Systems and methods for unipolar separation of emulsions and other mixtures
US-9975064-B2 · May 22, 2018 · US
US10918972B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-10918972-B2 |
| Application number | US-201716073394-A |
| Country | US |
| Kind code | B2 |
| Filing date | Jan 27, 2017 |
| Priority date | Jan 29, 2016 |
| Publication date | Feb 16, 2021 |
| Grant date | Feb 16, 2021 |
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Disclosed is a method for the break-up of at least one emulsion and separation of the light and heavy phase with at least an de-emulsification rate of more than 9% in only one apparatus within less than 5 min by applying at least one time dependent electrical field. The electrical field is a high frequency singular alternating current field with an electrical field strength between 2,000 and 100,000 V/m and a frequency between 12,000 Hz and 200,000 Hz. The present invention relates furthermore to a method for the treatment of at least one emulsion by applying at least one direct current field and at least one high frequency alternating current field.
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The invention claimed is: 1. A method for the separation of at least one liquid/liquid (L/L) emulsion with a water content of up to 70 mass % comprising applying at least one time dependent electrical field, wherein the at least one electrical field is a singular alternating current (AC) field with an electrical field strength between 2,000 and 100,000 V/m and a frequency (HF) between >10,000 Hz and 200,000 Hz, and wherein separation of the at least one L/L emulsion performed with a de-emulsification rate of at least 95% is achieved in less than 5 minutes. 2. The method according to claim 1 , wherein the at least one AC-field is applied with an electrical field strength between 4,000 and 70,000 V/m. 3. The method according to claim 1 , wherein the at least one AC-field is applied with a frequency between 12,000 and 150,000 Hz. 4. The method according to claim 1 , wherein the emulsion to be separated is a phenolic water emulsion of the Hock-synthesis with an equimolar Phenol/Acetone-ratio and water contents up to 70 wt. %. 5. The method according to claim 1 , wherein the at least one AC-field is applied with an electrical field strength between 30,000 and 50,000 V/m and a frequency between 16,000 and 40,000 Hz. 6. The method according to claim 1 , wherein separation of the at least one L/L emulsion performed with a de-emulsification rate of at least 95% is achieved in less than 3 minutes. 7. The method according to claim 1 , wherein separation of the at least one L/L emulsion performed with a de-emulsification rate of at least 95% is achieved in less than 2 minutes.
Separation by high-voltage electrical fields, not provided for in other groups of this subclass · CPC title
Electrostatic separation of liquids from liquids · CPC title
Separation of liquids from each other by electricity · CPC title
with electrical or magnetic means · CPC title
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