Method for thermal treatment of a surface coating on a metal part by microwaves

Patent metadata

Field	Value
Publication number	US-10882071-B2
Application number	US-201615561884-A
Country	US
Kind code	B2
Filing date	Mar 25, 2016
Priority date	Mar 27, 2015
Publication date	Jan 5, 2021
Grant date	Jan 5, 2021

Abstract

A process for treating a surface coating of a bulk metal part, comprises the steps of placing, in a cavity, at least one what is called metal part including what is called a surface coating that is able to absorb microwaves at the frequency ν 0 , the cavity being surrounded by one or a plurality of first susceptors the dimensions, material and arrangement of which are configured to screen the microwaves at the frequency ν 0 , in the vicinity of each the metal part, and in emitting the microwaves at the frequency ν 0 into the cavity.

First claim

The invention claimed is:

1. A process for treating a surface coating of a bulk metal part, comprising the steps of:
1) placing, in a cavity, at least one bulk metal part including a surface coating able to absorb microwaves at the frequency ν 0 , said cavity being directly surrounded by one or a plurality of first susceptors having dimensions, material, and an arrangement of which are configured to screen said microwaves at the frequency ν 0 , in the vicinity of each said bulk metal part;
2) emitting said microwaves at the frequency ν 0 into said cavity;
3) placing said one or plurality of first susceptors and said at least one bulk metal part in a first thermal confinement; and
4) surrounding said first thermal confinement with one or a plurality of second susceptors.

2. The process as claimed in claim 1 , wherein said material, arrangement and dimensions of said one or a plurality of first susceptors partially screen said microwaves at the frequency ν 0 , in the vicinity of each said bulk metal part, during the second step of claim 1 .

3. The process as claimed in claim 2 , wherein said arrangement of said one or a plurality of first susceptors forms a first volume and wherein the average of the intensity of the electromagnetic field emitted during the emitting of said microwaves at the frequency ν 0 in an interior of said first volume is:
higher than 1% of the average of the intensity of the electromagnetic field on an exterior of said first volume and
lower than 90% of the average of the intensity of the electromagnetic field on the exterior of said first volume.

4. The process as claimed in claim 3 , comprising a step of causing a receptacle to move, said receptacle being arranged at least partially in the interior of the first volume bounded by said one or a plurality of first susceptors, so as to agitate at least one said bulk metal part in the interior of the receptacle.

5. The process as claimed in claim 4 , wherein said receptacle is a drum able to agitate at least one said bulk metal part by rotating.

6. The process as claimed in claim 3 , wherein the average of the intensity of the electromagnetic field emitted during the emitting of said microwaves ate the frequency ν 0 into said cavity, in the interior of said first volume is higher than 2% of the average of the intensity of the electromagnetic field on the exterior of said first volume in said cavity.

7. The process as claimed in claim 3 , wherein the average of the intensity of the electromagnetic field emitted during the emitting of said microwaves at the frequency ν 0 into said cavity, in the interior of said first volume is higher than 5% of the average of the intensity of the electromagnetic field on the exterior of said first volume in said cavity.

8. The process as claimed in claim 3 , wherein the average of the intensity of the electromagnetic field emitted during the emitting of said microwaves at the frequency ν 0 into said cavity, in the interior of said first volume is lower than 80% of the average of the intensity of the electromagnetic field on the exterior of said first volume in said cavity.

9. The process as claimed in claim 1 , wherein said surface coating has an electrical conductivity lower than the electrical conductivity of a bulk material of each said bulk metal part.

10. The process as claimed in claim 1 , further comprising a step of measuring, during at least some of the step comprising emitting said microwaves, the temperature of said coating, then regulating the emission power of said microwaves depending on said measured temperature.

11. The process as claimed in claim 1 , wherein said arrangement of said one or a plurality of second susceptors forms a second volume bounded by said one or a plurality of second susceptors and wherein the average of the intensity of the electromagnetic field emitted during the emitting of said microwaves at the frequency ν 0 , in the interior of said second volume is: higher than 1% of the average of the intensity of the electromagnetic field on the exterior of said second volume and lower than 90% of the average of the intensity of the electromagnetic field on the exterior of said second volume.

12. The process as claimed in claim 11 , comprising a step of placing a plurality of at least one bulk metal part in the vicinity of one or a plurality of third susceptors arranged in an interior of the first volume bounded by said one or a plurality of first susceptors.

13. The process as claimed in claim 12 , wherein the material of said one or a plurality of first susceptors, and a material of said one or a plurality of second susceptors and a material of said one or a plurality of third susceptors is chosen from a refractory and semiconductor oxide of a transition metal, and a carbide.

14. The process as claimed in claim 12 , wherein the material of said one or a plurality of first susceptors, and a material of said one or a plurality of second susceptors and a material of said one or a plurality of third susceptors is chosen from silicon carbide and lanthanum chromite.

15. The process as claimed in claim 11 , wherein the average of the intensity of the electromagnetic field emitted during the emitting of said microwaves at the frequency no into said cavity, in the interior of said first volume is higher than 2% of the average of the intensity of the electromagnetic field on the exterior of the second volume.

16. The process as claimed in claim 11 , wherein the average of the intensity of the electromagnetic field emitted during the emitting of said microwaves at the frequency ν 0 into said cavity, in the interior of said first volume is higher than 5% of the average of the intensity of the electromagnetic field on the exterior of the second volume.

17. The process as claimed in claim 11 , wherein the average of the intensity of the electromagnetic field emitted during the emitting of said microwaves at the frequency ν 0 into said cavity, in the interior of said first volume is lower than 80% of the average of the intensity of the electromagnetic field on the exterior of the second volume.

18. The process as claimed in claim 1 , comprising a step of placing said one or a plurality of second susceptors and said first thermal confinement in a second thermal confinement.

19. A process for calcinating said coating as claimed in claim 1 .

20. A process for cross linking said coating as claimed in claim 1 .

Assignees

• Centre Nat Rech Scient
• Ecole Nat Superieure Dingenieurs De Caen

Inventors

• Marinel Sylvain
• Savary Etienne
• Thuault Anthony
• Heuguet Romain

Classifications

• B05D3/0254 Primary

  After-treatment · CPC title

• B05D2202/00

  Metallic substrate · CPC title

• H05B6/80

  Apparatus for specific applications (stoves or ranges F24C7/02) · CPC title

• C08J2327/22

  modified by chemical after-treatment · CPC title

• C08J7/08

  Heat treatment · CPC title