysis collected for verified mineral samples sourced from one or more mine sites from a conflict-free geographic region to determine if the unverified mineral sample is sourced from one or more mine sites from the conflict-free geographic region. If it is determined that the unverified mineral sample is sourced from one or more mine sites from the conflict-free geographic region, the method then involves converting the unverified mineral sample into an anode for the electrolytic capacitor. The electrolytic capacitor can be a solid electrolytic capacitor or a wet electrolytic capacitor.

First claim

What is claimed is:

1. A method of forming an electrolytic capacitor from an unverified mineral sample, the method comprising:
analyzing the unverified mineral sample via quantitative mineralogical analysis and comparing data collected during the quantitative mineralogical analysis for the unverified mineral sample to data in a database that corresponds to quantitative mineralogical analysis collected for verified mineral samples sourced from one or more mine sites from a conflict-free geographic region to determine if the unverified mineral sample is sourced from the one or more mine sites from the conflict-free geographic region, wherein analyzing the unverified mineral sample via quantitative mineralogical analysis comprises performing automated mineralogy testing on the unverified mineral sample and identifying grains for additional testing based on data obtained during automated mineralogy testing, wherein from about 25 grains to about 125 grains are identified for additional testing; and
if it is determined that the unverified mineral sample is sourced from the one or more mine sites from the conflict-free geographic region, converting the unverified mineral sample into an anode for the electrolytic capacitor.

2. The method of claim 1 , further comprising rejecting the unverified mineral sample if it cannot be determined that the mineral sample is sourced from the one or more mine sites from the conflict-free geographic region.

3. The method of claim 1 , wherein the conflict-free geographic region excludes the Democratic Republic of Congo, Angola, Burundi, Central African Republic, Congo Republic, Rwanda, Sudan, Tanzania, Uganda, and Zambia.

4. The method of 1 , further comprising performing one or more chemical assays on the unverified mineral sample, wherein the one or more chemical assays determines the amount of uranium, thorium, or tantalum present in the unverified mineral sample.

5. The method of claim 1 , wherein analyzing the unverified mineral sample via quantitative mineralogical analysis comprises polishing the unverified mineral sample to expose grain interiors present in the unverified mineral sample.

6. The method of claim 1 , further comprising performing electron micro probe analysis (EMPA) on the identified grains.

7. The method of claim 6 , further comprising performing laser ablation inductively coupled plasma spectrometry (LA-ICP-MS) on the identified grains.

8. The method of claim 7 , wherein it is determined that the unverified mineral sample is sourced from the one or mine sites from the conflict-free geographic region if data collected during the automated mineralogy testing, LA-ICP-MS, and/or EMPA for the unverified mineral sample substantially matches data collected during the automated mineralogy testing, LA-ICP-MS, and/or EMPA for one of the verified mineral samples sourced from the one or mine sites from the conflict-free geographic region.

9. The method of claim 1 , wherein the unverified mineral sample comprises a valve metal, wherein the valve metal comprises tantalum, niobium, or a combination thereof.

10. The method of claim 9 , wherein converting the unverified mineral sample into the anode for the electrolytic capacitor comprises:
separating the valve metal from the unverified mineral sample;
forming the valve metal into a valve metal powder;
pressing the valve metal powder to form the anode; and
sintering the anode.

11. The method of claim 10 , further comprising forming a dielectric layer over the sintered anode.

12. The method of claim 1 , wherein the electrolytic capacitor is a solid electrolytic capacitor.

13. The method of claim 12 , wherein the solid electrolytic capacitor includes a solid electrolyte.

14. The method of claim 13 , wherein solid electrolyte includes a conductive polymer or manganese dioxide.

15. The method of claim 1 , wherein the electrolytic capacitor is a wet electrolytic capacitor.

16. The method of claim 15 , wherein the wet electrolytic capacitor includes a cathode comprising a metal substrate coated with a conductive coating and a fluidic working electrolyte in communication with the anode and the cathode.

17. An electrolytic capacitor formed according to the method of claim 1 .

18. The electrolytic capacitor of claim 17 , wherein the electrolytic capacitor is a solid electrolytic capacitor or a wet electrolytic capacitor.

Assignees

• Avx Corp

Inventors

• Millman William A
• Loun Jan

Classifications

• H01G9/048

  characterised by their structure (H01G11/22 takes precedence) · CPC title

• H01G9/0525

  Powder therefor · CPC title

• H01G9/145

  Liquid electrolytic capacitors (H01G11/00 takes precedence) · CPC title

• H01G9/15

  Solid electrolytic capacitors (H01G11/00 takes precedence) · CPC title

• H01G9/07

  Dielectric layers · CPC title