Method for oxidizing a carbon black and a method for preparing the carbon black using the same

Patent metadata

Field	Value
Publication number	US-10920086-B2
Application number	US-201816203952-A
Country	US
Kind code	B2
Filing date	Nov 29, 2018
Priority date	Nov 29, 2017
Publication date	Feb 16, 2021
Grant date	Feb 16, 2021

Abstract

The present invention relates to a method for oxidizing a carbon black which can prevent or alleviate change in the surface oxidation degree of the carbon black by a residual ozone after surface oxidation reforming, and a method for preparing the carbon black by comprising it in a single continuous process.

First claim

What is claimed is:

1. A method for oxidizing a carbon black, comprising the steps of:
(a) generating ozone from oxygen in an ozone generator to obtain a mixed gas of oxygen and ozone;
(b) introducing the mixed gas into an oxidation reactor having each of an inlet and an outlet to oxidize a carbon black in the oxidation reactor;
(c) discharging the mixed gas through the outlet in the oxidation reactor; and
(d) removing the ozone remaining in the oxidized carbon black,
wherein the step (d) is carried out by introducing an inert purge gas into the oxidation reactor.

2. The method for oxidizing the carbon black according to claim 1 , wherein the change in pH of the carbon black measured after the completion of the step (d) compared to pH of the carbon black measured after the completion of the step (b) is less than 0.2, or the rate of change in pH is 5% or less.

3. The method for oxidizing the carbon black according to claim 1 , wherein the inert purge gas is at least one selected from a nitrogen, an argon, a helium and a neon.

4. The method for oxidizing the carbon black according to claim 1 , wherein the step (d) is carried out by raising the temperature in the oxidation reactor.

5. The method for oxidizing the carbon black according to claim 4 , wherein the step (d) is carried out by raising the temperature in the oxidation reactor to 300° C. or more.

6. The method for oxidizing the carbon black according to claim 1 , wherein the step (d) is carried out by rotating the oxidation reactor.

7. The method for oxidizing the carbon black according to claim 1 , wherein the step (d) is carried out in a screw feeder for transferring the oxidized carbon black.

8. The method for oxidizing the carbon black according to claim 7 , wherein the step (d) is carried out by raising the temperature in the screw feeder to 300° C. or more.

9. A method for preparing a carbon black, comprising the steps of:
(a) producing a carbon black in a combustion reactor;
(b) transferring the carbon black produced in the combustion reactor to an oxidation reactor; and
(c) generating ozone from oxygen in an ozone generator to obtain a mixed gas of oxygen and ozone;
(d) introducing the mixed gas into the oxidation reactor having each of an inlet and an outlet to oxidize the carbon black in the oxidation reactor;
(e) discharging the mixed gas through the outlet in the oxidation reactor; and
(f) removing the ozone remaining in the oxidized carbon black,
wherein the step (f) is carried out by introducing an inert purge gas into the oxidation reactor.

Assignees

• Oci Co Ltd

Inventors

• Lee Jae-Seok

Classifications

• C09C1/60

  Agglomerating, pelleting, or the like by dry methods · CPC title

• C09C1/565 Primary

  comprising an oxidative treatment with oxygen, ozone or oxygenated compounds, e.g. when such treatment occurs in a region of the furnace next to the carbon black generating reaction zone · CPC title

• C09C1/58

  Agglomerating, pelleting, or the like by wet methods · CPC title

• C09C1/50

  Furnace black {; Preparation thereof (separation or recovery C09C1/487)} · CPC title