Methods and apparatus for optically detecting magnetic resonance

Patent metadata

Field	Value
Publication number	US-10895542-B2
Application number	US-202016871123-A
Country	US
Kind code	B2
Filing date	May 11, 2020
Priority date	Jan 8, 2014
Publication date	Jan 19, 2021
Grant date	Jan 19, 2021

Abstract

A light-trapping geometry enhances the sensitivity of strain, temperature, and/or electromagnetic field measurements using nitrogen vacancies in bulk diamond, which have exterior dimensions on the order of millimeters. In an example light-trapping geometry, a laser beam enters the bulk diamond, which may be at room temperature, through a facet or notch. The beam propagates along a path inside the bulk diamond that includes many total internal reflections off the diamond's surfaces. The NVs inside the bulk diamonds absorb the beam as it propagates. Photodetectors measure the transmitted beam or fluorescence emitted by the NVs. The resulting transmission or emission spectrum represents the NVs' quantum mechanical states, which in turn vary with temperature, magnetic field strength, electric field strength, strain/pressure, etc.

First claim

The invention claimed is:

1. An apparatus, comprising:
a substrate;
a solid-state host including color centers and disposed on the substrate;
a microwave source, disposed on the substrate, to apply an electromagnetic field to the color centers; and
a detector, disposed on the substrate, to detect radiation emitted by the color centers in response to an excitation beam propagating along a propagation path within the solid-state host and to the electromagnetic field, wherein the propagation path follows a chaotic mode of the solid-state host.

2. The apparatus of claim 1 , further comprising a light source, disposed on the substrate, to generate and apply the excitation beam to the solid-state host.

3. The apparatus of claim 2 , wherein the solid-state host includes a facet, and wherein the light source is configured to apply the excitation beam to the facet of the solid-state host.

4. The apparatus of claim 3 , wherein a divergence angle of the excitation beam matches a numerical aperture of the facet.

5. The apparatus of claim 1 , wherein the propagation path includes multiple total internal reflections within the solid-state host.

6. The apparatus of claim 1 , wherein the microwave source includes a microwave antenna disposed on the substrate.

7. The apparatus of claim 1 , wherein the microwave source is configured to apply the electromagnetic field as a sequence of microwave pulses.

8. The apparatus of claim 7 , wherein the sequence of microwave pulses is a Hahn echo sequence or a Ramsey sequence.

9. The apparatus of claim 1 , wherein the detector includes a set of detectors disposed on the substrate, and wherein each detector of the set of detectors is positioned to detect the radiation emitted via a different surface of the solid-state host.

10. The apparatus of claim 1 , wherein the solid-state host is configured for emission of the radiation when held at a temperature from about 273 K to about 300 K.

11. The apparatus of claim 1 , wherein the solid-state host is configured for emission of the radiation when held at a temperature from about 4 K to about 150 K.

12. The apparatus of claim 1 , wherein the solid-state host is configured for emission of the radiation when held at a temperature greater than about 700 K.

13. A portable sensor, including:
a substrate;
a diamond including nitrogen-vacancy (NV) centers and disposed on the substrate, the diamond defining a propagation path and having a set of surfaces;
a microwave antenna, disposed on the substrate and couplable to a microwave source external to the portable sensor, to apply a sequence of microwave pulses to the NV centers;
a set of photodiodes, each photodiode in optical communication with a different surface of the diamond, to detect fluorescence emitted by the NV centers in response to an excitation beam propagating along the propagation path and to the sequence of microwave pulses, wherein the fluorescence is indicative of at least one of a magnetic field experienced by the NV centers, an electric field experienced by the NV centers, a temperature of the NV centers, a pressure exerted on the NV centers, or a strain exerted on the NV centers;
a set of lenses, disposed on the substrate, each lens of the set of lenses disposed between a different photodiode of the set of photodiodes and its corresponding surface, to increase collection, by that photodiode of a portion of the radiation emitted from that surface.

14. The portable sensor of claim 13 , wherein the fluorescence is further indicative of one or more of a number of NV centers addressed in the diamond by the excitation beam, a number of photons emitted by the NV centers excited by the excitation beam per second, or a collection efficiency of one or more photodiodes of the set of photodiodes.

15. The portable sensor of claim 13 , wherein a wavelength of the fluorescence is from about 600 nm to about 800 nm, and wherein each photodiode of the set of photodiodes and its corresponding lens of the set of lenses are collectively configured to collect up to about 20% of the portion of the radiation emitted from the corresponding surface of the set of surfaces of the diamond.

16. The portable sensor of claim 13 , further comprising a laser, disposed on the substrate, to generate and apply the excitation beam to the diamond.

17. The portable sensor of claim 16 , wherein the diamond includes a facet, wherein a divergence angle of the excitation beam matches a numerical aperture of the facet, and wherein the diode laser is configured to apply the excitation beam to the facet of the diamond.

Assignees

• Massachusetts Inst Technology

Inventors

• Clevenson Hannah A
• Englund Dirk

Classifications

• G01R33/323

  Detection of MR without the use of RF or microwaves, e.g. force-detected MR, thermally detected MR, MR detection via electrical conductivity, optically detected MR · CPC title

• G01N24/006 Primary

  using optical pumping (magnetometers using optical pumping G01R33/26, optical pumping of lasers H01S3/091) · CPC title